Analytical gas chromatography:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Orlando [u.a.]
Acad. Press
1987
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | Literaturangaben |
| Beschreibung: | X, 259 Seiten Diagramme |
| ISBN: | 0123843553 |
Internformat
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Datensatz im Suchindex
| _version_ | 1804118419787743232 |
|---|---|
| adam_text | ANALYTICAL GAS CHROMATOGRAPHY WALTER JENNINGS DEPARTMENT OF FOOD SCIENCE
AND TECHNOLOGY UNIVERSITY OF CALIFORNIA DAVIS, CALIFORNIA ACADEMIC
PRESS, INC. HARCOURT BRACE JOVANOVICH, PUBLISHERS SAN DIEGO NEW YORK
BOSTON LONDON SYDNEY TOKYO TORONTO CONTENTS PREFACE CHAPTER 1
INTRODUCTION 1.1 GENERAL CONSIDERATIONS 1 1.2 A SIMPLISTIC APPROACH 2
1.3 SIMPLISTIC COMPARISONS OF PACKED AND OPEN TUBULAER COLUMNS 4 1.4
ABBREVIATED THEORY OF THE CHROMATOGRAPHIE PROCESS 7 1.5 SEPARATION OF
COMPONENTS 15 1.6 EFFECT OF CARRIER GAS VELOCITY 18 REFERENCES 23
CHAPTER 2 OPA 2.1 2.2 2.3 2.4 2.5 2.6 2.7 N TUBULAER COLUMN GENERAL
CONSIDERATIONS THE TUBING SOURCES OF ACTIVITY STRUCTURAL FLAWS FLEXIBLE
COLUMNS OF CONVENTIONAL GLASSES SILANOL DEACTIVATION COLUMN COATING
REFERENCES 25 28 29 32 34 35 36 37 VI CONTENTS CHARTER 3 SAMPLE
INJECTION 3.1 GENERAL CONSIDERATIONS 40 3.2 EXTRACHROMATOGRAPHIC
PHENOMENA INFLUENCING BAND LENGTH * 41 3.3 CHROMATOGRAPHIE FACTORS
INFLUENCING BAND LENGTH 42 3.4 INJECTION INTO LARGE-DIAMETER OPEN
TUBULAER COLUMNS 44 3.5 SPLIT INJECTION 48 3.6 SPLITLESS INJECTION 50 3.7
PROGRAMMED TEMPERATURE VAPORIZING INJECTOR (PTV) 51 3.8 RETENTION GAP
FOCUSING 54 REFERENCES 57 CHAPTER 4 THE STATIONARY PHASE 4.1 GENERAL
CONSIDERATIONS 59 4.2 STATIONARY PHASE POLARITY AND SELECTIVITY 60 4.3
POLYSILOXANE STATIONARY PHASES: GENERAL COMMENTS 63 4.4 DIMETHYL
POLYSILOXANE STATIONARY PHASES 63 4.5 OTHER SILICONE STATIONARY PHASES
64 4.6 BONDED, CROSS-LINKED, AND/OR IMMOBILIZED STATIONARY PHASES 65 4.7
POLYETHYLENE GLYCOL STATIONARY PHASES 66 4.8 ENANTIOMER SEPARATIONS 68
4.9 OTHER SPECIAL-SELECTIVITY STATIONARY PHASES 70 4.10 GAS-SOLID
ADSORPTION COLUMNS 71 REFERENCES 71 CHAPTER 5 VARIABLES IN THE GAS
CHROMATOGRAPHIE PROCESS 5.1 GENERAL CONSIDERATIONS 74 5.2 REGULATION OF
THE GAS VELOCITY 75 5.3 THE VAN DEEMTER CURVE 75 5.4 OPTIMUM PRACTICAL
GAS VELOCITY 77 5.5 COMPUTER-GENERATED CURVES 78 5.6 EFFECT OF SOLUTE
PARTITION RATIOS ON OPTIMUM GAS VELOCITIES 79 5.7 EFFECT OF SOLUTE
PARTITION RATIOS ON SEPARATION POTENTIALS 85 5.8 EFFECT OF COLUMN LENGTH
88 5.9 EFFECT OF COLUMN DIAMETER 90 5.10 EFFECT OF STATIONARY PHASE FILM
THICKNESS 92 5.11 EFFECT OF STATIONARY PHASE DIFFUSIVITY 96 5.12 CHANGES
IN SOLUTE ELUTION ORDER 99 REFERENCES 100 CONTENTS VUE CHAPTER 6 COLUMN
SELECTION, INSTALLATION, AND USE 6.1 GENERAL CONSIDERATIONS 101 6.2
SELECTING THE STATIONARY PHASE 102 6.3 STATIONARY PHASE SELECTIVITY 104
6.4 SELECTING THE COLUMN LENGTH 105 6.5 SELECTING THE COLUMN DIAMETER
106 6.6 SELECTING THE STATIONARY PHASE FILM THICKNESS 107 6.7 COLUMN
INSTALLATION 107 6.8 COLUMN CONDITIONING 111 6.9 OPTIMIZING OPERATIONAL
PARAMETERS FOR SPECIFIC COLUMNS 111 6.10 COLUMNS FOR MASS SPECTROMETRY
151 REFERENCES 152 CHAPTER 7 INSTRUMENT CONVERSION AND ADAPTATION 7.1
GENERAL CONSIDERATIONS 153 7.2 OVEN CONSIDERATIONS 153 7.3 CARRIER GAS
CONSIDERATIONS 154 7.4 PACKED TO LARGE-DIAMETER OPEN TUBULAER CONVERSION
155 7.5 PACKED TO CAPILLARY CONVERSION 161 7.6 MAKEUP GAS CONSIDERATIONS
161 7.7 INLET DEACTIVATION 162 REFERENCES 163 CHAPTER 8 SPECIAL
ANALYTICAL TECHNIQUES 8.1 GENERAL CONSIDERATIONS 164 8.2 FLOW STREAM
SWITCHING 165 8.3 RECYCLE CHROMATOGRAPHY 168 8.4 MULTIDIMENSIONAL
