Systematic qualitative analysis:
Gespeichert in:
| 1. Verfasser: | |
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| Format: | Buch |
| Sprache: | Undetermined |
| Veröffentlicht: |
London
Butterworth
1961
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| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 198 S. |
Internformat
MARC
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Datensatz im Suchindex
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| adam_text | SYSTEMATIC
QUALITATIVE
ANALYSIS
i
An Introduction
G A MORRISON
MA,D Phil (Oxon )
Lecturer,
Department of Chemistry,
University College of Wales,
Aberystwyth
LONDON
BUTTERWORTHS
CONTENTS
l age
Prefacev
Introduction1
DISSOCIATION CONSTANTS, BUFFERED SOLUTIONS
AND SOLUBILITY CONSTANTS 6
APPARATUS AND TECHNIQUES 18
Use of apparatus 22
Procedures24
PRELIMINARY TESTS 30
Preparation of solutions of ions for analysis
bygroups48
SEPARATION INTO GROUPS: THEORY 51
Group I: the use of chloride 53
Group II: the use of sulphide in acid conditions 54
Group III: use of alkali 60
Group IV: the use of sulphide in alkaline con
ditions66
Group Y: the use of carbonate , 66
Group VI: the ail kali metals and magnesium 71
SEPARATION INTO GROUPS: PRACTICAL DETAILS 72
Group I 72
Group II 72
Group III 75
Group IV 78
Group V 79
vii
CONTENTS
Page
THE ANALYSIS OF GROUP I: THE SEPARATION OF
I LEAD, SILVER AND MERCUROUS MERCURY,
FTHALLOUS THALLIUM, TUNGSTATE AND SILI
CATE81
Practical details 83
Confirmatory tests 86
THE ANALYSIS OF GROUP II: THE SEPARATION OF
MERCURIC MERCURYT LEAD, BISMUTH, CAD-
MIUM, COPPER, ARSENIC, ANTIMONY AND
TIN, FGOLD, PLATINUM, PALLADIUM, SKLE-
NIUM, TELLURIUM AND MOLYBDENUM 91
GroupIla94
Group lib 96
Practical details: separation of sub-groups Ila
andlib97
Practical details: Group Ila 99
Practical details: Group lib 103
Confirmatory tests 107
THE ANALYSIS OF GROUP III: THE SEPARA J ION
OF ALUMINIUM, CHROMIUM AND II: ON,
(VANADIUM, BERYLLIUM, TITANIUM, CERJ UM,
THORIUM, ZIRCONIUM AND URANIUM 115
Practical details 117
Confirmatory tests 121
THE ANALYSIS OF GROUP IV: THE SEPARATION
OF ZINC}, NICKEL, COBALT, MANGANESE AND
FTHALLICTHALLTUM127
Practical details 128
Confirmatory tests 132
THE ANALYSIS OF GROUP V: THE SEPARATION
OF CALCIUM, STRONTIUM AND BARIUM 134
Practical details 135
Confirmatorytests136
viii
CONTENTS
Page
THE ANALYSIS OF GROUP YI: THE SEPARATION
OF POTASSIUM, SODIUM, MAGNESIUM AND
TLITH3UM 13S
Practical details 139
Confirmatory tests 141
ANALYSIS FOR ANIONS 144
U se of potassium permanganate and manga-
nous chloride 145
Preparation of solutions of anions for pre
cipitating reagents 147
Use of aqueous barium chloride 152
Use of aqueous silver nitrate 155
Useofaqueouscalciumchloride162
Use of aqueous neutral ferric chloride 165
The brown ring test 167
CONFIRMATION OF ANIONS 1 6 9
Shorter syllabus only 169
fLongersyllabus174
Example procedures for some mixtures of
related anions 1S3
APPENDIX185
Bench reagents 185
Side reagents 186
Index t 191
ix
|
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| spelling | Morrison, George A. Verfasser aut Systematic qualitative analysis London Butterworth 1961 198 S. txt rdacontent n rdamedia nc rdacarrier Qualitative Analyse (DE-588)4115680-8 gnd rswk-swf Anorganische Analyse (DE-588)4068735-1 gnd rswk-swf Qualitative Analyse (DE-588)4115680-8 s Anorganische Analyse (DE-588)4068735-1 s DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001341821&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Morrison, George A. Systematic qualitative analysis Qualitative Analyse (DE-588)4115680-8 gnd Anorganische Analyse (DE-588)4068735-1 gnd |
| subject_GND | (DE-588)4115680-8 (DE-588)4068735-1 |
| title | Systematic qualitative analysis |
| title_auth | Systematic qualitative analysis |
| title_exact_search | Systematic qualitative analysis |
| title_full | Systematic qualitative analysis |
| title_fullStr | Systematic qualitative analysis |
| title_full_unstemmed | Systematic qualitative analysis |
| title_short | Systematic qualitative analysis |
| title_sort | systematic qualitative analysis |
| topic | Qualitative Analyse (DE-588)4115680-8 gnd Anorganische Analyse (DE-588)4068735-1 gnd |
| topic_facet | Qualitative Analyse Anorganische Analyse |
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