Solid supports and catalysts in organic synthesis:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York [u.a.]
Horwood [u.a.]
1992
|
| Ausgabe: | 1. publ. |
| Schriftenreihe: | Organic chemistry series
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 338 S. graph. Darst. |
| ISBN: | 0136399983 |
Internformat
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Datensatz im Suchindex
| _version_ | 1804120904274280448 |
|---|---|
| adam_text | SOLID SUPPORTS AND CATALYSTS IN ORGANIC SYNTHESIS EDITOR PROFESSOR K.
SMITH, M.SC,PHD. HEAD OF DEPARTMENT OF CHEMISTRY UNIVERSITY COLLEGE OF
SWANSEA WALES ELLIS HORWOOD PTR PRENTICE HALL NEW YORK LONDON TORONTO
SYDNEY TOKYO SINGAPORE CONTENTS LIST OF CONTRIBUTORS IX PREFACE XIII
PART I STRUCTURES AND NATURE OF SOLIDS USED AS SUPPORTS/CATALYSTS 1
INORGANIC SUPPORTS AND CATALYSTS * AN OVERVIEW P. DIDDAMS 1.1 GENERAL
CONSIDERATIONS 3 1.2 SILICA 5 1.3 ALUMINA 8 1.4 CARBON 14 1.5 CLAY
MINERALS 18 1.6 ZEOLITES 26 1.7 CONCLUSION 36 BIBLIOGRAPHY 37 REFERENCES
39 2 ORGANIC SUPPORTS * AN OVERVIEW J. M. MAUD 2.1 INTRODUCTION 40 2.2
THE PREPARATION OF ORGANIC POLYMERIC SUPPORTS 40 2.3 THE NATURE OF THE
POLYMERIC SUPPORT 50 2.4 CONCLUSIONS 58 REFERENCES 59 PART II
TRADITIONAL ORGANIC REACTIONS AIDED BY SOLID SUPPORTS OR CATALYSTS 3
REACTIONS ASSISTED BY AMORPHOUS INORGANIC SOLIDS * A SURVEY M. BUTTERS
3.1 INTRODUCTION 65 3.2 SELECTIVE METHODS FOR THE PREPARATION OF ESTERS
68 3.3 BASE CATALYSIS FOR THE ACTIVATION OF OH ACIDS 69 3.4 SILICA GEL
AS A MEDIUM FOR THE FORMATION AND SELECTIVE CLEAVAGE OF ACETALS AND
KETALS 74 3.5 REAGENTS AND CATALYSTS FOR ELECTROPHILIC SUBSTITUTION OF
AROMATIC AND HETEROCYCLIC COMPOUNDS 76 VI CONTENTS 3.6 ELECTROCYCLIC
REACTIONS 78 3.7 NUCLEOPHILIC SUBSTITUTIONS BY OXYGEN AND NITROGEN
NUCLEOPHILES 81 3.8 ELIMINATION REACTIONS OVER SOLID SUPPORTS 85 3.9
SELECTIVE REDUCTIONS OVER SOLIDS 88 3.10 OXIDATION OVER SOLIDS 91 3.11
ALLYLIC CHLORINATION OVER SILICA 96 REFERENCES 97 4 REACTIONS ASSISTED
BY CLAYS AND OTHER LAMELLAR SOLIDS * A SURVEY J. A. BALLANTINE 4.1
INTRODUCTION 100 4.2 ACIDITY OF CLAYS AND TYPES OF CLAY CATALYSTS 101
4.3 PREPARATION OF CLAY CATALYSTS 102 4.4 CLAY-CATALYSED ORGANIC
REACTIONS WHERE THE CATALYST IS ACTING ESSENTIALLY AS A SOLID ACID 103
4.5 CLAY-SUPPORTED INORGANIC REAGENTS 116 4.6 GRAPHITE INTERCALATION
COMPOUNDS 119 4.7 CONCLUSION 122 REFERENCES 122 5 ZEOLITE-ASSISTED
ORGANIC SYNTHESIS * A SURVEY M. BUTTERS 5.1 INTRODUCTION 130 5.2
CHEMICAL DEHYDRATION; FORMATION OF ALKENES, ENAMINES, ACETALS AND
