Analytical Raman spectroscopy:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York u.a.
Wiley
1991
|
| Schriftenreihe: | Chemical analysis
114 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVIII, 462 S. graph. Darst. |
| ISBN: | 0471519553 |
Internformat
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Datensatz im Suchindex
| _version_ | 1809946422170091520 |
|---|---|
| adam_text |
ANALYTICAL RAMAN SPECTROSCOPY EDITED BY JEANETTE G. GRASSELLI DEPARTMENT
OF CHEMISTRY OHIO UNIVERSITY ATHENS, OHIO AND BERNARD J. BULKIN BP
RESEARCH CENTRE SUNBURY-ON-THAMES MIDDLESEX, ENGLAND A
WILEY-INTERSCIENCE PUBLICATION JOHN WILEY & SONS, INC. NEW YORK /
CHICHESTER / BRISBANE / TORONTO / SINGAPORE CONTENTS CHAPTER 1 THE RAMAN
EFFECT: AN INTRODUCTION 1 BERNARD J. BULKIN 1.1. BACKGROUND 1 1.2.
CLASSICAL DESCRIPTION OF RAMAN SPECTROSCOPY 4 1.3. RESULT OF QUANTUM
MECHANICAL TREATMENT OF RAMAN SCATTERING 8 1.4. SELECTION RULES:
CONTRASTING IR AND RAMAN SPECTRA 9 1.5. DEPOLARIZATION RATIOS 12 1.6.
RESONANCE RAMAN EFFECT 13 1.7. NONLINEAR RAMAN EFFECTS 15 1.8. GUIDE TO
THE LITERATURE OF RAMAN SPECTROSCOPY 17 REFERENCES 18 CHAPTER 2 MODERN
RAMAN INSTRUMENTATION AND TECHNIQUES D. BRUCE CHASE 21 2.1. 2.2.
INTRODUCTION COMPONENTS OF MODERN RAMAN SPECTROMETERS 2.2.1. SOURCES
2.2.1.1. CONTINUOUS WAVE LASERS 2.2.1.2. PULSED LASERS 2.2.1.3. LENSES
AND FILTERS 2.2.2. COLLECTION OPTICS 2.2.3. DISPERSIHG OPTICAL ELEMENTS:
MONOCHROMATORS 2.2.4. DETECTION SYSTEMS 2.2.4.1. SINGLE-CHANNEL SYSTEMS
21 22 22 22 24 24 26 28 29 29 IX X CONTENTS 2.2.4.2. MULTICHANNEL
SYSTEMS 2.2.4.3. COMPUTERS IN DETECTION SYSTEMS 2.3. SAMPLE HANDLING
2.3.1. GENERAL 2.3.2. MICROSAMPLING 2.4. PROBLEMS: FLUORESCENCE AND
THERMAL SAMPLE DEGRADATION 2.5. FOURIER TRANSFORM RAMAN SPECTROSCOPY
2.5.1. COMPONENTS 2.5.2. EXAMPLES OF THE ADVANTAGES OF FOURIER TRANSFORM
RAMAN MEASUREMENTS 2.5.3. PROBLEMS 2.6. FUTURE EFFORTS 2.7. ADDENDUM
2.7.1. LASERS 2.7.2. LENSES AND FILTERS 2.7.3. MONOCHROMATORS 2.7.4.
DETECTORS 2.7.5. MICROSAMPLING 2.7.6. FT-RAMAN SPECTROSCOPY REFERENCES
29 30 30 30 30 31 32 32 35 36 37 39 39 40 40 40 41 41 42 CHAPTER 3
EXPERIMENTAL CONSIDERATIONS FOR ACCURATE POLARIZATION MEASUREMENTS 45
JAMES R. SCHERER 3.1. INTRODUCTION 3.2. TOOLS FOR TUNING 3.3. LIGHT PATH
GEOMETRY 3.4. SAMPLE CONTAINER 3.5. POLARIZATION SCRAMBLER 3.6. THE
ANALYZER 3.7. POLARIZATION ORIENTATION OF THE EXCITATION LASER BEAM 3.8.
STANDARD RAMAN MEASUREMENT REFERENCES 45 46 47 53 54 56 56 57 57
CONTENTS XI CHAPTER 4 RAMAN SPECTROSCOPY OF INORGANIC SPECIES IN
SOLUTION 59 DONALD E. IRISH AND TORU OZEKI 4.1. INTRODUCTION 59 4.2.
