Chemical methods of rock analysis:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Oxford (u.a.)
Pergamon Pr.
1981
|
| Ausgabe: | 3. ed. |
| Schriftenreihe: | Pergamon series in analytical chemistry.
4. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 379 S. graph. Darst. |
| ISBN: | 0080238068 |
Internformat
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| 245 | 1 | 0 | |a Chemical methods of rock analysis |c P. G. Jeffery and D. Hutchison |
| 250 | |a 3. ed. | ||
| 264 | 1 | |a Oxford (u.a.) |b Pergamon Pr. |c 1981 | |
| 300 | |a XVI, 379 S. |b graph. Darst. | ||
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Datensatz im Suchindex
| _version_ | 1804116602149404672 |
|---|---|
| adam_text | Contents
Chapter 1, The Composition of Rook Material page 1
Geochemical reference material 3
Elements determined 9
Reporting an analysis 12
The selection of material for analysis 13
Crushing and grinding [k
Contamination 16
Chapter 2. Sample Decomposition
Decomposition with mineral acids 18
Decomposition with hydrochloric acid 18
Decomposition with nitric acid 18
Decomposition with hydrofluoric acid 19
Fusion procedures 21
Fusion with alkali fluoride 21
Fusion with potassium pyrosulphate 21
Fusion with sodium carbonate 22
Fusion with alkali hydroxide 24
Sinter or fusion with sodium peroxide 25
Fusion with boric oxide and alkali borates 26
Chapter 3- Classical Scheme for the Analysis of Silicate Rocks 29
Decomposition of the sample JO
Determination of silica 32
Separation and collection of silica 32
Ignition and volatilisation of silica J k
Determination of mixed oxides 35
Precipitation of the mixed oxides 35
Recovery of the aluminium traces 37
viii Contents
Ignition of the mixed oxides 37
Recovery of silica traces 38
Determination of aluminium by difference 33
Determination of calcium 39
Determination of magnesium 40
Determination of manganese in the magnesium residue 42
Chapter 4. The Rapid Analysis of Silicate Rocks 43
Individual schemes of rapid rock analysis 48
Schemes of Shapiro and Brannock 48
Scheme of Riley 48
Scheme of Langmyhr and Graff 48
Scheme of Ingamells 49
Scheme of Shapiro 49
Scheme of Belt 50
Scheme of Bernas 50
Scheme of Langmyhr and Paus 51
Schemes of Abbey 51
Chapter 5- The Alkali Metals 59
(Lithium, Sodium, Potassium, Rubidium, Caesium)
Determination of sodium and potassium in silicate
rocks by flame spectrophotometry 61
Determination of potassium in micas 64
Determination of lithium 64
Determination of rubidium and caesium 65
Chapter 6. Aluminium 70
Gravimetric determination with 8-hydroxyquinoline 73
Titrimetric determination with CyDTA 75
Photometric determination with 8-hydroxyquinoline 77
Photometric determination with pyrocatechol violet 78
Chapter 7. Antimony 81
Spectrophotometric determination of antimony in
silicate rocks 82
Determination of antimony by atomic absorption
spectroscopy 84
Contents ix
Chapter 8. Arsenic 86
Spectrophotometric determination of arsenic 8b
A molybdenum blue method using acid digestion 88
A molybdenum blue method using a fusion 90
An arsine-molybdenum blue method 91
Method using silver diethyldithiocarbamate 93
Determination of arsenic by atomic absorption
spectroscopy 9^+
Chapter 9- Barium 96
Gravimetric determination of barium in silicate rocks 9
Determination of barium by atomic absorption
spectroscopy 99
Chapter 10. Beryllium 102
Spectrophotometric determination of beryllium with
beryllon II 102
Determination of beryllium by atomic absorption
spectroscopy 105
Chapter 11. Bismuth 107
Chapter 12. Boron 109
Spectrophotometric determination of boron in silicate
rocks 109
Titrijnetric determination of boron in tourmaline 112
Chapter 13. Cadmium 115
Chapter 1*t. Calcium 117
Gravimetric determination of calcium 117
Titrimetric determination of calcium with EDTA 118
Determination of calcium in carbonate rooks (low
in magnesium) 120
Contents
Photometric determination of calcium 121
Determination of calcium by flame photometry 121
Determination of calcium by atomic absorption
spectroscopy 122
Chapter 15. Carbon
Determination of carbon dioxide 12*+
Method of Shapiro and Brannock 125
Method using Schrotter s apparatus 12°
Gravimetric method using absorption tubes and
acid decomposition 127
Gravimetric method using absorption tubes and
thermal decomposition 150
Titrimetric determination of carbon dioxide 133
Determination of carbon dioxide by gas chromatography 133
Determination of carbon ( non-carbonate carbon ) 13^
Combustion tube methods 13^
Determination of organic matter ?
