Chemistry of the metal-gas interface:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Oxford
Clarendon Press
1978
|
| Schriftenreihe: | Monographs on the physics and chemistry of materials
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIV, 594 Seiten Illustrationen, Diagramme |
| ISBN: | 0198513399 |
Internformat
MARC
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| 100 | 1 | |a Roberts, Meirion W. |d 1931-2014 |e Verfasser |0 (DE-588)141673532 |4 aut | |
| 245 | 1 | 0 | |a Chemistry of the metal-gas interface |c M. W. Roberts ; C. S. MacKee |
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Datensatz im Suchindex
| _version_ | 1813607918671495168 |
|---|---|
| adam_text |
CHEMISTRY OF
THE METAL - GAS
INTERFACE
BY
M W ROBERTS
AND
C S McKEE
i o j
mz§
CLARENDON PRESS • OXFORD
CONTENTS
1 SOME BASIC CONCEPTS
1 1 Introduction - 1
1 2 Electrons in solids 6
1 3 Adsorption 17
1 4 Surface characterization 20
1 5 Surface reactivity patterns and bonding 25
1 6 Thermochemistry of surface processes 33
161 Isothermal calorimeters 37
162 Adiabatic calorimeters 37
1 7 Kinetic studies 39
171 Absolute rate theory 41
2 CRYSTALLOGRAPHY OF METALS
2 1 Introduction 49
2 2 The basic point lattices 50
2 3 Metal crystals 52
2 4 Miller indices 56
2 5 Projections of crystals 61
2 6 Orientation of single crystals 65
2 7 Reciprocal space 67
2 8 Single-crystal metal surfaces 73
281 Surface models 73
282 The density and co-ordination of surface atoms 80
283 The stability of crystal surfaces 84
2 9 Crystal defects 88
2 10 Diffusion in solids and on solid surfaces 92
3 THE DETERMINATION OF SURFACE
STRUCTURE 93
3 1 Introduction 93
3 2 LEED: basic experimental observations 100
3 3 LEED: basic pattern interpretation 104
331 General physics of diffraction 104
332 Spot positions 105
333 Clean-surface patterns 113
334 Overlayer patterns 115
3 4 LEED: kinematic diffraction theory 121
341 Reciprocal-space intensity profiles 122
342 Spot intensity profiles—qualitative considerations 130
3 5 Spot intensity profiles: quantitative considerations 135
351 Kinematic theory 135
352 Modified kinematic theory 139
353 Data-reduction techniques 144
354 Dynamical theories 146
CONTENTS
3 6 Coincidence lattices 150
361 Scattering by a coincidence lattice 152
362 Multiple scattering 154
363 Parameter modulation 157
3 7 Diffraction by imperfect structures 158
371 Background intensity, diffuse spots, and ring pat
terns 160
372 Split spots and streaks 161
373 Patterns from faceted surfaces 165
4 ELECTRON SPECTROSCOPY
4 1 Introduction 158
411 Photoemission and the solid state 170
412 Quantum mechanical description and Koopmans'
theorem 173
4 2 Photoelectron spectroscopy 175
421 Applications in surface chemistry 181
422 Surface sensitivity and escape depth of photoelec-
trons 183
4 3 Auger electron spectroscopy (AES) 185
431 Introduction 185
432 Nomenclature in AES 188
433 Energies of Auger electrons 189
434 Quantitative analysis 192
435 Experimental techniques used in AES 194
436 Loss features in Auger spectroscopy 195
437 Applications of Auger spectroscopy 197
4 4 Appearance-potential spectroscopy (APS) 201
4 5 Ion-Neutralization spectroscopy (INS) 203
4 6 Summarizing comments 205
5 INFRARED, RAMAN AND PARTICLE
IMPACT SPECTROSCOPIES 212
5 1 Introduction 212
5 2 Infrared and Raman spectroscopy 213
521 Transmission infrared 213
522 Reflection infrared 215
523 Theoretical background to reflection method 217
524 Infrared emission spectroscopy 217
525 Raman spectroscopy 219
5 3 Electron-impact excitation of the vibrations of adsorbed
species 222
5 4 Electron-stimulated desorption (ESD) or electron-
impact desorption (EID) 224
541 Experimental methods in ESD studies 226
542 Cross-sections of ion desorption 226
543 Threshold values 227
5 5 Ion scattering and secondary-ion mass spectroscopy 228