IDENTIFICATION OF INORGANIC SPECIES IN SOLUTION 60 4.2.1. PRAESENTATION
OF THE RAMAN SPECTRUM 60 4.2.2. INTERPRETATION 62 4.3. QUANTITATIVE
ANALYSIS 76 4.3.1. CORRELATING RAMAN INTENSITIES AND SPECIES
CONCENTRATIONS 76 4.3.2. SPECTRAL ANALYSIS WITH BANDFITTING PROGRAMS 80
4.3.3. FACTOR ANALYSIS 83 4.3.4. THE GAUSS-Z PROGRAM 87 4.3.5. RAMAN
DIFFERENCE SPECTROSCOPY 90 4.4. CONCLUSION 90 APPENDIX 91
ACKNOWLEDGMENTS 103 REFERENCES 104 CHAPTER 5 QUANTITATIVE ANALYSIS BY
RAMAN SPECTROSCOPY 107 THOMAS J. VICKERS AND CHARLES K. MANN 5.1.
INTRODUCTION 107 5.2. HISTORICAL DEVELOPMENT 108 5.3. VARIATIONS IN
SOURCE, SAMPLE, AND OPTICS: EFFECT ON QUANTITATIVE ANALYSES 109 5.3.1.
ORDINATE ERRORS 110 5.3.2. ABSCISSA ERRORS 115 5.3.3. DATA TREATMENT 116
5.3.4. MULTICHANNEL VERSUS SCANNING MEASUREMENTS 123 5.4. FLUORESCENCE
AND RAMAN MEASUREMENTS 124 5.5. COMPARISON OF RAMAN AND IR MEASUREMENTS
FOR QUANTITATIVE ANALYSIS 127 XLL CONTENTS 5.5.1. SOLVENT BEHAVIOR 128
5.5.2. EMISSION VERSUS ABSORPTION 128 5.5.3. EXPERIMENTAL FLEXIBILITY
129 5.5.4. EXPERIMENTAL COMPARISON OF SENSITIVITY 130 ACKNOWLEDGMENTS
132 REFERENCES 133 CHAPTER 6 CHARACTERIZATION OF SEMICONDUCTORS BY RAMAN
SPECTROSCOPY 137 FRED H. POLLAK 6.1. INTRODUCTION 137 6.2. GENERAL
BACKGROUND OF RAMAN SCATTERING, PARTICULARLY RELATING TO CRYSTALLINE
SOLIDS 138 6.2.1. POLARIZABILITY THEORY OF RAMAN SCATTERING 138 6.2.2.
SECOND-ORDER RAMAN SCATTERING 141 6.2.3. LATTICE POLARIZABILITY
INCLUDING FREE CARRIER EFFECTS 142 6.2.4. FANO EFFECT 146 6.2.5.
POLARIZATION SELECTION RULES 146 6.2.5.1. ATOMIC DISPLACEMENT EFFECTS
147 6.2.5.2. LINEAR-Q AND SURFACE ELECTRIC FIELD-INDUCED EFFECTS 150
6.2.6. DISPERSION RELATIONS FOR LATTICE VIBRATIONS 152 6.3.
INSTRUMENTATION 154 6.4. SILICON AND OTHER GROUP IV SEMICONDUCTORS 157
6.4.1. MICROCRYSTALLINE GEOMETRIES 157 6.4.2. STRUCTURAL AND
CRYSTALLIZATION EFFECTS IN A-SI, A-GE, AND A-C 163 6.4.3. ION DAMAGE AND
LASER ANNEALING 167 6.4.4. REACTIVE ION ETCHING 170 6.4.5. STRAIN
EFFECTS 172 6.4.6. THE METAL/SI INTERFACE 174 6.4.7. LASER WRITING OF SI
MICROSTRUCTURES 180 6.4.8. TEMPERATURE PROBE 180 6.5. BINARY ZINCBLENDE
SEMICONDUCTORS 180 CONTENTS XLLL 6.5.1. CARRIER CONCENTRATION AND
SPACE/CHARGE LAYER EFFECTS 6.5.2. MICROCRYSTALLINE EFFECTS 6.5.3.