Chapter 16. Chlorine, Bromine and Iodine
Chapter 17. Chromium
138
Determination of water-soluble chlorine 13°
Determination of acid-soluble chlorine 13
Determination of total chlorine 139
Spectrophotometric determination of chlorine I*3
Determination of bromine 1
Determination of iodine 1^3
Determination of chromium with EDTA 1
Determination of chromium as alkali chromate 1^°
Determination of chromium using sym-diphenylcarbazide 151
Determination of chromium by atomic absorption
spectroscopy 153
Chapter 18. Cobalt 155
Spectrophotometric determination of cobalt using
nitroso-H-salt 15b
Determination of cobalt by atomic absorption
spectroscopy 159
Chapter 19. Copper 1bO
Spectrophotometric determination of copper with
2,2 -diquinolyl 161
Determination by atomic absorption spectroscopy 153
Chapter 20. Fluorine 1b5
Spectrophotometric determination of fluorine 166
Spectrophotometric determination without distillation 1b9
Pyrohydrolytic determination of fluorine 1b9
Determination of fluorine using an ion-selective
electrode 173
Chapter 21. Gallium 175
Spectrophotometric determination of gallium 175
Determination of gallium by atomic absorption 177
Chapter 22. Germanium 179
Spectrophotometric determination of germanium 179
Determination of germanium by atomic absorption
spectroscopy 181
Chapter 2J. Hydrogen 182
Water evolved at 105° 182
Method of Dean and Stark 185
Total water i8fa
Courville-Penfield method 18b
Shapiro and Brannock-Penfield method 186
Harvey-Penfield method 187
Gooch-Sergeant method 189
Contents
Chapter 2k.
Chapter 25.
Indium
Iron
191
192
Determination of metallic iron 192
Determination of ferrous iron 191*
Pratt method 196
Wilson method 197
Speotrophotometrio determination of ferrous iron 198
Determination of ferrous iron in carbonaceous shales 200
Determination of ferric iron 201
Determination of total iron 203
Spectrophotcmetric determination of total iron 20^
Titrimetric determination of total iron 207
Chapter 26.
Lead
213
Spectrophotometric determination of lead
Determination of lead by atomic absorption
spectroscopy
Determination by sublimation procedures
216
218
Chapter 27.
