Atom-Absorptions-Spektroskopie:
Gespeichert in:
Späterer Titel: | Welz, Bernhard Atomabsorptionsspektrometrie |
---|---|
1. Verfasser: | |
Format: | Buch |
Sprache: | German |
Veröffentlicht: |
Weinheim
Verl. Chemie
1975
|
Ausgabe: | 2., völlig neu bearb. Aufl. |
Schlagworte: | |
Online-Zugang: | Inhaltsverzeichnis |
Beschreibung: | Literaturverz. S. [251] - 278. - Ab der 3. Aufl. m.d.T.: Atomabsorptionsspektrometrie |
Beschreibung: | XII, 296 S. Ill., zahlr. graph. Darst. |
ISBN: | 3527256199 |
Internformat
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Datensatz im Suchindex
_version_ | 1804116740082237440 |
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adam_text | Titel: Atom-Absorptions-Spektroskopie
Autor: Welz, Bernhard
Jahr: 1975
Inhaltsverzeichnis
1. Einführung................................................1
1.1. Geschichte..............................................1
1.2. Atomspektren..........................3
1.3. Auswahl der Linien........................................6
1.4. Thermische Anregung......................................8
1.5. Absorptionskoeffizient......................................9
1.6. Linienbreite......................11
1.7. Messung der Absorption....................................12
1.8. Instrumentation.................... . 15
2. Lichtquellen........................19
2.1. Hohlkathodenlampen......................................19
2.2. Mehrelementlampen...................24
2.3. Zerlegbare Hohlkathodenlampen...............25
2.4. Hoch-Intensitäts-Lampen..................25
2.5. Dampf-Entladungslampen.................26
2.6. Elektrodenlose Entladungslampen...............26
2.7. Flammen als Lichtquellen..................28
2.8. Kontinuierliche Lichtquellen.................28
3. Atomisierung........................29
3.1. Atomisierung in Flammen..................29
3.1.1. Thermische Dissoziation.....................29
3.1.2. Die ideale Absorptionszelle....................32
3.1.3. Turbulenz-und Laminarbrenner.............32
3.1.4. Flammen.....................36
3.1.5. Brenner, Zerstäuber.................42
3.1.6. Probenboot-System.................45
3.2. Atomisierung ohne Flammen.................47
3.2.1. Atomisierung in geheizten Graphitrohröfen.........48
3.2.2. Vorteile der Graphitrohrküvetten.............56
3.2.3. Die verschiedenen Graphitrohrküvetten..........59
3.2.4. Störmöglichkeiten..................64
3.2.5. Sonstige flammenlose Atomisierungseinrichtungen.......69
3.2.6. Flammenlose Quecksilberbestimmung...........70
3.3. Wirksamkeit der Atomisierung................72
4. Optik..........................77
4.1. Spektrale Spaltbreite...................77
4.2. Reziproke Lineardispersion.................81
4.3. Prisma und Gitter....................83
4.4. Resonanz-Detektoren...................84
5. Elektronik und Anzeige....................87
5.1. Detektor.......................88
5.2. Emissionsrauschen....................89
5.3. Integration.......................91
5.4. Anzeige........................92
5.5. Automation......................96
6. Methodik.........................99
6.1. Reziproke Empfindlichkeit und Nachweisgrenze..........99
6.2. Interferenzen......................107
6.2.1. Chemische Interferenzen...........¡ ... . 108
6.2.2. Physikalische Interferenzen...............115
6.2.3. Organische Lösungsmittel...............117
6.2.4. Ionisations-Interferenz................119
6.2.5. Untergrund-Absorption................122
6.2.6. Spektrale Interferenzen................129
6.2.7. Analyse fester Proben............... • • 130
6.3. Analytische Verfahren...................131
6.3.1. Roütineverfahren..................132
6.3.2. Präzisions-Analyse..................133
6.3.3. Spurenanalyse...................134
6.3.4. Additionsmethode..................135
6.4. Lösungsmittel-Extraktion..................137