SYMMETRY-FORBIDDEN TRANSVERSE OPTICAL MODE SCATTERING 6.5.4. ION
IMPLANTATION AND ANNEALING 6.5.5. PROCESS-INDUCED DAMAGE 6.6. ALLOY
SEMICONDUCTORS 6.6.1. ALLOY COMPOSITION 6.6.2. ALLOY POTENTIAL
FLUCTUATIONS 6.6.2.1. OPTIC PHONONS 6.6.2.2. DISORDER-ACTIVATED
ZONE-EDGE PHONONS 6.6.3. ION IMPLANTATION AND ANNEALING 6.6.4. CARRIER
CONCENTRATION 6.6.5. HG^CD^TE 6.6.6. HETEROJUNCTIONS 6.6.7. TWO-PHONON
RAMAN SCATTERING 6.7. SURFACE FILMS INCLUDING OXIDES REFERENCES 181 185
186 186 193 200 200 200 200 205 206 206 207 208 209 211 214 CHAPTER 7
POLYMER APPLICATIONS 223 BERNARD J. BULKIN 7.1. INTRODUCTION 223 7.2.
RAMAN SPECTRUM OF POLYETHYLENE TEREPHTHALATE) 224 7.3. VIBRATIONAL
ANALYSIS OF POLYMERS AS A FOUNDATION TO UNDERSTANDING 226 7.4.
SENSITIVITY OF THE RAMAN SPECTRUM TO CONFORMATIONAL CHANGE 230 7.5.
LOW-FREQUENCY ( 200CM" L ) SPECTRA 231 7.6. FEATURES IN THE SPECTRA OF
FIBERS 233 7.7. CONSIDERATIONS IN SELECTING SPECTROSCOPIC PARAMETERS FOR
COMPARING SPECTRA 235 7.8. ORIENTATION, CONFORMATION, AND CRYSTALLINITY
237 7.9. AMORPHOUS ORIENTATION AND LOW-FREQUENCY SPECTRA 242 7.10.
DERIVATION OF POLYMER SPECIFIC HEATS 244 XIV CONTENTS 7.11. A GUIDE TO
OTHER RAMAN STUDIES OF POLYMERS 7.12. CONCLUSION REFERENCES 248 251 251
CHAPTER 8 ANISOTROPIC SCATTERING PROPERTIES OF UNIAXIALLY ORIENTED
POLYMERS: RAMAN STUDIES JOHN F. RABOLT 253 8.1. INTRODUCTION 8.2.
EXPERIMENTAL SCATTERING GEOMETRY 8.3. GEOMETRIE CONSIDERATIONS 8.4.
SYMMETRY CONSIDERATIONS 8.5. EXAMPLE: PLANAR ZIGZAG POLY(VINYLIDENE
FLUORIDE) ACKNOWLEDGMENT REFERENCES 253 254 256 257 269 273 273 CHAPTER
9 ORGANIC AND PETROCHEMICAL APPLICATIONS OF RAMAN SPECTROSCOPY 275
DONALD L. GERRARD 9.1. INTRODUCTION 275 9.2. ORGANIC AND PETROCHEMICAL
SAMPLE-HANDLING TECHNIQUES 277 9.2.1. VERSATILITY AND SIMPLICITY OWING
TO THE SCATTERING PROCESS 277 9.2.2. GLASS SAMPLE CONTAINERS AND AQUEOUS
SYSTEMS 279 9.2.3. EXCITATION USING VISIBLE LASERS 282 9.2.3.1. USEOF
FIBER OPTICS 283 9.3 CHARACTERIZATION OF NONPOLAR GROUPS 286 9.4.
QUANTITATIVE STUDIES 288 9.4.1. INTERNAL STANDARD METHOD 289 9.4.2.
REACTING SYSTEMS 290 9.5. SPATIAL RESOLUTION: RAMAN MICROSCOPY 291 9.6.
METHODS OF SIGNAL ENHANCEMENT 295 9.6.1. RESONANCE-ENHANCED RAMAN
CONTENTS XV SPECTROSCOPY AND APPLICATIONS IN ORGANIC AND PETROCHEMICAL
SYSTEMS 295 9.6.2. SURFACE-ENHANCED RAMAN SPECTROSCOY AND APPLICATIONS
301 9.6.2.1. ELECTROCHEMICAL APPLICATIONS 303 9.6.2.2. COLLOIDS 303
9.6.2.3. METAL-ISLAND FILMS 303 9.6.2.4. GENERAL ANALYTICAL APPLICATIONS
FOR ORGANIC MATERIALS 304 9.7. TIME-RESOLVED STUDIES: EXAMPLES OF IN
SITU STUDIES OF REACTING SYSTEMS 304 9.7.1. HOMOPOLYMERIZATION OF
STYRENE 308 9.7.2. HOMOPOLYMERIZATION OF METHYL METHACRYLATE 310 9.7.3.
