Open tubular columns in gas chromatography:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York
Plenum Pr.
1965
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIX, 164 S. |
Internformat
MARC
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Datensatz im Suchindex
| _version_ | 1804116739356622848 |
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| adam_text | OPEN TUBULAR
COLUMNS
IN GAS CHROMATOGRAPHY
L S Ettre
Chief Applications Chemist,
Analytical Division
The Perkin-Elmer Corporation, Norwalk, Connecticut
With a Foreword by
MJE Golay
$
PLENUMPRESS
NEWYORK
C out emits
First Part Introduction 1
1 1 Origins 1
1 2 Nomenclature 4
1 3 Terms and Definitions 5
1 31 Characterization of a Peak 6
1 32 The Partition Process 6
1 33 Peak Separation 7
1 34 Column Efficiency 8
1 35 Flow Rate and Gas Velocity 9
Second Part Theory and Practice 13
2 1 The Basic Golay Equation 13
2 2 Practical Conclusions from the Golay Equation 14
2 21 Column Efficiency 15
2 22 Carrier Gas Flow 20
2 23 Selection of Carrier Gas 24
2 24 Liquid-Film Thickness 25
2 3 Comparison with Packed Columns 26
2 31 Influence of the fl Values on Column Characteristics 27
2 32 Changes in the Necessary Column Efficiency 28
2 321 Number of Theoretical Plates Required at Various
a and k Values 28
2 322 Comparison of the Two Column Types 31
2 323 Examples 33
2 323 1 Analysis of p/m-Xy lenes33
2 323 2 Analysis of Fatty Acid Methyl Esters 35
2 33 Influence of Column Permeability 37
2 331 Specific Permeability 37
2 332 Correlation Between Specific Permeability and
PressureDropThroughtheColumn40
2 333 Comparison of Practical Columns 41
xvii
xviii Contents
2 34 The Performance Index 49
2 35 Modified Expressions Related to the Plate Number
Concept51
2 351 Number of Effective Plates 51
2 352 Height Equivalent to One Effective Plate 54
2 353 Modified Expression for the Number of Theoretical
Plates54
2 354 Resolution Factor 55
2 36 Practical Applications 55
2 4 The Influence of Temperature 63
2 5 Sample Capacity 65
2 6 Open Tubular Columns of Various Diameters 69
Third Part Preparation of Open Tubular Columns 75
3 1 Tubing 75
3 11 Plastic Tubing 75
3 12 Glass Tubing 76
3 13 Metal Tubing 77
3 2 Coating of the Column Tubing 79
3 21 Cleaning of the Column Tubing 79
3 22 Dynamic Coating Method 80
3 221 Volume of Coating Solution Larger Than the
VolumeofTubing81
3 222 Plug Method 83
3 23 Static Coating Method 85
3 24 Elimination of the Secondary Adsorption Effects of
ColumnTubing86
3 25 Column Conditioning and Storage 92
3 26 Recoating of Open Tubular Columns 92
3 3 Testing of Open Tubular Columns 93
3 31 The Use of the Polarity Mixture for Testing 94
3 32 Determination of the Air Peak Time 96
3 4 Increase of the Inside Surface Area ol the Column Tubing 97
3 41 Chemical Treatment of the Inside Wall of the Tubing 97
3 42 Deposition of a Porous Support Layer on the Inside
WalloftheTubing99
35 Adsorption-Type Open Tubular Columns 103
351PlatingMethods103
Contents xix
3 52 Adsorption Columns with Chemically Modified Inside
Wall 104
3 53 Open Tubular Columns Coated with an Adsorptive
Layer106
3 54 Modification of the Van Deemter-Golay Equation for
Open Tubular Adsorption Columns 109
Fourth Part The Gas Chromatographic System 111
4 1 Sample Introduction 112
4 11 Sample Introduction Systems 112
4 12 Split Systems 114
4 121 Dynamic Splitting 115
4 122 Static Splitting 116
4 2 The Pneumatic System 117
H421CarrierGasRegulation117
4 22 Connecting Tubes 119
4 3 Column Heating 120
4 31 Isothermal Operation 120
4 32 Programmed-Temperature Operation 120
4 33 Applications of Temperature-Programmed Open Tubu
larColumns122
4 34 Compensation of Liquid-Phase Bleeding During Temp
erature Programming 130
4 4 Detection and Recording 131
4 41 Commonly Used Detectors 133
4 42 Auxiliary Detectors 135
4 43 Recording Systems 136
Fifth Part Bibliography 137
Sixth Part Supplements 157
6 1 Calculation of the Air Peak Time 157
6 11 The Method of Peterson and Hirsch 157
6 12 The Method of Gold 160
6 2 Instrumentation 162
|
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| author | Ettre, Leslie S. 1922-2010 |
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| discipline | Chemie / Pharmazie Chemie |
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| illustrated | Not Illustrated |
| indexdate | 2024-07-09T15:43:18Z |
| institution | BVB |
| language | English |
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| physical | XIX, 164 S. |
| publishDate | 1965 |
| publishDateSearch | 1965 |
| publishDateSort | 1965 |
| publisher | Plenum Pr. |
| record_format | marc |
| spelling | Ettre, Leslie S. 1922-2010 Verfasser (DE-588)137321341 aut Open tubular columns in gas chromatography New York Plenum Pr. 1965 XIX, 164 S. txt rdacontent n rdamedia nc rdacarrier Chromatographie - Analyse Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Gaschromatographie (DE-588)4019330-5 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001498660&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Ettre, Leslie S. 1922-2010 Open tubular columns in gas chromatography Chromatographie - Analyse Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4019330-5 |
| title | Open tubular columns in gas chromatography |
| title_auth | Open tubular columns in gas chromatography |
| title_exact_search | Open tubular columns in gas chromatography |
| title_full | Open tubular columns in gas chromatography |
| title_fullStr | Open tubular columns in gas chromatography |
| title_full_unstemmed | Open tubular columns in gas chromatography |
| title_short | Open tubular columns in gas chromatography |
| title_sort | open tubular columns in gas chromatography |
| topic | Chromatographie - Analyse Chromatographie en phase gazeuse Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chromatographie - Analyse Chromatographie en phase gazeuse Gas chromatography Gaschromatographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001498660&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT ettreleslies opentubularcolumnsingaschromatography |