CONDENSED HETEROCYCLES 132 5.3 PREPARATION OF ESTERS, ETHERS, AND AMIDES
ASSISTED BY REMOVAL OF SMALL REACTANTS FROM REACTION EQUILIBRIA USING
ZEOLITE MOLECULAR SIEVES 137 5.4 SEPARATION OF ISOMERS AND CLOSELY
RELATED COMPOUNDS FROM A MIXTURE 140 5.5 SELECTIVE PHOTOREARRANGEMENTS
WITHIN ZEOLITE CAVITIES 141 5.6 ELECTROCYCLIC REACTIONS 143 5.7 SHAPE
SELECTIVE ELECTROPHILIC AROMATIC SUBSTITUTION 147 5.8 CONTROL OF ALKENE
ADDITION REACTIONS 153 5.9 ISOMERIZATION AND OLIGOMERIZATION OF ALKENES
156 5.10 NUCLEOPHILIC SUBSTITUTIONS OF EPOXIDES AND ALKYL HALIDES 156
5.11 REDUCTION REACTIONS 159 5.12 OXIDATION REACTIONS 161 5.13
PHOTOCHLORINATION OF ALKANES 165 REFERENCES 165 6 REACTIONS INVOLVING
POLYMERIC RESINS * A SURVEY J. M. MAUD 6.1 INTRODUCTION 171 6.2
POLYMER-SUPPORTED ORGANIC SUBSTRATES 172 6.3 POLYMER-SUPPORTED REAGENTS
AND CATALYSTS 174 6.4 CONCLUSIONS 188 REFERENCES 188 CONTENTS VII PART
III SOLIDS IN BIOLOGICAL CHEMISTRY AND MOLECULAR BIOLOGY 7 SOLID PHASE
PEPTIDE SYNTHESIS J. S. DAVIES 7.1 INTRODUCTION 195 7.2 SYNTHETIC
STRATEGY FOR PEPTIDE SYNTHESIS 196 7.3 THE AUTOMATED SOLID PHASE
PROTOCOL 207 7.4 ALTERNATIVE APPROACHES TO SOLID PHASE SYNTHESIS *
SIMULTANEOUS (OR PARALLEL) MULTIPLE PEPTIDE SYNTHESIS (SMPS) 213 7.5
SELECTED EXAMPLES OF OLIGOPEPTIDE SYNTHESIS 216 REFERENCES 218 8 SOLID
PHASE OLIGONUCLEOTIDE SYNTHESIS H. A. WHITE 8.1 INTRODUCTION 225 8.2
APPLICATIONS OF OLIGONUCLEOTIDES 226 8.3 GENERAL STRATEGY FOR
OLIGONUCLEOTIDE SYNTHESIS 226 8.4 PHOSPHOTRIESTER SYNTHESIS 232 8.5
PHOSPHORAMIDITE SYNTHESIS 236 8.6 HYDROGEN PHOSPHONATE AND
PHOSPHOROTHIOITE SYNTHESES 238 8.7 THE SOLID PHASE 240 8.8
OLIGONUCLEOTIDE PURIFICATION 243 8.9 SYNTHESIS OF OLIGORIBONUCLEOTIDES
244 8.10 PROBLEMS IN OLIGONUCLEOTIDE SYNTHESIS 246 8.11 PREPARATION OF
OLIGONUCLEOTIDE MIXTURES 246 8.12 PREPARATION OF MODIFIED
OLIGONUCLEOTIDES AND VARIANT OLIGONUCLEOTIDES 247 8.13 FUTURE
DEVELOPMENTS 249 REFERENCES 249 9 IMMOBILIZED BIOCATALYSTS J. M. WOODLEY
9.1 INTRODUCTION 254 9.2 BIOLOGICAL CATALYSIS 255 9.3 BIOCATALYST
IMMOBILIZATION 257 9.4 TECHNIQUES FOR IMMOBILIZATION 258 9.5 IMPLICATION
OF INTRODUCING A SOLID SUPPORT 262 9.6 USES OF IMMOBILIZED BIOCATALYSTS
266 9.7 CONCLUDING REMARKS 268 REFERENCES 269 PART IV INDIVIDUAL
APPLICATIONS 10 HYDROGENATION AND HYDROGENATION CATALYSTS M. E. FAKLEY
AND F. KING 10.1 BACKGROUND 275 10.2 PRACTICAL CONSIDERATIONS 276 10.3
NEW HETEROGENEOUS HYDROGENATION CATALYSTS 277 10.4 FUNCTIONAL GROUP
REDUCTIONS 278 10.5 FUTURE TRENDS 284 VIII CONTENTS 10.6 APPENDICES 284
REFERENCES 286 11 DESIGNING MICRO-REACTORS * A PERSONAL ACCOUNT P.
