Infrared spectra of cellulose and its derivatives:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
New York, NY
Consult. Bureau
1966
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | EST: Infrakrasnye spektry celljulozy i ee proizvodnych <engl.> |
| Beschreibung: | 333 S. |
Internformat
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Datensatz im Suchindex
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| adam_text | INFRARED SPECTRA
OF CELLULOSE
AND ITS DERIVATIVES
By
Rostislav Georgievich Zhbankov
Institute of Physics
Academy of Sciences of the Belorussian SSR
Minsk
jj CONSULTANTS BUREAU • NEW YORK -1966
i/
CONTENTS
I
CHAPTER I Methods for Obtaining the Infrared Spectra of
Cellulose and Related Materials 1
Investigation of Unchanged Fibrous Material 18
The Suspension Method 20
, The Solid Immersion Media Method 20
i Production of Thin Fiber Films Without Use of an Immersion
Medium 23
j Production of Infrared Spectra of Cellulose from Alkaline
Aqueous Solutions 31
Production of Thin Films of Water-Soluble Compounds from
Their Aqueous Solutions 31
CHAPTER II Model Cellulose Compounds Unmodified
| i Celluloses 35
j , Monosaccharides 37
i , Disaccharides ~ 51
j Polysaccharides • 53
j ; Cellulose from One-Year-Old Plants 57
Cellulose from Young Wood Shoots 63
Cellulose from Woods of Various Ages 68
f, Samples of Technical Cellulose 71
CHAPTER III Hydrocellulose Products of the Partial Hydrolysis of
Cellulose 73
Cellulose Regenerated After Treatment with Alkali of
Various Concentrations 80
Cellulose Subjected to Grinding 84
Viscose Fibers 86
Effect of Hydrogen Bonds on the Structure of Cellulose 86
Alkaline Cellulose 89
Products of the Partial Hydrolysis of Cellulose 90
xi
xii CONTENTS
CHAPTER IV Cellulose Esters and Ethers 93
Cellulose Acetates Produced under Homogeneous
Conditions of Acetylation and Partial Hydrolysis 100
Cellulose Acetates Produced under Heterogeneous
Conditions of Acetylation and Partial Hydrolysis 103
Comparison of Spectral Data with the Results of Viscometric
Analyses of Cellulose Acetates 105
Acetylcellulose Fibers with Different Acetyl Group Contents -107
Special Features of the Spectra of Ethers and Esters of
Cellulose Ill
CHAPTER V Oxidation Products of Cellulose Salts of Oxidation
Products of Cellulose 117
Monocarboxycellulose 119
Dialdehydrocellulose 122
Dialdehydrocellulose Oxidized by Nitrogen Oxides 123
Dicarboxycellulose 124
Dialcoholcellulose 124
Salts of Oxidation Products of Cellulose 125
Salts of Cellulose Oxidation Products with Inorganic Cations 127
Salts of Cellulose Oxidation Products with Organic Cations 129
CHAPTER VI New Types of Cellulose Derivative 131
Esters of Cellulose with Phosphorus-Containing Acids 132
Esters of Cellulose with Chlorinated Aliphatic Acids 137
Stable Xanthate Derivatives of Cellulose 140
Investigation of the Products of Thermal Decomposition of
Cellulose Methylxanthate 145
Cellulose Compounds Containing New Functional Groups 148
Graft Copolymers of Cellulose with Poly-2-methyl-5-
vinylpyridine 150
Graft Copolymers of Cellulose and Carbon Chain Polymers,
Obtained by Initiating the Graft Polymerization with
Pentavalent Vanadium Compounds 157
Products of the Ion-Exchange of Graft Copolymers of
Cellulose and Polyacrylhydroxamic Acid with Ions of
Fe3+ and Cu2+ 160
CHAPTER VII The Possibilities of the Infrared Spectroscopic
Method for Investigation of the Properties of Cellulose and
Its Derivatives 167
The 2000-4000 cm1 Region 167
The 1500-2000 cm1 Region 174
The 1200-1500 cm1 Region 177
CONTENTS xiii
The 950-1200 cm1 Region 181
The 700-950 cm1 Region 182
The 400-700 cm1 Region 184
APPENDICES* 187
Appendix I Spectra of Mono-, Di-, and Polysaccharides
and their Derivatives, and Spectra of Polyhydric
Alcohols 189
Appendix II Spectra of Unmodified Celluloses 219
Appendix III Spectra of Celluloses Regenerated After
Treatment with Aqueous Alkali of Various Concentra
tions Spectra of Viscose Silk and of Alkaline Cellu
lose 235
Appendix IV Spectra of Products of Partial Hydrolysis and
Ethanolysis of Cellulose 244
Appendix V Spectra of Cellulose Ethers and Esters 249
Appendix VI Spectra of Oxidation Products of Cellulose 263
Appendix VII Spectra of Salts of Cellulose Oxidation
Products 273
Appendix VIII Spectra of New Types of Cellulose
Derivatives and of Modified Celluloses 277
Appendix IX Characteristic Vibration Frequencies of
Groups and Bonds in the Molecules of Cellulose and
Its Derivatives 304
LITERATURE CITED 325
•A detailed listing of all the spectra presented in each Appendix appears
the first page of that Appendix
|
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| physical | 333 S. |
| publishDate | 1966 |
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| spelling | Žbankov, Rotislav G. Verfasser aut Infrared spectra of cellulose and its derivatives New York, NY Consult. Bureau 1966 333 S. txt rdacontent n rdamedia nc rdacarrier EST: Infrakrasnye spektry celljulozy i ee proizvodnych <engl.> Cellulose (DE-588)4147454-5 gnd rswk-swf Infrarot-Spektrum (DE-588)4137742-4 gnd rswk-swf Cellulose (DE-588)4147454-5 s Infrarot-Spektrum (DE-588)4137742-4 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001391094&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Žbankov, Rotislav G. Infrared spectra of cellulose and its derivatives Cellulose (DE-588)4147454-5 gnd Infrarot-Spektrum (DE-588)4137742-4 gnd |
| subject_GND | (DE-588)4147454-5 (DE-588)4137742-4 |
| title | Infrared spectra of cellulose and its derivatives |
| title_auth | Infrared spectra of cellulose and its derivatives |
| title_exact_search | Infrared spectra of cellulose and its derivatives |
| title_full | Infrared spectra of cellulose and its derivatives |
| title_fullStr | Infrared spectra of cellulose and its derivatives |
| title_full_unstemmed | Infrared spectra of cellulose and its derivatives |
| title_short | Infrared spectra of cellulose and its derivatives |
| title_sort | infrared spectra of cellulose and its derivatives |
| topic | Cellulose (DE-588)4147454-5 gnd Infrarot-Spektrum (DE-588)4137742-4 gnd |
| topic_facet | Cellulose Infrarot-Spektrum |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001391094&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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