Magnesium
221
Chapter
Gravimetric determination with 8-hydroxyquinoline 225
Titrimetric determination of calcium and magnesium 226
Determination of calcium and magnesium by atomic
absorption spectroscopy 228
Manganese 231
Spectrophotometric determination of manganese as
permanganate 233
Oxidation with potassium periodate 231*
Oxidation with ammonium persulphate 235
Spectrophotometric determination with formaldoxime 236
Determination of manganese by atomic absorption
spectroscopy 237
Contents xiii
Chapter 29. Mercury 238
Determination of mercury in silicate rocks 238
Vapour absorption for the determination of mercury 239
Method using acid decomposition 240
Method using thermal decomposition 242
Chapter 30. Molybdenum and Tungsten 245
Spectrophotometric determination of molybdenum and
tungsten in silicate rocks 246
Determination of molybdenum in silicate rocks by
atomic absorption spectroscopy 250
Chapter 31. Nickel 252
Gravimetric determination with dimethylglyoxime 253
Spectrophotometric determination with dimethylglyoxiflie 255
Determination of nickel by atomic absorption
spectroscopy 258
Chapter 32. Niobium and Tantalum 260
Spectrophotometric determination of niobium 262
Determination of tantalum 264
Chapter 33. Nitrogen 265
Determination of nitrogen 265
Chapter 34. Phosphorus 267
Determination of phosphorus using a vanadomolybdate
reagent 269
Determination of phosphorus as a molybdenum blue 271
Chapter 35. Scandium, Yttrium and the Lanthanide Rare Earths 274
Determination of scandium in silicate rocks 274
Determination of yttrium 275
xiv Contents
Determination of the lanthanide rare earths 275
Spectrophotometric determination of rare earths
in silicate rocks 277
Determination of yttrium and certain rare earths
by atomic absorption spectroscopy ^80
Chapter 36. Selenium and Tellurium 284
Determination of selenium 284
Photometric determination using 2,2 -diaminobenzidine 285
Determination of tellurium 288
Chapter 37. Silicon 290
Gravimetric determination of silica in quartzites
and sandstones 292
Gravimetric determination in silicate and carbonate
rocks 293
Determination in carbonate rocks 294
Gravimetric determination without dehydration 295
Spectrophotometric determination of silica 296
Combined gravimetric and photometric determination
of silica 300
Determination of silica by atomic absorption
spectroscopy 302
Chapter 38. Silver, Gold and the Platinum Metals 304
Determination of silver in silicate rocks 3°4
Determination of gold in silicate rocks 305
Determination of platinum metals in silicate rocks 308
Chapter 39. Strontium 311
Determination of strontium by flame photometry 312
Determination of strontium in silicate rocks by
atomic absorption spectroscopy 311*
Chapter 40 Sulphur 317
Contents xv
Determination of free sulphur 317
Determination of sulphide-sulphur 317
Water-soluble sulphur 319
Determination of acid-soluble sulphur 319
Determination of total sulphur 320
Gravimetric determination 321
Titrimetric determination 322
Chapter 1+1. Thallium 325
Spectrophotometric determination with brilliant green 325
Fluorimetric determination in silicate rocks 327
Chapter hi. Thorium 330
Spectrophotometric determination using fluoride
precipitation 332
Spectrophotometric determination using anion-
exchange separation 335
Chapter 43. Tin
Spectrophotometric determination with catechol violet 3^0
Spectrophotometric determination using salicylidene-
anino-2-thiophenol 3^3
Determination of tin by atomic absorption spectroscopy Jkk
Chapter kk. Titanium 3^5
Spectrophotometric method using hydrogen peroxide 3^0
Spectrophotometric method using diantipyrylmethane 3W
Determination of titanium by atomic absorption
spectroscopy 350
Chapter f5. Uranium 352
Spectrophotometric determination following anion
exchange separation 353
Contents
Chapter ^6. Vanadium
557
Spectrophotometric determination of vanadium as
phosphotungstate 357
Spectrophotometric determination using N-benzoyl-
o-tolylhydroxylamine 359
Determination of vanadium by atomic absorption
spectroscopy 361
Chapter k7. Zinc
363
Spectrophotometric determination following ion-
exchange separation
Determination of zinc by atomic absorption
spectroscopy
363
366
Chapter k . Zirconium and Hafnium
368
Spectrophotometric determination of total zirconium
and hafnium 3fa8
Determination of hafnium 370