7. Verwandte Analysenmethoden..................139
7.1. Flammen-Emissions-Spektroskopie..............139
7.2. Atom-Fluoreszenz-Spektroskopie...............144
8. Die einzelnen Elemente....................149
8.1. Aluminium......................149
8.2. Antimon........................150
8.3. Arsen........................151
8.4. Barium........................152
8.5. Beryllium.......................153
8.6. Blei.........................154
8.7. Bor.........................155
8.8. Cadmium.......................155
8.9. Caesium.......................156
8.10. Calcium.......................156
8.11. Chrom........................158
8.12. Eisen........................159
8.13. Gallium.......................160
8.14. Germanium......................161
8.15. Gold........................161
Inhaltsverzeichnis XI
8.16. Hafnium.......................162
8.17. Indium........................163
8.18. Iridium........................163
8.19. Jod.........................165
8.20. Kalium........................165
8.21. Kobalt........................166
8.22. Kupfer........................167
8.23. Lanthan, Lanthaniden..................168
8.24. Lithium.......................171
8.25. Magnesium......................173
8.26. Mangan.......................175
8.27. Molybdän.......................176
8.28. Natrium.......................177
8.29. Nichtmetalle......................178
8.30. Nickel........................i80
8.31. Niob........................181
8.32. Osmium.......................i8l
8.33. Palladium.......................182
8.34. Phosphor.......................183
8.35. Platin........................184
8.36. Quecksilber......................l85
8.37. Rhenium.......................186
8.38. Rhodium...........................186
8.39. Rubidium.......................188
8.40. Ruthenium......................188
8.41. Scandium.......................188
8.42. Schwefel.......................189
8.43. Selen........................190
8.44. Silber........................191
8.45. Silicium.......................191
8.46. Strontium.......................192
8.47. Tantal.............................193
8.48. Technetium......................193
8.49. Tellur........................194
8.50. Thallium.......................194
8.51. Titan........................194
8.52. Uran........................195
8.53. Vanadin.......................
8.54. Wismut........................196
8.55. Wolfram.......................
8.56. Yttrium.......................Zl
S zta : : : : : : : : : : : : : : : : : : : : : ; : »8
8.59. Zirkonium......................
9. Spezielle Anwendungen....................203
9.1. Medizin, Biochemie, Toxikologie...............203
9.2. Lebensmittel-und Agrikulturchemie..............215
9.3. Wasser- und Luftuntersuchung................220
9.4. Geochemie.......................224
9.5. Metallurgie und Galvanik..................231
9.6. Petrochemie......................239
9.7. Glas, Keramik, Zement..................244
9.8. Kunststoffe, Textilien, Papier................245
9.9. Sonstige Industrieprodukte.................247
Literaturverzeichnis......................251
Sachregister.........................279
Anhang...........................291
Übersicht über einige kommerzielle
Atom-Absorptions-Spektrophotometer
|
any_adam_object | 1 |
author | Welz, Bernhard 1936-2018 |
author_GND | (DE-588)106263897 |
author_facet | Welz, Bernhard 1936-2018 |
author_role | aut |
author_sort | Welz, Bernhard 1936-2018 |
author_variant | b w bw |
building | Verbundindex |
bvnumber | BV002281270 |
callnumber-first | Q - Science |
callnumber-label | QD96 |
callnumber-raw | QD96.A8 |
callnumber-search | QD96.A8 |
callnumber-sort | QD 296 A8 |
callnumber-subject | QD - Chemistry |
classification_rvk | VG 8730 VG 8731 |
classification_tum | CHE 237f |
ctrlnum | (OCoLC)1960095 (DE-599)BVBBV002281270 |
dewey-full | 535.84 |