COPOLYMERIZATIONS AND MULTICOMPONENT POLYMERIZATIONS: THE USE OF
MATHEMATICAL DECONVOLUTION 311 9.7.4. OTHER APPLICATIONS 312 9.8.
FLUORESCENCE IN ORGANIC SYSTEMS 312 9.8.1. FLUORESCENCE REDUCTION 313
9.8.1.1. SAMPLE PURISSCATION 313 9.8.1.2. "BURNING OUT" WITH THE LASER
BEAM 313 9.8.1.3. THE USE OF UV AND NEAR-IR LASERS 314 9.8.1.4.
FLUORESCENCE-QUENCHING AGENTS 315 9.8.1.5. ANTI-STOKES RAMAN
SPECTROSCOPY 316 9.8.2. EXTRACTION OF THE RAMAN SIGNAL FROM THE
FLUORESCENCE BACKGROUND 316 9.8.2.1. BACKGROUND SUBTRACTION 316 9.8.2.2.
USE OF PICOSECOND PULSING AND GATING 316 9.8.2.3. NONLINEAR RAMAN
SPECTROSCOPY 317 9.8.3. CONCLUSIONS 317 REFERENCES 317 CHAPTER 10 RAMAN
SPECTROSCOPY IN CATALYSTS 325 MEHMED MEHICIC AND JEANETTE G. GRASSELLI
10.1. INTRODUCTION 325 10.1.1. ADVANTAGES OF RAMAN SPECTROSCOPY IN
CATALYTIC STUDIES 325 XVI CONTENTS 10.1.2. MISCELLANEOUS APPLICATIONS
333 10.2. ZEOLITES 334 10.3. HYDRODESULFURIZATION CATALYSTS 339 10.3.1.
MO0 3 -BASED CATALYSTS 342 10.3.1.1. BACKGROUND AND PREPARATION
VARIABLES 342 10.3.1.2. PROMOTER (COBALT-CONTAINING) STRUCTURES 345
10.3.1.3. PROMOTER (NICKEL-CONTAINING) STRUCTURES 347 10.3.1.4.
ACTIVATED (SULFIDED) MOLYBDENUM-CONTAINING CATALYSTS 349 10.3.1.5.
CONCLUSION 351 10.3.2. W0 3 -BASED CATALYSTS 352 10.4. OXIDATION
CATALYSIS 355 10.4.1. VANADIUM OXIDE CATALYSTS 355 10.4.2. MANGANESE
OXIDE CATALYSTS 358 10.4.3. BISMUTH MOLYBDATE CATALYSTS 359 10.4.4. IRON
OXIDE CATALYSTS 374 10.5. OTHER SYSTEMS 375 10.5.1. METATHESIS CATALYSIS
375 10.5.2. OLEFIN HYDROGENATION 377 10.5.3. SYNGAS PROCESSES 377
10.5.3.1. FISCHER-TROPSCH CATALYSIS 378 10.5.3.2. HYDROFORMYLATION
CATALYSIS 380 10.5.3.3. METHANATION 381 10.5.4. OLEFIN DEHYDROGENATION
381 REFERENCES 382 CHAPTER 11 RAMAN SPECTROSCOPY FOR BIOLOGICAL
APPLICATIONS 397 PHAM V. HUONG 11.1. INTRODUCTION 397 11.2. SPECIFIC
PROBLEMS IN BIOLOGICAL STUDIES 398 11.2.1. IDENTIFICATION OF
BIOMOLECULES 398 CONTENTS XV11 11.2.2. STRUCTURE IN AQUEOUS SOLUTIONS
398 11.2.3. DYNAMICS AND INTERACTIONS 398 11.3. INSTRUMENTATION AND
PROCEDURES 398 11.4. STRUCTURES 401 11.4.1. RAMAN SPECTRA OF LIVING
ORGANISMS/TISSUES/CELLS 401 11.4.1.1. EYE LENS 402 11.4.1.2. BIOLOGICAL
MEMBRANES 402 11.4.2. RAMAN SPECTRA OF ISOLATED BIOMOLECULES 402
11.4.2.1. STRUCTURES AND CONFORMATIONS OF T-RNA 402 11.5. 11.6. 11.7.
11.8. 11.4.2.1.1. STRUCTURES IN SOLUTIONS AND SOLIDS 11.4.2.1.2.
