An introduction to dynamic light scattering by macromolecules:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
Boston u. a.
Acad. Press
1990
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XX, 449 S. graph. Darst. |
| ISBN: | 0126272603 |
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| adam_text | AN INTRODUCTION TO NAMIC LIGHT SCATTERING BY MACROMOLE CULES KENNETH S.
SCHMITZ DEPARTMENT OF CHEMISTRY UNIVERSITY OF MISSOURI-KANSAS CITY
KANSAS CITY, MISSOURI ACADEMIC PRESS, INC. HARCOURT BRACE JOVANOVICH,
PUBLISHERS BOSTON SAN DIEGO NEW YORK LONDON SYDNEY TOKYO TORONTO TABLE
OF CONTENTS PREFACE XV ACKNOWLEDGEMENTS XIX ABOUT THE COVER XX CHAPTER
1. INTRODUCTION 1 1.0. BROWNIAN MOTION 1 1.1. BRIEF HISTORY OF DYNAMIC
LIGHT SCATTERING 2 1.2. TIME SCALES 3 1.3. ORGANIZATION OF THE TEXTBOOK
5 1.4. NOMENCLATURE 8 CHAPTER 2. BASIC CONCEPTS OF LIGHT SCATTERING 11
2.0. INTRODUCTION 11 PART I. INTERACTION OF LIGHT WITH MATTER 12 2.1.
THE NATURE OF LIGHT 12 2.2. THE ELECTRICAL NATURE OF MATTER 12 2.3. THE
SCATTERED ELECTRIC FIELD 13 2.4. FLUCTUATIONS IN THE POLARIZABILITY 15
PART II. TOTAL INTENSITY LIGHT SCATTERING 16 2.5. TOTAL (INTEGRATED)
INTENSITY OF SCATTERED LIGHT 16 2.6. LIGHT SCATTERING BY SMALL,
NONINTERACTING PARTICLES 20 2.7. LIGHT SCATTERING BY LARGE,
NONINTERACTING PARTICLES 21 2.8. LIGHT SCATTERING BY SMALL, INTERACTING
PARTICLES 25 2.9. LIGHT SCATTERING BY LARGE, INTERACTING PARTICLES:
ONE-CONTACT APPROXIMATION 26 VII VLLL TABLE OF CONTENTS 2.10. SOLUTION
STRUCTURE FACTOR 28 PART III. DYNAMIC LIGHT SCATTERING 31 2.11.
TIME-DEPENDENT TOTAL INTENSITY 31 2.12. ELECTRIC FIELD AND INTENSITY
CORRELATION FUNCTIONS 31 2.13. CENTER-OF-MASS DIFFUSION 32 2.14. EFFECT
OF RATIO C P /K 3 OND M 33 2.15. OSMOTIC SUSCEPTIBILITY CORRECTION 34
2.16. DYNAMIC LIGHT SCATTERING BY ABSORBING MOLECULES 35 2.17.
EVALUATION OF P (K,0)*AC P (K,0) 37 SUMMARY 38 PROBLEMS 38 ADDITIONAL
READING 42 CHAPTER 3. TRANSLATIONAL DIFFUSION*HYDRODYNAMIC DISSIPATION
43 3.0. INTRODUCTION 43 3.1. MACROSCOPIC DESCRIPTION OF MASS TRANSPORT
43 3.2. D M AND THE OSMOTIC SUSCEPTIBILITY 45 3.3. EFFECT OF EXTERNAL
FIELD*SEDIMENTATION 46 3.4. FRICTION FACTORS ASSOCIATED WITH D TR AND D
M 47 3.5. DETERMINATION OF THE MOLECULAR WEIGHT 49 3.6. DETERMINATION OF
THE EQUIVALENT HYDRODYNAMIC SHAPE OF REGULAER SOLIDS 50 3.7.
