Programmed temperature gas chromatography:
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
New York
Wiley
1966
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XVI, 305 S. |
Internformat
MARC
| LEADER | 00000nam a2200000 c 4500 | ||
|---|---|---|---|
| 001 | BV001939943 | ||
| 003 | DE-604 | ||
| 005 | 20170608 | ||
| 007 | t | ||
| 008 | 890928s1966 |||| 00||| eng d | ||
| 035 | |a (OCoLC)635978810 | ||
| 035 | |a (DE-599)BVBBV001939943 | ||
| 040 | |a DE-604 |b ger |e rakddb | ||
| 041 | 0 | |a eng | |
| 049 | |a DE-91 |a DE-355 |a DE-83 |a DE-11 | ||
| 050 | 0 | |a QD271 | |
| 082 | 0 | |a 544.926 | |
| 084 | |a VG 7400 |0 (DE-625)147205:253 |2 rvk | ||
| 100 | 1 | |a Harris, Walter E. |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Programmed temperature gas chromatography |c Walter E. Harris ; Henry W. Habgood |
| 264 | 1 | |a New York |b Wiley |c 1966 | |
| 300 | |a XVI, 305 S. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 7 | |a Chromatographie en phase gazeuse |2 ram | |
| 650 | 4 | |a Gas chromatography | |
| 650 | 0 | 7 | |a Gaschromatographie |0 (DE-588)4019330-5 |2 gnd |9 rswk-swf |
| 655 | 7 | |a Temperaturprogramm |2 gnd |9 rswk-swf | |
| 689 | 0 | 0 | |a Gaschromatographie |0 (DE-588)4019330-5 |D s |
| 689 | 0 | 1 | |a Temperaturprogramm |A f |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Habgood, Henry W. |e Verfasser |4 aut | |
| 856 | 4 | 2 | |m HEBIS Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 940 | 1 | |q TUB-nveb | |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-001264430 | ||
Datensatz im Suchindex
| _version_ | 1804116380209905664 |
|---|---|
| adam_text | Programmed Temperature
Gas Chromatography
WALTER E HARRIS
Professor of Analytical Chemistry
Department of Chemistry
University of Alberta
Edmonton, Alberta, Canada
HENRY W HABGOOD
Chief Fuels Branch
Research Council of Alberta
Edmonton, Alberta, Canada
John Wiley amp; Sons, Inc , New York / London / Sydney
Contents
Principal symbols x n i
CHAPTERI
GASCHROMATOGRAPHYANDTEMPERATUREPROGRAMMING
1 01 General Introduction 1
1 02 Temperature Programming 11
1 03 Terms and Concepts • • 15
1 04 Summary • • • • • 21
References21
CHAPTER2
TEMPERATUREEFFECTSINGASCHROMATOGRAPHY
2 01 Flow Rate and Pressure Drop 23
2 02 Retention Volume 29
2 03 Band Broadening 34
2 04 Summary 46
References47
CHAPTER3
RETENTIONTHEORYIRETENTIONVOLUMEAND
RETENTIONTEMPERATURE
3 01 Corrected Isothermal Retention Volume 49
3 02 Stepwise Increase in Temperature 51
3 03 Linear Temperature Program 52
3 04 Characteristic Curves of Linear PTGC 56
3 05 Retention Volumes in Linear PTGC 59
3 06 Nonlinear Heating Programs 63
3 07 Effect of Pressure Drop 71
3 08 Exact Solutions to Characteristic Equations 75
3 09 Summary 82
References82
ix
X Contents
CHAPTER4
RETENTIONTHEORYIIOPTIONALANDAPPROXIMATEFORMS
FORTHECALCULATIONSOFPTGC
4 01 Reduced-Temperature Scale: Baumann, Klaver, and Johnson 84
4 02 Universal Curves: Said and Sternberg 86
4 03 Effect of Neglecting the Column Dead space 91
4 04 Calculations Neglecting Dead Space: Rowan 96
4 05 Significant Temperature: Giddings 101
4 06 Direct Use of Observed Retention Volumes and Retention
Times Instead of Pressure-Corrected Values 104
4 07 Summary 107
References107
CHAPTER5
COLUMNEFFICIENCYRESOLUTION
5 01 Column Efficiency: Number of Theoretical Plates 109
5 02 Band Broadening Due to Sample Injection and to Nonuni-
formity of Temperature
503Resolution
5 04 Intrinsic Resolution
5 05 Approximate Expression for Intrinsic Resolution of Closely
Spaced Peaks
5 06 Effect of Large Column Dead Space Capillary Columns
5 07 Relative Retention
5 08 Effective Peak Number
5 09 Maximizing Resolution
5 10 Summary
References
CHAPTER6
QUALITATIVEASPECTSOFRETENTIONTEMPERATURE
6 01 Homologous-Series Relationships 141
6 02 Retention Temperature Constants 149
6 03 Retention Indices 153
6 04 Other Index Systems Carbon Number, Steroid Number,
Phenyl Number 162
6 05 Relative Retention Volumes Theoretical-Nonane System 166
6 06 Summary 167
References168
Contents xi
CHAPTER7
PRACTICALINONINSTRUMENTAL
7 01 When to Choose Temperature Programming 169
7 02 Programming Conditions 172
7 03 Stationary Phase 178
7 04 Inert Support 186
7 05 Column Conditioning 187
7 06 Carrier Gas 188
7 07 Sample Injection 190
7 08 Speed of Analysis 201
7 09 Errors 203
7 10 Detection Limit 210
7 11 Reporting of Data Calculations 214
7 12 Summary 219
References 221
CHAPTER8
PRACTICALIIINSTRUMENTAL
8 01 Stabilization of Carrier-Gas Flow Rate 223
8 02 Base-Line Control, Dual Columns, and Dual Channels 226
8 03 Temperature Control 233
8 04 Laboratory-Built Instruments 242
8 05 Selection of Apparatus 245
8 06 Suppliers of Commercial Equipment 247
8 07 Summary 249
References250
CHAPTER9
SELECTEDAPPLICATIONS
9 01 Mixtures of Wide Boiling Range 251
9 02 Simulated Distillation 266
9 03 Trace Analysis 271
9 04 Pyrolysis Gas Chromatography 273
9 05 Preparative PTGC 276
9 06 Summary 279
References280
APPENDIX
Retention Indices of Hydrocarbons 283
AUTHORINDEX289
SUBJECTINDEX293
|
| any_adam_object | 1 |
| author | Harris, Walter E. Habgood, Henry W. |
| author_facet | Harris, Walter E. Habgood, Henry W. |
| author_role | aut aut |
