New methods of analytical chemistry:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
London
Chapman & Hall
1964
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XV, 366 Seiten |
Internformat
MARC
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| 100 | 1 | |a Belcher, Ronald |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a New methods of analytical chemistry |c Ronald Belcher and Cecil L. Wilson |
| 250 | |a 2. ed. | ||
| 264 | 1 | |a London |b Chapman & Hall |c 1964 | |
| 300 | |a XV, 366 Seiten | ||
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| 650 | 7 | |a Chimie Analytique |2 biup | |
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Datensatz im Suchindex
| _version_ | 1804116737334968320 |
|---|---|
| adam_text | New Methods of
Analytical Chemistry
Ronald Belcher
Ph D,D Sc ,FRIC,F Inst F
Professor of Analytical Chemistry
University of Birmingham
and
Cecil L Wilson
Ph D,D Sc ,FRIC,FICr
Professor of Inorganic and Analytical Chemistry
The Queen s University of Belfast
in association with
T S West
Ph D,D Sc ,FRIC
Reader in Analytical Chemistry
Imperial College, University of London
t
CHAPMAN AND HALL LTD
11 NEW FETTER LANE, LONDON E C 4
Contents
Page
Preface to the Second Edition v
Extracts from Preface to First Edition vii
I TITRIMETRIC STANDARDS 1
A CONVENTIONAL ACID-BASE STANDARDS 1
1 Sodium carbonate 1
2 Hydrochloric acid 2
3 Sulphuric acid 2
4 Borax 4
5 Potassium hydrogen phthalate 4
6 Sulphamic acid 5
7 Potassium hydrogen iodate 5
B RECENTLY RECOMMENDED AC ID-BASE
STANDARDS 6
1 4-Aminopyridine 6
2 Cadmium hydrogen ethylenediamine-Ar-hydroxy-
ethyl-iVjA^N -triacetate 7
3 Calcium hydrogen malate hexahydrate 10
4 Di-(/w-nitrobenzenesulphonyl)amine 11
5 Potassium hydrogen bis-(3,5-dinitrobenzoate) 12
6 Sodium hydrogen diglycolate 13
7 2,4,6-Trinitrobenzoic acid 14
8 Tris-(hydroxymethyl)aminomethane 14
C OXIDATION-REDUCTION STANDARDS 16
1 Barium thiosulphate monohydrate 16
2 Cerate solutions 18
3 Copper-II oxide 19
4 Ferrous salts 19
II INDICATORS 20
A ACID-BASE INDICATORS 21
(i) CHEMILUMINESCENT INDICATORS 21
1 Lucigenin 21
2 Lophine 22
ix
X CONTENTS
Page
(ii) MIXED INDICATORS 23
1 Mixed one-colour indicators 23
2 A mixed-screened indicator 24
3 Mixed chemiluminescent indicators 25
(iii) MISCELLANEOUS ACID-BASE INDICAIORS 25
1 Basic ferric sulphate 25
2 Nitron hydrochloride 26
3 Nitrophenylhydrazone derivatives 27
B REDOX INDICATORS 27
(i) DETERMINATION OF INDICATOR REDOX POTENTIAL 28
(ii) PHENANTHROLINES AND BIPYRIDYLS 29
1 Tris-l,10-phenanthroline osmium-II perchlor-
ate 32
2 Sulphonated phenanthrolines 33
(iii) DIPHENYLAMINE DERIVATIVES 34
1 Variamine Blue B 35
2 3,3 -Dimethoxybenzidine-jV,A!-di-o-benzoic
acid 36
(iv) MISCELLANEOUS REDOX INDICATORS 36
1 Bromothymol blue 36
2 Copper phthalocyanine tetrasulphonic acid 37
3 Rhodamine 6G 39
4 Sulphosalicylic acid-vanadium-V 40
5 Triphenylmethane dyes 41
6 Triphenylmethylarsonium chloride 42
C METALLOCHROMIC INDICATORS 44
(i) CALCIUM AND MAGNESIUM INDICATORS 44
1 Glyoxal bis-(2-hydroxyanil) 44
2 Acid Alizarin Black SN 45
3 Methyl thymol blue 46
4 Glycine thymol blue 47
5 Calcichrome 48
6 Calmagite 49
7 Beryllon II 49
8 Xylidyl blue II (Magon) 50
9 Thymolphthalexone 51
10 Scarlet 3B 52
CONTENTS XI
Page
(ii) COPPER SELECTIVE INDICATORS - 52
1 Fast Sulphon Black F 52
2 Ponceau 3R 53
(iii) GENERAL PURPOSE INDICATORS 54
1 Naphthol violet and glycine nuphthol violet 54
2 Alizarin complexan 56
3 Naphthyl azoxine 57
4 Indicators related to PAN 58
5 Arsenazo 59
6 /V-Benzoyl-yV-phenylhydroxyla mine 59
(iv) METALLOFLUORESCENT INDICATORS 60
1 Calcein 60
2 Calcein Blue 62
3 o-Dianisidine-JV, N, N , W-tetra-acetic acid 63
4 Benzidine-3,3 -dicarboxylic aetd-N,N,N ,N -
tetra-acetic acid 63