dewey-hundreds | 500 - Natural sciences and mathematics |
dewey-ones | 535 - Light and related radiation |
dewey-raw | 535.84 |
dewey-search | 535.84 |
dewey-sort | 3535.84 |
dewey-tens | 530 - Physics |
discipline | Chemie / Pharmazie Physik Chemie |
edition | 2., völlig neu bearb. Aufl. |
format | Book |
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id | DE-604.BV002281270 |
illustrated | Illustrated |
indexdate | 2024-07-09T15:43:18Z |
institution | BVB |
isbn | 3527256199 |
language | German |
oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001499120 |
oclc_num | 1960095 |
open_access_boolean | |
owner | DE-M49 DE-BY-TUM DE-703 DE-355 DE-BY-UBR DE-20 DE-29 DE-29T DE-Aug7 DE-19 DE-BY-UBM DE-706 DE-83 DE-11 DE-188 DE-210 |
owner_facet | DE-M49 DE-BY-TUM DE-703 DE-355 DE-BY-UBR DE-20 DE-29 DE-29T DE-Aug7 DE-19 DE-BY-UBM DE-706 DE-83 DE-11 DE-188 DE-210 |
physical | XII, 296 S. Ill., zahlr. graph. Darst. |
publishDate | 1975 |
publishDateSearch | 1975 |
publishDateSort | 1975 |
publisher | Verl. Chemie |
record_format | marc |
spelling | Welz, Bernhard 1936-2018 Verfasser (DE-588)106263897 aut Atom-Absorptions-Spektroskopie Bernhard Welz 2., völlig neu bearb. Aufl. Weinheim Verl. Chemie 1975 XII, 296 S. Ill., zahlr. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturverz. S. [251] - 278. - Ab der 3. Aufl. m.d.T.: Atomabsorptionsspektrometrie Atomic absorption spectroscopy Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd rswk-swf Chemisches Element (DE-588)4009874-6 gnd rswk-swf Atomspektroskopie (DE-588)4143333-6 gnd rswk-swf Absorption (DE-588)4000245-7 gnd rswk-swf Anorganische Chemie (DE-588)4002145-2 gnd rswk-swf Atomabsorptionsspektroskopie (DE-588)4068917-7 s DE-604 Chemisches Element (DE-588)4009874-6 s 1\p DE-604 Analytische Chemie (DE-588)4129906-1 s 2\p DE-604 Anorganische Chemie (DE-588)4002145-2 s 3\p DE-604 Atomspektroskopie (DE-588)4143333-6 s 4\p DE-604 Absorption (DE-588)4000245-7 s 5\p DE-604 3. Aufl. u.d.T. Welz, Bernhard Atomabsorptionsspektrometrie HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001499120&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 4\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 5\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
spellingShingle | Welz, Bernhard 1936-2018 Atom-Absorptions-Spektroskopie Atomic absorption spectroscopy Analytische Chemie (DE-588)4129906-1 gnd Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd Chemisches Element (DE-588)4009874-6 gnd Atomspektroskopie (DE-588)4143333-6 gnd Absorption (DE-588)4000245-7 gnd Anorganische Chemie (DE-588)4002145-2 gnd |
subject_GND | (DE-588)4129906-1 (DE-588)4068917-7 (DE-588)4009874-6 (DE-588)4143333-6 (DE-588)4000245-7 (DE-588)4002145-2 |
title | Atom-Absorptions-Spektroskopie |
title_auth | Atom-Absorptions-Spektroskopie |
title_exact_search | Atom-Absorptions-Spektroskopie |
title_full | Atom-Absorptions-Spektroskopie Bernhard Welz |
title_fullStr | Atom-Absorptions-Spektroskopie Bernhard Welz |
title_full_unstemmed | Atom-Absorptions-Spektroskopie Bernhard Welz |
title_new | Welz, Bernhard Atomabsorptionsspektrometrie |
title_short | Atom-Absorptions-Spektroskopie |
title_sort | atom absorptions spektroskopie |
topic | Atomic absorption spectroscopy Analytische Chemie (DE-588)4129906-1 gnd Atomabsorptionsspektroskopie (DE-588)4068917-7 gnd Chemisches Element (DE-588)4009874-6 gnd Atomspektroskopie (DE-588)4143333-6 gnd Absorption (DE-588)4000245-7 gnd Anorganische Chemie (DE-588)4002145-2 gnd |
topic_facet | Atomic absorption spectroscopy Analytische Chemie Atomabsorptionsspektroskopie Chemisches Element Atomspektroskopie Absorption Anorganische Chemie |
url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001499120&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
work_keys_str_mv | AT welzbernhard atomabsorptionsspektroskopie |