ENDO-MELTING (ORDERED TO DISORDERED STATE) 11.4.2.1.3. CONFORMATION
TRANSITIONS BETWEEN ORDERED STATES MOLECULAR DYNAMICS INTERACTIONS
11.6.1. SELECTIVE ENHANCEMENT OF RAMAN BANDS CORRESPONDING TO THE
INTERACTION SITE OF HEMOGLOBIN 11.6.2. CHANGES IN THE ACTIVE SITE OF
HEMOGLOBIN WITH INTERACTIONS 11.6.3. A-HELICAL AND RANDOM-COIL
STRUCTURES IN PROTEINS MECHANISMS 11.7.1. VISION 11.7.2. TRANSMISSION IN
NERVO US SYSTEMS 11.7.3. PROTONATION OF BIOMOLECULES 11.7.4. S*H/S*S
CONVERSION 11.7.5. CARCINOGENESIS CONCLUSIONS ACKNOWLEDGMENTS REFERENCES
402 406 407 408 409 409 410 410 412 412 413 414 415 417 421 421 421
XV111 CONTENTS CHAPTER 12 CHEMICAL APPLICATIONS OF GAS-PHASE RAMAN
SPECTROSCOPY 425 WILLIAM F. MURPHY 12.1. 12.2. 12.3. 12.4. INTRODUCTION
EXPERIMENTAL ASPECTS 12.2.1. INSTRUMENTATION 12.2.1.1. SOURCE 12.2.1.2.
SAMPLE IRRADIATION 12.2.1.3. SAMPLE CELLS 12.2.1.4. TRANSFER OPTICS
12.2.1.5. MONOCHROMATOR AND DETECTOR 12.2.2. INSTRUMENTAL CALIBRATION
12.2.2.1. FREQUENCY CALIBRATION 12.2.2.2. INTENSITY RESPONSE CALIBRATION
APPLICATIONS 12.3.1. THEORETICAL BACKGROUND 12.3.2. METHODOLOGY
12.3.2.1. MEASUREMENT OF SPECIES ABUNDANCE 12.3.2.2. MEASUREMENT OF
TEMPERATURE 12.3.3. SURVEY OF APPLICATIONS 12.3.3.1. COMBUSTION
DIAGNOSTICS 12.3.3.2. REMOTE SENSING 12.3.3.3. ANALYTICAL APPLICATIONS
CONCLUSIONS REFERENCES 425 426 426 426 427 427 428 429 430 430 432 434
434 437 437 438 440 440 442 443 446 447 INDEX 452 |
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| illustrated | Illustrated |
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| isbn | 0471519553 |
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| physical | XVIII, 462 S. graph. Darst. |
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| publisher | Wiley |
| record_format | marc |
| series | Chemical analysis |
| series2 | Chemical analysis A Wiley-Interscience publication |
| spelling | Analytical Raman spectroscopy ed. by Jeanette G. Grasselli ... New York u.a. Wiley 1991 XVIII, 462 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 114 A Wiley-Interscience publication Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Raman-Spektroskopie (DE-588)4176916-8 s DE-604 Grasselli, Jeanette G. Sonstige oth Chemical analysis 114 (DE-604)BV000008780 114 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=005943949&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Analytical Raman spectroscopy Chemical analysis Raman-Spektroskopie (DE-588)4176916-8 gnd |
| subject_GND | (DE-588)4176916-8 |
| title | Analytical Raman spectroscopy |
| title_auth | Analytical Raman spectroscopy |
| title_exact_search | Analytical Raman spectroscopy |
| title_full | Analytical Raman spectroscopy ed. by Jeanette G. Grasselli ... |
| title_fullStr | Analytical Raman spectroscopy ed. by Jeanette G. Grasselli ... |
| title_full_unstemmed | Analytical Raman spectroscopy ed. by Jeanette G. Grasselli ... |
| title_short | Analytical Raman spectroscopy |
| title_sort | analytical raman spectroscopy |
| topic | Raman-Spektroskopie (DE-588)4176916-8 gnd |
| topic_facet | Raman-Spektroskopie |
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