Preconcentration of trace elements:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English Russian |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier
1990
|
| Schriftenreihe: | Wilson and Wilson's comprehensive analytical chemistry
25 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIX, 372 S. Ill., graph. Darst. |
| ISBN: | 0444873767 |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804117099391483904 |
|---|---|
| adam_text | Wilson and Wilson s
COMPREHENSIVE ANALYTICAL CHEMISTRY
Edited by
G SVEHLA, Ph D,D Sc ,FRSC,FICI
Professor of Analytical Chemistry
University College, Cork, Ireland
VOLUME XXV
PRECONCENTRATION
OF
TRACEELEMENTS
by
Yu A ZOLOTOV and N M KUZ MIN
ELSEVIER
AMSTERDAM-OXFORD-NEW YORK-TOKYO
Contents
Editor s Preface XV
Authors Preface XVII
Chapter 1 GENERAL CHARACTERISTICS OF PRE-
CONCENTRATION 1
1 1 Concentration and separation 1
1 2 Significance of preconcentration and fields of application 3
1 3 Quantitative characteristics of preconcentration 5
1 4 Selective and group preconcentration 7
1 5 Removal of matrix and separation of trace elements 9
References 10
Chapter 2 METHODS OF PRECONCENTRATION 11
2 1 Classification and general characteristics of methods 11
2 2 Solvent extraction 15
221 Characteristics of solvent extraction as a method
of preconcentration 15
222 Extraction of trace elements 19
2221 Chelates 19
2222 Neutral coordinatively solvated
compounds 26
2223 Ionic associates 31
223 Extraction of matrix 34
224 Extraction concentration techniques 37
225 Extraction chromatography 40
226 Automation 44
2 3 Sorption methods 45
231 General characteristics of methods 45
IX
232 Activated charcoals - 51
233 Synthetic ion exchangers 57
234 Complex-forming sorbents 62
2341 Complex-forming sorbents with
inoculated groups 62
2342 Polymeric heterochain sorbents 69
2343 Sorbents modified with complex-forming
reagents 73
235 Inorganic sorbents 74
236 Automating the sorption concentration process 75
2 4 Precipitation and co-precipitation methods 79
241 Precipitation 80
2411 Matrix precipitation 80
2412 Precipitation of trace elements 81
242 Co-precipitation of trace elements 81
2421 General 81
2422 Inorganic co-precipitants 85
2423 Organic co-precipitants 87
2 5 Electrochemical methods 94
251 Electrodeposition 94
252 Electrodeposition as part of str ipping
voltammetry 102
253 Other electrochemical methods 106
2531 Cementation 106
2532 Preconcentration using mercury as
chemical reagent 108
2533 Electrodissolution 109
2534 Electrodialysis Ill
2535 Electroosmosis 113
2536 Electrophoresis 114
2537 Electrodiffusion 115
2 6 Evaporation methods 116
261 Evaporation 116
262 Sublimation 121
263 Volatilization after chemical transformations 122
2631 Mineralization of organic and biological
samples 122
2632 Volatilization of inorgnnic compounds
with preliminary chemical transformation 128
2 7 Controlled crystallization 135
X
271 Directed crystallization 138
272 Zone melting 144
2 8 Pyrometallurgical methods 145
281 Fire assay 145
282 Other pyrometallurgical methods 153
2 9 Flotation 155
291 Flotation after co-precipitation 157
292 Ionic flotation 157
2 10 Filtration and other related membrane methods 160
2 11 Chemical transport reactions 165
2 12 Thermodiffusion 166
2 13 Combination of preconcentration methods 167
2 14 Comparison of preconcentration methods 172
References 179
Chapter 3 COMBINING PRECONCENTRATION WITH THE
DETERMINATION METHODS 205
3 1 Combined and hybrid methods 205
3 2 Atomic emission spectrometry 211
321 General remarks 211
322 Fractional volatilization 214
323 Other volatilization and related methods 216
324 Extraction 219
325 Sorption methods 220
326 Electrodeposition 221
3 2 7 Other concentration methods 222
3 3 Atomic absorption spectrometry 222
331 Extraction 223
332 Sorption 228
333 Volatilization and related methods 229
334 Other methods 231
3 4 Atomic fluorescence spectrometry 233
3 5 Spectrophotometry and fluorimetry 235
351 Extraction 236
352 Other methods 239
3 6 X-ray fluorescence spectrometry 240
361 Precipitation and co-precipitation 241
362 Sorption methods 242
363 Extraction 244
364 Other methods 245