5 3,3 -Dihydroxybenzidine-iV,A ,A-tetra-
acetic acid 64
6 Acetylhydrazone of salicylaldehyde 64
7 8-Hydroxyquinoline 65
8 3-Hydroxy-2-naphthoic acid 65
(v) SCREENED METALLOFLUORESCENT INDICATORS 66
(vi) CHEMILUMINESCENT COMPLEXOMETRIC INDICATORS 67
(vii) EXTRACTIVE END-POINTS 69
D MISCELLANEOUS INDICATORS 71
(i) MERCURIMETRIC INDICATORS 71
1 Diphenylcarbazone and 2-nitroso-l-naphthol 71
2 Phloroglucinol 72
(ii) HALIDE TITRATIONS 72
Potassium rhodizonate 72
(iii) CYANIDE TITRATIONS 73
Resacetophenone oxime 73
III TITRANTS 74
1 Chlorite 74
2 Chloramine-T 77
xji CONTENTS
Page
3 Ferricyanide 83
4 Vanadate 90
5 Hydrazine 93
6 Ascorbic acid 96
7 o-Hydroxymercuribenzoic acid 98
8 Oxine Blue 100
9 Bis(2-hydroxyethyl)dithiocarbamate 101
10 Miscellaneous 103
(i) Hydroquinone 103
(ii) Bromine monochloride 104
(iii) Lead tetra-acetate 105
(iv) JV-Bromosuccinimide 105
(v) Bismuthon 106
(vi) Thioglycolic acid 106
(vii) Miscellaneous 106
IV ORGANIC REAGENTS 108
1 Acetoacetanilide 108
2 4-Alkyl-1,2-cyclohexanedionedioximes 109
3 Benzenephosphinic acid 111
4 Benzo-l,2,3-triazole 113
5 jV-Benzoyl-TV-phenylhydroxylamine 115
6 A^iV-Dialkylethanolammonium orotatos 129
7 Ethylenediaminetetra-acetic acid congeners 131
8 3-Hydroxy-l-/)-chlorophenyl-3-triazinc 156
9 3 Hydroxy-l,3-diphenyltriazine 157
10 2-(o-Hydroxyphenyl)-benzimidazole 159
11 2-(o-Hydroxyphenyl)-benzoxazole 161
12 Mandelic acid 165
13 l-Phenyltetrazoline-5-thione 169
14 Sodium-A -(/V-bromo-C-tetradecyl-bet;!iny])-( -
tetradecyl-betaine 170
15 Tetraphenylboron and its analogues 174
16 Tetraphenylphosphonium chloride 184
17 2-Thiophene-/ra«j-aldoxime 187
18 0-(/?-Toluylsulphonamido)aniline 189
V INORGANIC REAGENTS 191
1 Argentic oxide 191
2 Fluoboric acid 193
CONTENTS xiii
Page
3 Periodic acid 195
4 Tris-(ethylenediamine)-cobalt-III chloride 199
VI SELECTIVE SPECTROPHOTOMETRIC METHODS 203
1 Alizarin fluorine blue for fluoride 203
2 4-Amino-4 -chlorodiphenyl for sulphate 206
3 Arsenazo for hafnium 207
4 Bis-(cyclohexanone)-oxalyldihydrazone for copper 208
5 Calcichrome for calcium 210
6 l,3-Dimethyl-4-imino-5-isonitroso-uracil for copper 211
7 Fast Sulphon Black F for beryllium 212
8 Fast Sulphon Black F for copper 214
9 Glyoxal bis-(2-hydroxyanil) for calcium 214
10 5-(4-Nitrophenylazo)-salicylic acid for magnesium 215
11 Proline thymol blue for copper 217
12 Pyrogallol red for silver 218
13 Pyrogallol red for chloride 220
14 Spectrophotometric reagents for boron 222
15 Selective spectrophotometric methods involving
extraction 225
VII PRECIPITATION FROM HOMOGENEOUS SOLU
TION 228
A CHANGE OF pH 229
1 Determination of bismuth in the presence of lead 229
2 Precipitation of magnesium in the presence of
sodium and potassium 229
3 Precipitation of niobium 230
B DIRECT GENERATION OF PRECIPITATING
AGENT 231
1 Phosphate 231
2 Ammonia 231
3 8-Hydroxyquinoline 233
4 Dimethylglyoxime 234
5 Cupferron 236
6 l-Nitroso-2-naphthol 237
7 Salicylaldoxime 238
8 Quercetin 239
xiv CONTENTS
Page
C PRECIPITATION BY REMOVAL OF SOLVENT 241
1 Determination of aluminium 241
D BREAKDOWN OF COMPLEXES 241
1 Breakdown of peroxy compounds 241
2 Oxidation of bismuth-EDTA complex 242
3 Replacement of one ion by another in an EDTA
complex 243
4 Breakdown of argentous ammines 244
VIII SOLVENT EXTRACTION 247
A GENERAL CONSIDERATIONS 247
(i) ION-ASSOCIATION COMPLEXES 247
(ii) CHELATE SYSTEMS 254
B SPECIFIC APPLICATIONS 256
(i) 8-HYDROXYQUINOLINE AND ITS DERIVATIVES 256
1 8-Hydroxyquinoline 256
2 5,7-Dihalogen substituted derivatives 257
3 2-Methyl-8-hydroxyquinoline 258
4 8-Mercaptoquinoline 260
5 Other derivatives 261
(ii) SUBSTITUTED DITHIZONES 263
(iii) BASIC DYESTUFFS 264
1 Methyl violet 265
2 Brilliant Green 265
3 Other basic dyestuffs 266