DETERMINATION OF THE EQUIVALENT HYDRODYNAMIC SHAPE OF IRREGULAER RIGID
STRUCTURES 52 3.8. ANISOTROPIE TRANSLATIONAL DIFFUSION OF CYLINDERS 55
3.9. DIFFUSION OF RANDOM-FLIGHT, LINEAR MOLECULES 57 3.10. DIFFUSION OF
LINEAR POLYMERS UNDER THETA CONDITIONS 58 3.11. EXCLUDED VOLUME*THE
FLORY LIMIT 61 3.12. EXCLUDED VOLUME EFFECT ON TRANSLATIONAL DIFFUSION
OF LINEAR MOLECULES 62 3.13. FLEXIBLE CIRCULAR MOLECULES 65 3.14.
FLEXIBLE BRANCHED MOLECULES AND STARS 66 3.15. CROSSOVER EXPONENTIAL,
PHASE SEPARATION, AND CHAIN DIMENSIONALITY 69 SUMMARY 72 PROBLEMS 72
ADDITIONAL READING 76 CHAPTER 4. MULTIPLE DECAY ANALYSIS OF THE
CORRELATION FUNCTION 77 4.0. INTRODUCTION 77 4.1. EFFECT OF
POLYDISPERSITY ON THE SCATTERING AMPLITUDES 77 4.2. SINGLE/DOUBLE
EXPONENTIAL ANALYSIS 79 4.3. CUMULANT ANALYSIS 79 TABLE OF CONTENTS IX
4.4. ASYMPTOTIC ANALYSIS METHOD 81 4.5. EXPANSION METHODS APPLIED TO
SIMULATED DATA 81 4.6. LAMBDA DEPRESSION ANALYSIS 85 4.7. Z-TRANSFORM
AND METHOD OF SPIKE RECOVERY 86 4.8. LINEAR PROGRAMMING METHOD 87 4.9.
INVERSE LAPLACE TRANSFORM METHODS*GENERAL COMMENTS 88 4.10. OVERLAY
HISTOGRAM METHOD WITH EXPONENTIAL SAMPLING 91 4.11. CONTIN AND DISCRETE
91 4.12. EFFECT OF NOISE ON THE ANALYSIS OF C(K, T) 92 4.13. MULTIPLE
SCATTERING*DIFFUSING WAVE SPECTROSCOPY 95 SUMMARY 96 PROBLEMS 97 -
ADDITIONAL READING 98 CHAPTER 5. DILUTE TO CONGESTED SOLUTIONS OF RODS
AND FLEXIBLE COILS 99 5.0. INTRODUCTION 99 5.1. THE AUTOCORRELATION
FUNCTION 99 5.2. THE CYLINDRICAL PARTICLE*GENERAL DEVELOPMENT 100 5.3.
CENTROSYMMETRIC PARTICLES*THE RIGID ROD FOR KL 1 102 5.4.
CENTROSYMMETRIC PARTICLES*THE RIGID ROD FOR KL » 1 105 5.5.
IRREGULAR-SHAPED PARTICLES WITH CYLINDRICAL SYMMETRY 107 5.6.
SEMI-FLEXIBLE LINEAR POLYMERS 109 5.7. THE CONTINUUM MODEL FOR LINEAR
POLYMERS 110 5.8. THE DISCRETE MODEL FOR LINEAR POLYMERS 114 5.9. THE
CORRELATION FUNCTION FOR FLEXIBLE COILS 116 5.10. ESTIMATION OF THE
ROUSE-ZIMM PARAMETERS 122 5.11. INTERNAL MODES FOR CIRCULAR DNA* THE
SODA MODEL 122 5.12. EFFECT OF HYDRODYNAMIC INTERACTION ON S(K, CO) 125
5.13. INTERMEDIATE K REGION 126 5.14. BROWNIAN DYNAMICS CALCULATIONS 128
5.15. SEMIDILUTE SOLUTION REGIME FOR FLEXIBLE POLYMERS: THE BLOB MODEL
129 5.16. LINEAR POLYMERS IN CONCENTRATED SOLUTIONS, GELS, AND MELTS:
THE REPTATION MODEL 131 5.17. THE CROSSOVER MODEL FOR CONGESTED POLYMER
SOLUTIONS 134 5.18. UNIVERSAL SCALING CURVES FOR THE CORRELATION LENGTHS
140 5.19. PROBE DIFFUSION IN A POLYMER MATRIX 142 5.20. STRETCHED
EXPONENTIAL REPRESENTATION OF POLYMER SOLUTIONS AND MELTS 145 5.21.