AUTHOR INDEX
SUBJECT INDEX
371
3T7
|
| any_adam_object | 1 |
| author | Jeffery, Paul G. Hutchison, D. |
| author_facet | Jeffery, Paul G. Hutchison, D. |
| author_role | aut aut |
| author_sort | Jeffery, Paul G. |
| author_variant | p g j pg pgj d h dh |
| building | Verbundindex |
| bvnumber | BV002147505 |
| callnumber-first | Q - Science |
| callnumber-label | QE438 |
| callnumber-raw | QE438 |
| callnumber-search | QE438 |
| callnumber-sort | QE 3438 |
| callnumber-subject | QE - Geology |
| classification_rvk | RB 10126 |
| ctrlnum | (OCoLC)7675115 (DE-599)BVBBV002147505 |
| dewey-full | 552/.06 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 552 - Petrology |
| dewey-raw | 552/.06 |
| dewey-search | 552/.06 |
| dewey-sort | 3552 16 |
| dewey-tens | 550 - Earth sciences |
| discipline | Geologie / Paläontologie Geographie |
| edition | 3. ed. |
| format | Book |
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| genre | (DE-588)4144950-2 Bestimmungsbuch gnd-content |
| genre_facet | Bestimmungsbuch |
| id | DE-604.BV002147505 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:41:07Z |
| institution | BVB |
| isbn | 0080238068 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001408710 |
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| owner_facet | DE-91 DE-BY-TUM DE-824 DE-11 DE-188 |
| physical | XVI, 379 S. graph. Darst. |
| publishDate | 1981 |
| publishDateSearch | 1981 |
| publishDateSort | 1981 |
| publisher | Pergamon Pr. |
| record_format | marc |
| series | Pergamon series in analytical chemistry. |
| series2 | Pergamon series in analytical chemistry. |
| spelling | Jeffery, Paul G. Verfasser aut Chemical methods of rock analysis P. G. Jeffery and D. Hutchison 3. ed. Oxford (u.a.) Pergamon Pr. 1981 XVI, 379 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Pergamon series in analytical chemistry. 4. Roches - Analyse Roches - Analyse ram Rocks Analysis Geochemische Analyse (DE-588)4290341-5 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Gestein (DE-588)4020734-1 gnd rswk-swf Chemisches Verfahren (DE-588)4454573-3 gnd rswk-swf Nachweis (DE-588)4115334-0 gnd rswk-swf (DE-588)4144950-2 Bestimmungsbuch gnd-content Gestein (DE-588)4020734-1 s Nachweis (DE-588)4115334-0 s Chemisches Verfahren (DE-588)4454573-3 s 1\p DE-604 Geochemische Analyse (DE-588)4290341-5 s 2\p DE-604 Analytische Chemie (DE-588)4129906-1 s 3\p DE-604 Hutchison, D. Verfasser aut Pergamon series in analytical chemistry. 4. (DE-604)BV001898412 4. HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001408710&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 3\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Jeffery, Paul G. Hutchison, D. Chemical methods of rock analysis Pergamon series in analytical chemistry. Roches - Analyse Roches - Analyse ram Rocks Analysis Geochemische Analyse (DE-588)4290341-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Gestein (DE-588)4020734-1 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Nachweis (DE-588)4115334-0 gnd |
| subject_GND | (DE-588)4290341-5 (DE-588)4129906-1 (DE-588)4020734-1 (DE-588)4454573-3 (DE-588)4115334-0 (DE-588)4144950-2 |
| title | Chemical methods of rock analysis |
| title_auth | Chemical methods of rock analysis |
| title_exact_search | Chemical methods of rock analysis |
| title_full | Chemical methods of rock analysis P. G. Jeffery and D. Hutchison |
| title_fullStr | Chemical methods of rock analysis P. G. Jeffery and D. Hutchison |
| title_full_unstemmed | Chemical methods of rock analysis P. G. Jeffery and D. Hutchison |
| title_short | Chemical methods of rock analysis |
| title_sort | chemical methods of rock analysis |
| topic | Roches - Analyse Roches - Analyse ram Rocks Analysis Geochemische Analyse (DE-588)4290341-5 gnd Analytische Chemie (DE-588)4129906-1 gnd Gestein (DE-588)4020734-1 gnd Chemisches Verfahren (DE-588)4454573-3 gnd Nachweis (DE-588)4115334-0 gnd |
| topic_facet | Roches - Analyse Rocks Analysis Geochemische Analyse Analytische Chemie Gestein Chemisches Verfahren Nachweis Bestimmungsbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001408710&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV001898412 |
| work_keys_str_mv | AT jefferypaulg chemicalmethodsofrockanalysis AT hutchisond chemicalmethodsofrockanalysis |