XI
3 7 Spark-source mass spectrometry 246
3 8 Electron spin resonance 250
381 Determination of paramagnetic ions 250
382 Use of spin-labelled reagents 251
3 9 Activation analysis 254
391 General remarks 254
392 Preconcentration before irradiation 256
393 Preconcentration after irradiation
(radiochemical separation) 257
3931 Extraction methods 258
3932 Sorption methods 260
394 Automation 262
3 10 Electrochemical methods 262
3 10 1 Stripping voltammetry 263
3 10 2 Indirect polarographic analysis of extracts 264
3 10 3 Other electrochemical methods 267
3 11 Catalymetry 268
3 12 Chromatographic methods 270
3 12 1 Gas chromatography 270
3 12 2 High-performance liquid chromatography 273
3 13 Other methods 274
References 276
Chapter 4 PRECONCENTRATION IN ANALYSIS OF
VARIOUS SUBSTANCES 289
4 1 Environmental samples 289
411 Distinguishing features 289
412 Natural and waste waters 291
413 Air 300
414 Soils and bottom sediments 301
4 2 Mineral raw material 303
4 3 Metals, alloys and other inorganic substances and
materials, including high-purity substances 308
431 General 308
432 Volatilization methods 314
433 Solvent extraction 318
434 Other methods of preconcentration 328
4 4 Organic substances and biological samples 329
441 Distinguishing features 329
442 Dry ashing 332
XII
443 Wet ashing 334
444 Other methods of preconcentration 336
445 Combining preconcentration techniques 337
References 340
i
Subject Index 351
XIII
|
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| id | DE-604.BV002746084 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:49:01Z |
| institution | BVB |
| isbn | 0444873767 |
| language | English Russian |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001755828 |
| oclc_num | 421841828 |
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| owner | DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-83 DE-188 |
| owner_facet | DE-19 DE-BY-UBM DE-355 DE-BY-UBR DE-83 DE-188 |
| physical | XIX, 372 S. Ill., graph. Darst. |
| publishDate | 1990 |
| publishDateSearch | 1990 |
| publishDateSort | 1990 |
| publisher | Elsevier |
| record_format | marc |
| series | Wilson and Wilson's comprehensive analytical chemistry |
| series2 | Wilson and Wilson's comprehensive analytical chemistry |
| spelling | Zolotov, Jurij A. 1932- Verfasser (DE-588)11947929X aut Koncentrirovanie mikroelementov Preconcentration of trace elements by Yu. A. Zolotov and N. M. Kuz'min Amsterdam [u.a.] Elsevier 1990 XIX, 372 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Wilson and Wilson's comprehensive analytical chemistry 25 Aus dem Russ. übers. Oligo-éléments - Analyse Konzentration (DE-588)4125568-9 gnd rswk-swf Spurenanalyse (DE-588)4056593-2 gnd rswk-swf Spurenanalyse (DE-588)4056593-2 s Konzentration (DE-588)4125568-9 s DE-604 Kuz'min, Nikolaj M. Verfasser aut Wilson and Wilson's comprehensive analytical chemistry 25 (DE-604)BV000900805 25 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001755828&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Zolotov, Jurij A. 1932- Kuz'min, Nikolaj M. Preconcentration of trace elements Wilson and Wilson's comprehensive analytical chemistry Oligo-éléments - Analyse Konzentration (DE-588)4125568-9 gnd Spurenanalyse (DE-588)4056593-2 gnd |
| subject_GND | (DE-588)4125568-9 (DE-588)4056593-2 |
| title | Preconcentration of trace elements |
| title_alt | Koncentrirovanie mikroelementov |
| title_auth | Preconcentration of trace elements |
| title_exact_search | Preconcentration of trace elements |
| title_full | Preconcentration of trace elements by Yu. A. Zolotov and N. M. Kuz'min |
| title_fullStr | Preconcentration of trace elements by Yu. A. Zolotov and N. M. Kuz'min |
| title_full_unstemmed | Preconcentration of trace elements by Yu. A. Zolotov and N. M. Kuz'min |
| title_short | Preconcentration of trace elements |
| title_sort | preconcentration of trace elements |
| topic | Oligo-éléments - Analyse Konzentration (DE-588)4125568-9 gnd Spurenanalyse (DE-588)4056593-2 gnd |
| topic_facet | Oligo-éléments - Analyse Konzentration Spurenanalyse |
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