Laser microanalysis:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
New York u.a.
Wiley
1989
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| Schriftenreihe: | Chemical analysis
105 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 288 S. |
| ISBN: | 0471637076 |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804116910914142208 |
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| adam_text | LASER MICROANALYSIS LIESELOTTE MOENKE-BLANKENBURG
MARTIN-LUTHER-UNIVERSITY HALLE -WITTENBERG DEPARTMENT OF CHEMISTRY
HALLE, GERMAN DEMOCRATIC REPUBLIC WILEY A WILEY-INTERSCIENCE PUBLICATION
JOHN WILEY & SONS NEW YORK / CHICHESTER / BRISBANE / TORONTO / SINGAPORE
CONTENTS CHAPTER 1 INTRODUCTION 1 REFERENCES 3 CHAPTER 2 THE LASER AS A
RADIATION SOURCE 5 2.1. PRINCIPLE 5 2.2. SOLID-STATE RESONATORS 7 2.2.1.
RUBY 7 2.2.2. NEODYMIUM-DOPED GLASS AND GARNET 8 2.3. PROPERTIES OF
LASER RADIATION 9 2.3.1. COURSE OF THE DISCHARGE IN THE FLASHTUBE 10
2.3.2. DEGREE OF REFLECTION OF THE MIRROR COATING OF THE REFLECTOR 10
2.3.3. TEMPERATURE OF THE RESONATOR ROD 10 2.3.4. OSCILLATION AND
EMISSION BEHAVIOR OF THE LASER V 11 2.3.5. STABILITY OF THE COMPONENTS
OF THE RESONATOR 11 2.4. SS-SWITCHING TECHNIQUE 12 2.4.1. SS-SWITCHING
WITH THE AID OF ELECTRO-OPTICAL SWITCHES 12 2.4.2. SS-SWITCHING WITH THE
AID OF ROTATING REFLECTORS 13 2.4.3. SS-SWITCHING WITH SATURABLE
ABSORBERS 14 2.5. MODE OF ACTION OF AN ENERGY AND SPIKE-NUMBER MEASURING
ACCESSORY 15 REFERENCES 19 CHAPTER 3 LASER-TARGET INTERACTION:
MICROPLASMA GENERATION 21 3.1. FOCUSING OF LASER RADIATION 21 3.2.
TECHNICAL DATA OF NORMAL-MODE PULSE AND SS-SWITCHED SOLID- STATE LASERS
USED FOR LASER MICROANALYSIS 23 XIII XIV CONTENTS 3.3. VAPORIZATION OF
SOLIDS 24 3.3.1. VAPORIZATION BY NORMAL LASER PULSES 25 3.3.2.
VAPORIZATION BY GIANT PULSE OR SEMI-SS-SWITCHED LASER PULSE 29 3.3.3.
VAPOR PRESSURE AND TEMPERATURE 35 3.3.4. INFLUENCES OF SAMPLE PARAMETERS
ON VAPRIZATION 37 3.3.4.1. THERMAL PROPERTIES OF SOLIDS 37 3.3.4.2.
REFLECTIVITY 38 3.4. MICROPLASMA FEATURES FOR ANALYTICAL USE 39 S 3.4.1.
FOUNDATIONS 39 3.4.2. LOCAL THERMODYNAMIC EQUILIBRIUM 41 3.4.3. ENERGY
BALANCE; ENERGY LOSSES IN AND ABOVE THE TARGET 43 3.5. ADDITIONAL
EXCITATION AND LONIZATION OF LASER-BEAM-PRODUCED VAPOR BY SPARK
DISCHARGES AND OTHER SOURCES 48 3.6. VAPORIZATION AND EXCITATION UNDER
VARIABLE PRESSURE AND IN VARIOUS GAS MEDIA 57 3.7. MATRIX EFFECTS 64
REFERENCES 65 CHAPTER 4 PRESUMPTIONS FOR QUANTITATIVE LASER
MICROANALYSIS OF SOLIDS: STATISTICS IN ANALYTICAL CHEMISTRY 75 4.1.
ACCURACY AND PRECISION OF LASER MICROANALYSIS 76 4.2. HOMOGENEITY TESTS
OF REFERENCE MATERIALS 77 4.3. SUMMARY OF USEFUL STATISTICS FOR
SPECTROANALYTICAL CHEMISTRY 84 4.3.1. LINEAR REGRESSION 84 4.3.2. LINEAR
CORRELATION 86 4.3.3. ONE-WAY ANALYSIS OF VARIANCE 86 4.3.4. TWO-WAY
ANALYSIS OF VARIANCE 88 REFERENCES 90 CHAPTER 5 LASER MICROANALYSIS
BASED ON OPTICAL EMISSION SPECTROMETRY 93 5.1. INSTRUMENTS 93 5.1.1.