COMPUTER SIMULATION OF KOLINSKI, SKOLNICK, AND YARIS FOR CONGESTED
SOLUTION MOTION 147 5.22. POLYMER MELTS AND THE GLASS TRANSITION 147 X
TABLE OF CONTENTS 5.23. RIGID AND SEMIFLEXIBLE RODS IN CONGESTED
SOLUTIONS 148 5.24. COMPUTER SIMULATIONS OF CONGESTED SOLUTIONS OF RODS
150 SUMMARY 150 PROBLEMS 151 ADDITIONAL READING 155 CHAPTER 6.
HYDRODYNAMIC AND SHORT-RANGE INTERPARTICLE INTERACTIONS 157 6.0.
INTRODUCTION 157 6.1. THE GENERALIZED LANGEVIN EQUATION 157 6.2. THE
STOKES SOLVENT FLOW FIELD DUE TO AN ISOLATED SPHERE 158 6.3. THE STOKES
FRICTION FACTOR AND FAXEN S THEOREM 163 6.4. TRANSMISSION OF THE
INDIRECT INTERACTION 163 6.5. TIME-DEPENDENT DIFFUSION COEFFICIENTS 164
6.6. X-DEPENDENCE OF THE INITIAL DECAY RATE OF G^K, T) 167 6.7.
LOWEST-ORDER CORRECTION TO D M FOR IDENTICAL SPHERES: THE BATCHELOR AND
THE ANDERSON-REED MODELS 170 6.8. HIGHER-ORDER PAIRWISE INTERACTION
TERMS: THE METHOD OF REFLECTIONS 177 6.9. EFFECT OF DIVERGENT TERMS ON D
M 180 6.10. CONCENTRATED SOLUTIONS: THE METHOD OF INDUCED FORCES 181
6.11. EVALUATION OF SSELF 184 6.12. EVALUATION OF OE^ LF 187 6.13. D
SELF AND THE GLASS TRANSITION FOR HARD SPHERES 190 6.14. ARE
HYDRODYNAMIC INTERACTIONS SCREENED? 194 6.15. EVALUATION OF APP (AT, T)
195 6.16. TERTIARY SOLUTIONS OF HARD SPHERES 195 6.17. IS MACAVITY
THERE? 198 SUMMARY 200 PROBLEMS 201 CHAPTER 7. POLYELECTROLYTE SOLUTIONS
205 7.0. INTRODUCTION 205 7.1. THE POISSON-BOLTZMANN EQUATION AND THE
DEBYE-HUECKEL SCREENING LENGTH 205 7.2. STATISTICAL PROPERTIES OF
ELECTROLYTE SYSTEMS 207 7.3. SMALL ION-POLYION COUPLED MODES: GENERAL
FRAMEWORK 207 7.4. SMALL ION-POLYION COUPLED MODES: K = 0 LIMIT 210 7.5.
D APP (K)/D APP (K = 0)V.K FOR WEAKLY COUPLED POLYELECTROLYTES 212 7.6.
INCLUSION OF HYDRODYNAMIC INTERACTION: THE BELLONI-DRIFFORD MODEL FOR
POLYELECTROLYTE SOLUTIONS 215 7.7. DYNAMIC ATTENUATION 217 7.8.