(iv) MONOXIMES AND DIOXIMES 267
(v) 1,10-PHENANTHROLINE AND ITS DERIVATIVES 270
1 1,10-Phenanthroline 270
2 4,7-Diphenyl-l,10-phenanthroline 271
(vi) ACETYLACETONE 272
(vii) DISPLACEMENT REAGENTS 274
(viii) MISCELLANEOUS REAGENTS 275
IX MISCELLANEOUS METHODS 279
1 Titrimetric determination of ammonium 279
2 Titrimetric determination of arsenic 282
CONTENTS XV
Page
3 Titrimetric determination of barium sulphate 284
4 Titrimetric determination of beryllium 285
5 Gravimetric determination of bismuth 287
6 Titrimetric determination of boron 288
7 Gravimetric determination of cadmium 289
8 Titrimetric determination of calcium 291
9 Gravimetric determination of copper 292
10 Titrimetric determination of copper and iron in one
solution 294
11 Gravimetric determination of fluoride 295
12 Titrimetric determination of hydrazine and methyl-
hydrazine in admixture 296
13 Titrimetric determination of iron 299
(a) Reduction by hypophosphite 299
(b) Reduction by stannous chloride 300
(c) With permanganate 301
14 Gravimetric determination of lithium 302
(a) as trilithium phosphate 302
{b) as lithium potassium ferricyanide-hexamethyl-
enetetramine 307
15 Titrimetric determination of lithium 309
16 Titrimetric determination of manganese 311
17 Titrimetric determination of mercury 312
(a) alkalimetrically 312
(b) with cyanide 314
(c) with thiocyanate 315
18 Titrimetric determination of molybdenum 316
19 Gravimetric determination of nickel 318
20 Titrimetric determination of oxalic acitl 318
21 Titrimetric determination of perchloratc 320
22 Determination of phosphate as quinoline molybdo-
phosphate 322
23- Gravimetric determination of scandium 330
24 Determination of silica as quinoline molybdosilicate 331
25 Titrimetric determination of sulphate 338
26 Titrimetric determination of titanium, aluminium and
iron occurring together 341
27 Titrimetric determination of thiosulphate and nitrite 344
28 Gravimetric determination of tungsten 346
|
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| discipline | Chemie / Pharmazie Chemie |
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| spelling | Belcher, Ronald Verfasser aut New methods of analytical chemistry Ronald Belcher and Cecil L. Wilson 2. ed. London Chapman & Hall 1964 XV, 366 Seiten txt rdacontent n rdamedia nc rdacarrier Chimie Analytique biup Chimie analytique Chemistry, Analytic Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 s DE-604 Chemische Analyse (DE-588)4009840-0 s 1\p DE-604 Wilson, Cecil L. Verfasser aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001497421&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Belcher, Ronald Wilson, Cecil L. New methods of analytical chemistry Chimie Analytique biup Chimie analytique Chemistry, Analytic Chemische Analyse (DE-588)4009840-0 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4009840-0 (DE-588)4129906-1 |
| title | New methods of analytical chemistry |
| title_auth | New methods of analytical chemistry |
| title_exact_search | New methods of analytical chemistry |
| title_full | New methods of analytical chemistry Ronald Belcher and Cecil L. Wilson |
| title_fullStr | New methods of analytical chemistry Ronald Belcher and Cecil L. Wilson |
| title_full_unstemmed | New methods of analytical chemistry Ronald Belcher and Cecil L. Wilson |
| title_short | New methods of analytical chemistry |
| title_sort | new methods of analytical chemistry |
| topic | Chimie Analytique biup Chimie analytique Chemistry, Analytic Chemische Analyse (DE-588)4009840-0 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Chimie Analytique Chimie analytique Chemistry, Analytic Chemische Analyse Analytische Chemie |
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