Comparisons of fused silica and other glass columns in gas chromatography:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Heidelberg [u.a.]
Hüthig
1981
|
| Schriftenreihe: | Chromatographic methods
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | VIII, 80 S. Ill., graph. Darst. |
| ISBN: | 377850729X |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804120218508722176 |
|---|---|
| adam_text | vii
Contents
1 Introduction 1
1 1 General 1
1 2 Column Types 1
2 Materials of Construction 5
2 1 General 5
2 2 Types of Glass 6
221 Soda-Lime Glasses 9
222 Borosi I icate Glasses 9
223 Lead Glasses 10
224 Fused Quartz and Fused Silica Glasses 11
2 3 Surface Structures 11
2 4 Drawing of Capillary Columns 14
3 Pretreatment of the Capillary 16
3 1 General 16
3 2 Lewis Acid Sites 17
321 Leaching Treatments 17
322 Comparison of Leached Glass and Fused
Silica in Terms of Lewis Acid Sites 19
3 3 Silanol Groups 20
331 Surface Active Agents 25
332 Salt Deposits 26
333 Film Deactivation 27
334 Polysiloxane Deactivation 28
335 Silylation Deactivation 29
336 Comparison of Deactivation Prospects
on Glass and Fused Silica 32
4 Evaluation of Column Inertness 33
4 1 General 33
4 2 Testing Uncoated Capillaries 34
4 3 Testing Coated Columns 36
431 Extra-Column Contributions 36
432 Effect of Test Conditions 38
433 Effect of Test Compounds 39
434 Test Solutions 40
435 RatioTesting 44
436 Conclusions 49
viii Contents
5 Physical Characteristics of the Column 50
5 1 General Considerations 50
5 2 Advantages Conferred by Column Flexi
bility 51
521 Straightening of Column Ends 51
522 Limitations of Instrumental Configur
ation 52
523 Optimizing the Detector Interface 53
524 Precise Column Alignment 56
525 Special Sampling Techniques 58
526 Other Advantages Conferred by Flexibil
ity 59
6 Cost Comparisons of Glass and Fused
Silica Columns 61
7 Application Examples 63
References 74
Subject Index 79
|
| any_adam_object | 1 |
| author | Jennings, Walter 1922-2012 |
| author_GND | (DE-588)109834186 |
| author_facet | Jennings, Walter 1922-2012 |
| author_role | aut |
| author_sort | Jennings, Walter 1922-2012 |
| author_variant | w j wj |
| building | Verbundindex |
| bvnumber | BV006012158 |
| classification_rvk | VG 7400 |
| ctrlnum | (OCoLC)439441378 (DE-599)BVBBV006012158 |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV006012158 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T16:38:36Z |
| institution | BVB |
| isbn | 377850729X |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-003780309 |
| oclc_num | 439441378 |
| open_access_boolean | |
| owner | DE-703 DE-29 DE-20 DE-83 DE-188 DE-11 |
| owner_facet | DE-703 DE-29 DE-20 DE-83 DE-188 DE-11 |
| physical | VIII, 80 S. Ill., graph. Darst. |
| publishDate | 1981 |
| publishDateSearch | 1981 |
| publishDateSort | 1981 |
| publisher | Hüthig |
| record_format | marc |
| series2 | Chromatographic methods |
| spelling | Jennings, Walter 1922-2012 Verfasser (DE-588)109834186 aut Comparisons of fused silica and other glass columns in gas chromatography by Walter G. Jennings Heidelberg [u.a.] Hüthig 1981 VIII, 80 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chromatographic methods Glaskapillargaschromatographie (DE-588)4157443-6 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Säule (DE-588)4178902-7 gnd rswk-swf Glaskapillarsäule (DE-588)4157444-8 gnd rswk-swf Glaskapillargaschromatographie (DE-588)4157443-6 s DE-604 Analytische Chemie (DE-588)4129906-1 s Gaschromatographie (DE-588)4019330-5 s Glaskapillarsäule (DE-588)4157444-8 s Säule (DE-588)4178902-7 s HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003780309&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Jennings, Walter 1922-2012 Comparisons of fused silica and other glass columns in gas chromatography Glaskapillargaschromatographie (DE-588)4157443-6 gnd Analytische Chemie (DE-588)4129906-1 gnd Gaschromatographie (DE-588)4019330-5 gnd Säule (DE-588)4178902-7 gnd Glaskapillarsäule (DE-588)4157444-8 gnd |
| subject_GND | (DE-588)4157443-6 (DE-588)4129906-1 (DE-588)4019330-5 (DE-588)4178902-7 (DE-588)4157444-8 |
| title | Comparisons of fused silica and other glass columns in gas chromatography |
| title_auth | Comparisons of fused silica and other glass columns in gas chromatography |
| title_exact_search | Comparisons of fused silica and other glass columns in gas chromatography |
| title_full | Comparisons of fused silica and other glass columns in gas chromatography by Walter G. Jennings |
| title_fullStr | Comparisons of fused silica and other glass columns in gas chromatography by Walter G. Jennings |
| title_full_unstemmed | Comparisons of fused silica and other glass columns in gas chromatography by Walter G. Jennings |
| title_short | Comparisons of fused silica and other glass columns in gas chromatography |
| title_sort | comparisons of fused silica and other glass columns in gas chromatography |
| topic | Glaskapillargaschromatographie (DE-588)4157443-6 gnd Analytische Chemie (DE-588)4129906-1 gnd Gaschromatographie (DE-588)4019330-5 gnd Säule (DE-588)4178902-7 gnd Glaskapillarsäule (DE-588)4157444-8 gnd |
| topic_facet | Glaskapillargaschromatographie Analytische Chemie Gaschromatographie Säule Glaskapillarsäule |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=003780309&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT jenningswalter comparisonsoffusedsilicaandotherglasscolumnsingaschromatography |