| author_sort | Harris, Walter E. |
| author_variant | w e h we weh h w h hw hwh |
| building | Verbundindex |
| bvnumber | BV001939943 |
| callnumber-first | Q - Science |
| callnumber-label | QD271 |
| callnumber-raw | QD271 |
| callnumber-search | QD271 |
| callnumber-sort | QD 3271 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 7400 |
| ctrlnum | (OCoLC)635978810 (DE-599)BVBBV001939943 |
| dewey-full | 544.926 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 544 - [Unassigned] |
| dewey-raw | 544.926 |
| dewey-search | 544.926 |
| dewey-sort | 3544.926 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>01435nam a2200397 c 4500</leader><controlfield tag="001">BV001939943</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20170608 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">890928s1966 |||| 00||| eng d</controlfield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)635978810</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)BVBBV001939943</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield><subfield code="e">rakddb</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-91</subfield><subfield code="a">DE-355</subfield><subfield code="a">DE-83</subfield><subfield code="a">DE-11</subfield></datafield><datafield tag="050" ind1=" " ind2="0"><subfield code="a">QD271</subfield></datafield><datafield tag="082" ind1="0" ind2=" "><subfield code="a">544.926</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">VG 7400</subfield><subfield code="0">(DE-625)147205:253</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Harris, Walter E.</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Programmed temperature gas chromatography</subfield><subfield code="c">Walter E. Harris ; Henry W. Habgood</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">New York</subfield><subfield code="b">Wiley</subfield><subfield code="c">1966</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XVI, 305 S.</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1=" " ind2="7"><subfield code="a">Chromatographie en phase gazeuse</subfield><subfield code="2">ram</subfield></datafield><datafield tag="650" ind1=" " ind2="4"><subfield code="a">Gas chromatography</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Gaschromatographie</subfield><subfield code="0">(DE-588)4019330-5</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="655" ind1=" " ind2="7"><subfield code="a">Temperaturprogramm</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Gaschromatographie</subfield><subfield code="0">(DE-588)4019330-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Temperaturprogramm</subfield><subfield code="A">f</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Habgood, Henry W.</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">HEBIS Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="940" ind1="1" ind2=" "><subfield code="q">TUB-nveb</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-001264430</subfield></datafield></record></collection> |
| genre | Temperaturprogramm gnd |
| genre_facet | Temperaturprogramm |
| id | DE-604.BV001939943 |
| illustrated | Not Illustrated |
| indexdate | 2024-07-09T15:37:35Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001264430 |
| oclc_num | 635978810 |
| open_access_boolean | |
| owner | DE-91 DE-BY-TUM DE-355 DE-BY-UBR DE-83 DE-11 |
| owner_facet | DE-91 DE-BY-TUM DE-355 DE-BY-UBR DE-83 DE-11 |
| physical | XVI, 305 S. |
| psigel | TUB-nveb |
| publishDate | 1966 |
| publishDateSearch | 1966 |
| publishDateSort | 1966 |
| publisher | Wiley |
| record_format | marc |
| spelling | Harris, Walter E. Verfasser aut Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood New York Wiley 1966 XVI, 305 S. txt rdacontent n rdamedia nc rdacarrier Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd rswk-swf Temperaturprogramm gnd rswk-swf Gaschromatographie (DE-588)4019330-5 s Temperaturprogramm f DE-604 Habgood, Henry W. Verfasser aut HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Harris, Walter E. Habgood, Henry W. Programmed temperature gas chromatography Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| subject_GND | (DE-588)4019330-5 |
| title | Programmed temperature gas chromatography |
| title_auth | Programmed temperature gas chromatography |
| title_exact_search | Programmed temperature gas chromatography |
| title_full | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_fullStr | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_full_unstemmed | Programmed temperature gas chromatography Walter E. Harris ; Henry W. Habgood |
| title_short | Programmed temperature gas chromatography |
| title_sort | programmed temperature gas chromatography |
| topic | Chromatographie en phase gazeuse ram Gas chromatography Gaschromatographie (DE-588)4019330-5 gnd |
| topic_facet | Chromatographie en phase gazeuse Gas chromatography Gaschromatographie Temperaturprogramm |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001264430&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT harriswaltere programmedtemperaturegaschromatography AT habgoodhenryw programmedtemperaturegaschromatography |