CHROMATOGRAPHY 170 8.5 SPECIFICALLY DESIGNED STATIONARY PHASES 171 8.6
VAPOR SAMPLES AND HEADSPACE INJECTIONS 174 REFERENCES 176 CHAPTER 9
SELECTED APPLICATIONS 9.1 GENERAL CONSIDERATIONS 178 9.2 FOOD, FLAVOR,
AND FRAGRANCE APPLICATIONS 180 9.3 PETROLEUM- AND CHEMICAL-RELATED
APPLICATIONS 194 9.4 ENVIRONMENTAL APPLICATIONS 209 VLLL CONTENTS 9.5
BIOLOGICAL AND MEDICAL APPLICATIONS 219 REFERENCES 228 CHAPTER 10
TROUBLESHOOTING 10.1 10.2 10.3 10.4 10.5 10.6 10.7 10.8 10.9 GENERAL
CONSIDERATIONS USE OF TEST MIXTURES COLUMN BLEED TEMPERATURE AND OXYGEN
EFFECTS COLUMN REJUVENATION PEAK DISTORTION OTHER SORPTIVE RESIDUES
COLUMN COUPLING AND JUNCTION PROBLEMS FLAME JET PROBLEMS REFERENCES 231
232 235 238 239 241 243 243 246 247 APPENDIX ABBREVIATIONS, TERMS, AND
NOMENCLATURE 249 INDEX 253
|
| any_adam_object | 1 |
| author | Jennings, Walter 1922-2012 |
| author_GND | (DE-588)109834186 |
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| dewey-full | 543/.0896 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543/.0896 |
| dewey-search | 543/.0896 |
| dewey-sort | 3543 3896 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie Medizin |
| format | Book |
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| illustrated | Not Illustrated |
| indexdate | 2024-07-09T16:10:00Z |
| institution | BVB |
| isbn | 0123843553 |
| language | English |
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| physical | X, 259 Seiten Diagramme |
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| publishDate | 1987 |
| publishDateSearch | 1987 |
| publishDateSort | 1987 |
| publisher | Acad. Press |
| record_format | marc |
| spelling | Jennings, Walter 1922-2012 Verfasser (DE-588)109834186 aut Analytical gas chromatography Walter Jennings Orlando [u.a.] Acad. Press 1987 X, 259 Seiten Diagramme txt rdacontent n rdamedia nc rdacarrier Literaturangaben Capillarité ram Chromatographie en phase gazeuse ram Capillarity Chromatography, Gas methods Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Chromatographie (DE-588)4010153-8 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 s DE-604 Chromatographie (DE-588)4010153-8 s Analytische Chemie (DE-588)4129906-1 s GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=002627052&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Jennings, Walter 1922-2012 Analytical gas chromatography Capillarité ram Chromatographie en phase gazeuse ram Capillarity Chromatography, Gas methods Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Chromatographie (DE-588)4010153-8 gnd |
| subject_GND | (DE-588)4019330-5 (DE-588)4129906-1 (DE-588)4010153-8 |
| title | Analytical gas chromatography |
| title_auth | Analytical gas chromatography |
| title_exact_search | Analytical gas chromatography |
| title_full | Analytical gas chromatography Walter Jennings |
| title_fullStr | Analytical gas chromatography Walter Jennings |
| title_full_unstemmed | Analytical gas chromatography Walter Jennings |
| title_short | Analytical gas chromatography |
| title_sort | analytical gas chromatography |
| topic | Capillarité ram Chromatographie en phase gazeuse ram Capillarity Chromatography, Gas methods Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Chromatographie (DE-588)4010153-8 gnd |
| topic_facet | Capillarité Chromatographie en phase gazeuse Capillarity Chromatography, Gas methods Gas chromatography Gaschromatographie Analytische Chemie Chromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=002627052&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT jenningswalter analyticalgaschromatography |