TECHNICAL DETAILS OF LASER MICROANALYZERS 93 5.1.2. CONSTRUCTION AND
MODE OF ACTION OF SPECTRAL APPARATUS AND RADIATION DETECTORS 104
CONTENTS XV 5.1.2.1. FUNDAMENTAL CONCEPTS 104 5.1.2.2. SPECTROGRAPHS
WITH PHOTOGRAPHIC RECORDING 105 5.1.2.3. PHOTOELECTRIC RECORDING 106
5.2. FIELD OF APPLICATION 120 5.2.1. MINERALOGY, GEOCHEMISTRY, AND
COSMOCHEMISTRY 120 5.2.2. METALLURGY AND RELATED FIELDS 140 5.2.3.
SILICATE TECHNIQUE, CRYSTAL SYNTHESIS, CHEMISTRY, FORENSIC SCIENCE,
ARCHAEOLOGY, RESTORATION OF ART OBJECTS, MEDICINE, AND BIOLOGY 141
REFERENCES 172 CHAPTER 6 LASER MICROVAPORIZATION COMBINED WTTH PLASMA
EXCITATION BASED ON OPTICAL EMISSION SPECTROMETRY 181 6.1. ICP
SPECTROMETRY OF SOLIDS 181 6.1.1. INSTRUMENTATION OF LM-ICP-OES 183
6.1.2. THEORETIC AND METHODIC INVESTIGATIONS 188 6.1.3. FIELDS OF
APPLICATION 191 6.2. MIP SPECTROMETRY OF SOLIDS 196 6.3. DCP
SPECTROMETRY OF SOLIDS 200 6.4. COMPARISON OF LM-ICP-OES, LM-MIP-OES,
AND LM-DCP- OES 204 REFERENCES 204 CHAPTER 7 LASER MICROANALYSIS BASED
ON ATOMIC ABSORPTION SPECTROMETRY 207 REFERENCES 213 CHAPTER 8 LASER
MICROANALYSIS BASED ON ATOMIC FLUORESCENCE SPECTROMETRY 215 REFERENCES
216 CHAPTER 9 LASER MICROANALYSIS BASED ON MASS SPECTROMETRY 219 9.1.
FOUNDATION AND HISTORICAL DEVELOPMENT 219 9.2. ANALYTICAL FEATURES 224
9.3. INSTRUMENTS 227 XVI CONTENTS 9.3.1. ION SOURCES 227 9.3.2.
ANALYZERS 231 9.4. FIELDS OF APPLICATION 236 9.4.1. CHEMICAL ANALYSIS OF
INORGANIC MATERIALS 236 9.4.2. CHEMICAL ANALYSIS OF ORGANIC MATERIALS
259 REFERENCES 259 CHAPTER 10 LASER MICRO ICP MASS SPECTROMETRY 271
REFERENCES 273 CHAPTER 11 COMPARISON WITH OTHER METHODS OF SOLID-STATE
ANALYSIS 275 REFERENCES 278 INDEX 281
|
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| author | Moenke-Blankenburg, Lieselotte 1934- |
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| bvnumber | BV002504845 |
| classification_rvk | VG 8850 |
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| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV002504845 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T15:46:01Z |
| institution | BVB |
| isbn | 0471637076 |
| language | Undetermined |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001613457 |
| oclc_num | 246315344 |
| open_access_boolean | |
| owner | DE-12 DE-355 DE-BY-UBR DE-83 |
| owner_facet | DE-12 DE-355 DE-BY-UBR DE-83 |
| physical | XVI, 288 S. |
| publishDate | 1989 |
| publishDateSearch | 1989 |
| publishDateSort | 1989 |
| publisher | Wiley |
| record_format | marc |
| series | Chemical analysis |
| series2 | Chemical analysis A Wiley-interscience publication |
| spelling | Moenke-Blankenburg, Lieselotte 1934- Verfasser (DE-588)128895004 aut Laser microanalysis New York u.a. Wiley 1989 XVI, 288 S. txt rdacontent n rdamedia nc rdacarrier Chemical analysis 105 A Wiley-interscience publication Laserspektroskopie (DE-588)4034620-1 gnd rswk-swf Mikroanalyse (DE-588)4169804-6 gnd rswk-swf Laserspektroskopie (DE-588)4034620-1 s Mikroanalyse (DE-588)4169804-6 s DE-604 Chemical analysis 105 (DE-604)BV000008780 105 GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001613457&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Moenke-Blankenburg, Lieselotte 1934- Laser microanalysis Chemical analysis Laserspektroskopie (DE-588)4034620-1 gnd Mikroanalyse (DE-588)4169804-6 gnd |
| subject_GND | (DE-588)4034620-1 (DE-588)4169804-6 |
| title | Laser microanalysis |
| title_auth | Laser microanalysis |
| title_exact_search | Laser microanalysis |
| title_full | Laser microanalysis |
| title_fullStr | Laser microanalysis |
| title_full_unstemmed | Laser microanalysis |
| title_short | Laser microanalysis |
| title_sort | laser microanalysis |
| topic | Laserspektroskopie (DE-588)4034620-1 gnd Mikroanalyse (DE-588)4169804-6 gnd |
| topic_facet | Laserspektroskopie Mikroanalyse |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001613457&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000008780 |
| work_keys_str_mv | AT moenkeblankenburglieselotte lasermicroanalysis |