ELECTROLYTE DISSIPATION 218 TABLE OF CONTENTS XI 7.9. POLYELECTROLYTE
DISSIPATION 224 7.10. COUNTERION CONDENSATION*THE MANNING THEORY 225
7.11. SMALL-ION DISTRIBUTION ABOUT CHARGED RODS, PLANES, AND SPHERES 229
7.12. THE ELECTROSTATIC CONTRIBUTION TO THE PERSISTENCE LENGTH OF
FLEXIBLE POLYELECTROLYTES 231 7.13. COMPOSITE DIFFUSION COEFFICIENT FOR
FLEXIBLE POLYIONS IN THE DEBYE-HUECKEL LIMIT 239 7.14. SEMIDILUTE REGIME
FOR POLYELECTROLYTES: SCALING LAWS 244 7.15. EFFECT OF SMALL IONS ON THE
SCATTERING POWER OF POLYELECTROLYTES 245 SUMMARY 249 PROBLEMS 250
CHAPTER8. COLLOIDS 261 8.0. INTRODUCTION 261 8.1. THE ELECTRIC DOUBLE
LAYER 264 8.2. THE STERN LAYER 264 8.3. THE GOUY REGION AND THE
DEBYE-HUECKEL REGION 265 8.4. GENERAL FEATURES OF THE PROBLEM OF THE
INTERACTION BETWEEN CHARGED SURFACES 267 8.5. THE DOUBLE LAYER ABOVE
SPHERICAL AND PLANAR SURFACES 267 8.6. CLASSICAL DLVO: REPULSIVE
INTERACTION BETWEEN SPHERES IN THE ASYMPTOTIC LIMITS OF A P /A DH 269
8.7. CLASSICAL DLVO: HAMAKER EXPRESSION FOR THE VAN DER WAALS- LONDON
ATTRACTIVE INTERACTION 272 8.8. PROPERTIES OF THE CLASSICAL DLVO
POTENTIAL 273 8.9. APPLICATIONS OF THE DLVO POTENTIAL TO REAL SYSTEMS
273 8.10. ANALYTICAL EXPRESSION FOR S(K AR) FOR THE HARD SPHERE
POTENTIAL IN THE PERCUS-YEVICK APPROXIMATION 279 8.11. BEYOND THE
CLASSICAL DLVO POTENTIAL 279 8.12. DIFFUSION IN STRUCTURED COLLOIDAL
SUSPENSIONS 285 8.13. FRACTAL OBJECTS 289 8.14. HOW LONG IS THE COAST
OF BRITAIN? 291 8.15. DIFFUSION VERSUS ACTIVATION CONTROL IN
BIMOLECULAR SOLUTION KINETICS 292 8.16. EQUILIBRIUM AND KINETICS
DISTRIBUTION OF CLUSTER SIZES FOR DIFFUSION-LIMITED AGGREGATION 293
8.17. TIME EVOLUTION OF THE NUMBER OF CLUSTERS FOR IRREVERSIBLE
AGGREGATION 297 8.18. STATIC SCATTERING PROPERTIES OF COLLOIDAL
AGGREGATES 299 8.19. DYNAMIC LIGHT SCATTERING BY COLLOIDAL AGGREGATES
302 8.20. ORIENTATION CONSTRAINTS ON DLA KINETICS 307 XLL TABLE OF
CONTENTS 8.21. COMPUTER SIMULATION OF COLLOIDAL AGGREGATION 309 SUMMARY
312 PROBLEMS 312 ADDITIONAL READING 317 CHAPTER 9. EXTERNAL
PERTURBATIONS 319 9.0. INTRODUCTION 319 9.1. GENERAL MATHEMATICAL
FRAMEWORK 319 9.2. THE ZETA POTENTIAL 321 9.3. ELECTROPHORETIC MOBILITY
AND THE ZETA POTENTIAL 321 9.4. THE EFFECT OF NONUNIFORM DISTRIBUTION
AND ELECTRIC FIELD STRENGTH-DEPENDENT ZETA POTENTIALS 327 9.5.