CONTENTS XI
6 EXPERIMENTAL ASPECTS OF
SURFACE KINETICS 234
6 1 Introduction 234
6 2 Gas-solid collisions 235
621 Molecular-beam scattering 235
622 Thermal accommodation coefficient measurements 235
6 3 Surface diffusion 237
631 Field electron emission 238
632 Field ion emission 242
6 4 Kinetics of adsorption 249
641 The rate of impingement of gas molecules on a
surface 250
642 The rate of adsorption 256
643 Rate of desorption in relation to sticking
probability 263
6 5 Kinetics of desorption 264
7 PHYSICAL ADSORPTION 280
7 1 Introduction 280
7 2 Forces in physical adsorption 281
7 3 Work-function studies 288
731 Adsorption of inert gases on single-crystal
planes 289
7 4 Structural aspects of the adsorbed layer 295
7 5 Analysis of physical-adsorption isotherm data 299
7 6 Conclusions 302
8 MODELS FOR THE ADSORPTION AND
DESORPTION PROCESSES 305
8 1 Generalized model for the interaction of a gas-phase
particle with a solid 305
8 2 The initial gas-surface collision 307
821 Linear harmonic oscillator chain model 309
822 The hard- and soft-cube models 311
823 The square-well model 314
824 Conclusions regarding the initial gas-surface colli
sion 315
8 3 Surface diffusion 316
831 Type 1 diffusion 316
832 Type 2 diffusion 320
833 Type 3 diffusion 321
8 4 Kinetic models for chemisorption 323
8 5 The effect of adsorbate-adsorbate interactions 337
8 6 Conclusion 343
9 CARBON MONOXIDE 346
9 1 Introduction 346
911 Molecular-orbital description of carbon monoxide 346
xii - CONTENTS
9 2 Kinetic and adsorption studies 347
921 Polycrystalline tungsten + CO 347
'922 CO adsorption on W (110) 350
923 Molybdenum and other transition raetals 351
9 3 Work-function studies on single-crystal planes of tung
sten 355
9 4 Isotopic studies 357
9*5 Electron-impact desorption 358
9 6 LEED studies 359
961W (211) surface 359
962 Pt (111), (100), and stepped Pt surfaces 359
963 Ni (100) and (111) surfaces 360
964 Cu (100) surface 362
9 7 Field emission and field ion microscopy (FEM and FIM) 363
9 8 Infrared spectroscopy 364
981 CO adsorption on Cu 366
982 CO adsorption on W and Pt 367
9 9 Electron-spectroscopic studies of CO adsorbed on Mo
and W 369
991 XPS studies of CO adsorption 369
992 UPS studies of CO adsorption 371
9 10 XPS and UPS studies of the Fe + CO system 373
9 11 Mechanism of CO bonding 373
9 12 Conclusions 377
10 HYDROGEN AND NITROGEN 382
10 1 Introduction 382
10 2 Hydrogen interaction with metals 382
10 2 1 General aspects 382
10 2 2 Hydrogen adsorption on tungsten and
- molybdenum 384
10 2 3 Hydrogen adsorption on nickel, palladium, and
platinum
10 3 Kinetic and related studies of nitrogen interaction with
metals 405
10 3 1 General aspects 405
10 3 2 Nitrogen adsorption on tungsten -high-energy
binding states 407
10 3 3 Nitrogen adsorption on tungsten--states of in
termediate binding energy 425
10 3 4 Nitrogen adsorption on tungsten- -states of low
| binding energy 427
10 3 5 Nitrogen adsorption on rhenium 428
10 3 6 Nitrogen adsorption on nickel, palladium, and
platinum 429
10 4 Electron spectroscopic studies of nitrogen and related
molecules 432
10 5 Conclusions 434
CONTENTS XIII
11 THE INTERACTION OF OXYGEN WITH
METAL SURFACES 439
11 1 Introduction 439
11 2 Oxygen chemisorption and incorporation 440
11 2 1 Kinetics of oxygen chemisorption and incorpo
ration 441
11 3 Oxide-film growth or oxidation 453
11 4 Rash desorption and the nature of surface oxygen 459
11 5 Electron spectroscopy 461
11 5 1 Interaction of oxygen with metals 461
11 5 2 Interaction of water vapour with metals 469
11 6 Low-energy electron diffraction 471
11 7 Conclusions 478
12 METAL ADSORPTION ON METALS 483
12 1 Introduction 483
12 2 Surface diffusion and nucleation 484
12 2 1 Single-atom mobilities 484
12 2 2 Clustering 490
12 2 3 The effects of impurities and lattice defects 492