LASZLO 11.1 INTRODUCTION 288 11.2 FROM PREBIOTIC CHEMISTRY TO
PRESENT-DAY FRONTIERS OF CHEMISTRY 289 11.3 THE RELEVANCE OF ROCKETRY
AND DRUNKENNESS TO THE DESIGN OF A NEW OXIDIZING REAGANT 292 11.4
CONCENTRATION EFFECTS BY CLAYS 293 11.5 CATALYSIS BY CLAYS 295 11.6 THE
CATALYTIC SITES 296 11.7 CONCLUSIONS. THE SIGNIFICANCE OF CLAYS IN A
WIDER CONTEXT 298 ACKNOWLEDGEMENTS 298 REFERENCES 301 12 MICROWAVE
ACTIVATION OF REACTIONS ON ORGANIC SOLID SUPPORTS G. BRAM, A. LOUPY AND
D. V ILLEMIN 12.1 MICROWAVES 302 12.2 APPLICATION OF COMMERCIAL
MICROWAVE OVENS TO ORGANIC SYNTHESIS IN SOLUTION 302 12.3 SOLID
MATERIALS UNDER MICROWAVES 309 12.4 MICROWAVE-ACTIVATED ORGANIC
SYNTHESIS ON SOLID SUPPORTS 312 REFERENCES 324 INDEX 327
|
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| genre | (DE-588)4143413-4 Aufsatzsammlung gnd-content |
| genre_facet | Aufsatzsammlung |
| id | DE-604.BV006626918 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T16:49:30Z |
| institution | BVB |
| isbn | 0136399983 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-004235526 |
| oclc_num | 25025057 |
| open_access_boolean | |
| owner | DE-12 DE-355 DE-BY-UBR DE-20 DE-19 DE-BY-UBM |
| owner_facet | DE-12 DE-355 DE-BY-UBR DE-20 DE-19 DE-BY-UBM |
| physical | XIV, 338 S. graph. Darst. |
| publishDate | 1992 |
| publishDateSearch | 1992 |
| publishDateSort | 1992 |
| publisher | Horwood [u.a.] |
| record_format | marc |
| series2 | Organic chemistry series |
| spelling | Solid supports and catalysts in organic synthesis ed. K. Smith 1. publ. New York [u.a.] Horwood [u.a.] 1992 XIV, 338 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Organic chemistry series Catalyst supports Catalysts Organic compounds Synthesis Katalyse (DE-588)4029921-1 gnd rswk-swf Katalysator (DE-588)4029919-3 gnd rswk-swf Trägersubstanz (DE-588)4131813-4 gnd rswk-swf Organische Synthese (DE-588)4075695-6 gnd rswk-swf Hilfsstoff (DE-588)4024893-8 gnd rswk-swf Trägerkatalysator (DE-588)4185817-7 gnd rswk-swf Festkörper (DE-588)4016918-2 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Organische Synthese (DE-588)4075695-6 s Festkörper (DE-588)4016918-2 s Hilfsstoff (DE-588)4024893-8 s DE-604 Katalysator (DE-588)4029919-3 s Trägerkatalysator (DE-588)4185817-7 s Trägersubstanz (DE-588)4131813-4 s Katalyse (DE-588)4029921-1 s Smith, Keith Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=004235526&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Solid supports and catalysts in organic synthesis Catalyst supports Catalysts Organic compounds Synthesis Katalyse (DE-588)4029921-1 gnd Katalysator (DE-588)4029919-3 gnd Trägersubstanz (DE-588)4131813-4 gnd Organische Synthese (DE-588)4075695-6 gnd Hilfsstoff (DE-588)4024893-8 gnd Trägerkatalysator (DE-588)4185817-7 gnd Festkörper (DE-588)4016918-2 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4029919-3 (DE-588)4131813-4 (DE-588)4075695-6 (DE-588)4024893-8 (DE-588)4185817-7 (DE-588)4016918-2 (DE-588)4143413-4 |
| title | Solid supports and catalysts in organic synthesis |
| title_auth | Solid supports and catalysts in organic synthesis |
| title_exact_search | Solid supports and catalysts in organic synthesis |
| title_full | Solid supports and catalysts in organic synthesis ed. K. Smith |
| title_fullStr | Solid supports and catalysts in organic synthesis ed. K. Smith |
| title_full_unstemmed | Solid supports and catalysts in organic synthesis ed. K. Smith |
| title_short | Solid supports and catalysts in organic synthesis |
| title_sort | solid supports and catalysts in organic synthesis |
| topic | Catalyst supports Catalysts Organic compounds Synthesis Katalyse (DE-588)4029921-1 gnd Katalysator (DE-588)4029919-3 gnd Trägersubstanz (DE-588)4131813-4 gnd Organische Synthese (DE-588)4075695-6 gnd Hilfsstoff (DE-588)4024893-8 gnd Trägerkatalysator (DE-588)4185817-7 gnd Festkörper (DE-588)4016918-2 gnd |
| topic_facet | Catalyst supports Catalysts Organic compounds Synthesis Katalyse Katalysator Trägersubstanz Organische Synthese Hilfsstoff Trägerkatalysator Festkörper Aufsatzsammlung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=004235526&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT smithkeith solidsupportsandcatalystsinorganicsynthesis |