APPLICATION OF A CONSTANT ELECTRIC FIELD: DOPPLER SHIFT SPECTROSCOPY
(DSS) 335 9.6. APPLICATION OF A PERIODIC PULSED ELECTRIC FIELD*PPEF 344
9.7. APPLICATION OF A SINUSOIDAL ELECTRIC FIELD*QELS-SEF 348 9.8.
FREQUENCY AND FIELD STRENGTH DEPENDENT DP EF AND/I P 351 9.9. SINUSOIDAL
ENHANCEMENT OF CORRELATED STRUCTURES*SECS 353 9.10. A COMPARISON OF DSS,
PPEF, AND QELS-SEF TECHNIQUES 354 9.11. HYDRODYNAMIC FIELDS: CONSTANT
AND OSCILLATORY SOLVENT FLOW 357 9.12. MECHANICAL EXCITATION OF GELS 362
9.13. DIFFUSION UNDER HIGH-PRESSURE CONDITIONS 364 9.14. REACTION
KINETICS 366 SUMMARY 371 PROBLEMS 372 CHAPTER 10. DYNAMIC LIGHT
SCATTERING FROM COMPLEX MEDIA 377 10.0. INTRODUCTION 377 10.1. SPLITTING
OF RELAXATION MODES FOR DNA FRAGMENTS AS A FUNCTION OF IONIC STRENGTH
377 10.2. SPLITTING OF RELAXATION MODES OF HIGHLY POLYMERIZED DNA 380
10.3. ORDERING IN POLYELECTROLYTE SOLUTIONS 383 10.4. THE
ORDINARY-EXTRAORDINARY TRANSITION* JEU DU MOLECULES SOMNOLENTES 390
ADDITIONAL READING 396 APPENDIX A. MATHEMATICAL NOTATION 397 APPENDIX B.
STRUCTURE FACTORS FOR MULTICOMPONENT SYSTEMS 399 APPENDIX C. THE
ORNSTEIN-ZERNIKE RELATION AND THE PAIR DISTRIBUTION FUNCTION 405 TABLE
OF CONTENTS XLLL APPENDIX D. MSA AND RMSA SOLUTION TO THE
ORNSTEIN-ZERNIKE RELATIONSHIP 411 APPENDIX E. THE MEDINA-NOYOLA
FORMALISM FOR THE TRACER FRICTION FACTOR 417 GLOSSARY 423 BIBLIOGRAPHY
429 INDEX 445
|
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| indexdate | 2024-07-09T16:39:55Z |
| institution | BVB |
| isbn | 0126272603 |
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| spelling | Schmitz, Kenneth S. Verfasser aut An introduction to dynamic light scattering by macromolecules Kenneth S. Schmitz Boston u. a. Acad. Press 1990 XX, 449 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymerlösung (DE-588)4175242-9 gnd rswk-swf Dynamische Lichtstreuung (DE-588)4263784-3 gnd rswk-swf Kolloidchemie (DE-588)4134420-0 gnd rswk-swf Lichtstreuung (DE-588)4167602-6 gnd rswk-swf Polymerlösung (DE-588)4175242-9 s Lichtstreuung (DE-588)4167602-6 s DE-604 Kolloidchemie (DE-588)4134420-0 s Dynamische Lichtstreuung (DE-588)4263784-3 s GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003838016&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Schmitz, Kenneth S. An introduction to dynamic light scattering by macromolecules Polymerlösung (DE-588)4175242-9 gnd Dynamische Lichtstreuung (DE-588)4263784-3 gnd Kolloidchemie (DE-588)4134420-0 gnd Lichtstreuung (DE-588)4167602-6 gnd |
| subject_GND | (DE-588)4175242-9 (DE-588)4263784-3 (DE-588)4134420-0 (DE-588)4167602-6 |
| title | An introduction to dynamic light scattering by macromolecules |
| title_auth | An introduction to dynamic light scattering by macromolecules |
| title_exact_search | An introduction to dynamic light scattering by macromolecules |
| title_full | An introduction to dynamic light scattering by macromolecules Kenneth S. Schmitz |
| title_fullStr | An introduction to dynamic light scattering by macromolecules Kenneth S. Schmitz |
| title_full_unstemmed | An introduction to dynamic light scattering by macromolecules Kenneth S. Schmitz |
| title_short | An introduction to dynamic light scattering by macromolecules |
| title_sort | an introduction to dynamic light scattering by macromolecules |
| topic | Polymerlösung (DE-588)4175242-9 gnd Dynamische Lichtstreuung (DE-588)4263784-3 gnd Kolloidchemie (DE-588)4134420-0 gnd Lichtstreuung (DE-588)4167602-6 gnd |
| topic_facet | Polymerlösung Dynamische Lichtstreuung Kolloidchemie Lichtstreuung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003838016&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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