12 2 4 Faceting 495
12 3 Transition-metal adsorption on tungsten 498
12 4 Alkali and alkaline-earth adsorption on transition
metals 503
12 4 1 Surface structures 503
12 4 2 Binding energies 509
12 4 3 Work-function changes and dipole moments 512
12 5 Quantum-mechanical treatment of chemisorption 518
12 5 1 General principles 518
12 5 2 The Anderson model 529
12 5 3 Surface molecules 530
12 5 4 Indirect adatom-adatom interactions 531
12 5 5 Alternative approaches to chemisorption theory 532
13 THE IMPACT OF NEW EXPERIMENTAL
DEVELOPMENTS ON HETEROGENEOUS
CATALYSIS S36
13 1 Introduction 536
13 2 Catalytic behaviour of tuntsten carbide 536
13 3 Nature of'a supported molybdenum hexacarl onyl olefin
disproportionation catalyst 539
13 4 Unsuspected surface reactions 539
13 5 Role of minor elements 541
13 6 Crystal orientation in metal surfaces 542
13 7 Atomic composition of alloy surfaces 543
13 8 Surface reactions of adsorbed hydrocarbons 545
xivCONTENTS
13 9 Small-molecule reactions at stepped surfaces 546
13 10 Theoretical studies 548
APPENDIX Wave theory 553
AUTHOR INDEX 559
SUBJECT INDEX 570 |
| any_adam_object | 1 |
| author | Roberts, Meirion W. 1931-2014 McKee, C. S. |
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| discipline | Chemie / Pharmazie Physik Chemie |
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| id | DE-604.BV002258600 |
| illustrated | Illustrated |
| indexdate | 2024-10-22T10:01:31Z |
| institution | BVB |
| isbn | 0198513399 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001484258 |
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| spelling | Roberts, Meirion W. 1931-2014 Verfasser (DE-588)141673532 aut Chemistry of the metal-gas interface M. W. Roberts ; C. S. MacKee Oxford Clarendon Press 1978 XIV, 594 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Monographs on the physics and chemistry of materials Gases in metals Metals Surfaces Surface chemistry Gas (DE-588)4019320-2 gnd rswk-swf Adsorption (DE-588)4000536-7 gnd rswk-swf Oberflächenanalyse (DE-588)4172243-7 gnd rswk-swf Metalloberfläche (DE-588)4169612-8 gnd rswk-swf Metalloberfläche (DE-588)4169612-8 s Adsorption (DE-588)4000536-7 s Gas (DE-588)4019320-2 s DE-604 Oberflächenanalyse (DE-588)4172243-7 s McKee, C. S. Verfasser (DE-588)1031497374 aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001484258&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Roberts, Meirion W. 1931-2014 McKee, C. S. Chemistry of the metal-gas interface Gases in metals Metals Surfaces Surface chemistry Gas (DE-588)4019320-2 gnd Adsorption (DE-588)4000536-7 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Metalloberfläche (DE-588)4169612-8 gnd |
| subject_GND | (DE-588)4019320-2 (DE-588)4000536-7 (DE-588)4172243-7 (DE-588)4169612-8 |
| title | Chemistry of the metal-gas interface |
| title_auth | Chemistry of the metal-gas interface |
| title_exact_search | Chemistry of the metal-gas interface |
| title_full | Chemistry of the metal-gas interface M. W. Roberts ; C. S. MacKee |
| title_fullStr | Chemistry of the metal-gas interface M. W. Roberts ; C. S. MacKee |
| title_full_unstemmed | Chemistry of the metal-gas interface M. W. Roberts ; C. S. MacKee |
| title_short | Chemistry of the metal-gas interface |
| title_sort | chemistry of the metal gas interface |
| topic | Gases in metals Metals Surfaces Surface chemistry Gas (DE-588)4019320-2 gnd Adsorption (DE-588)4000536-7 gnd Oberflächenanalyse (DE-588)4172243-7 gnd Metalloberfläche (DE-588)4169612-8 gnd |
| topic_facet | Gases in metals Metals Surfaces Surface chemistry Gas Adsorption Oberflächenanalyse Metalloberfläche |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001484258&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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