Physical chemistry of surfaces:
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Buch |
| Sprache: | German |
| Veröffentlicht: |
New York
Interscience Publ.
1967
|
| Ausgabe: | 2. ed. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XX, 747 S. Ill., graph. Darst. |
| ISBN: | 0470007931 |
Internformat
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| 245 | 1 | 0 | |a Physical chemistry of surfaces |c Arthur W. Adamson |
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| 650 | 4 | |a Chemistry, Physical and theoretical | |
| 650 | 4 | |a Surface Properties | |
| 650 | 4 | |a Surface chemistry | |
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Datensatz im Suchindex
| _version_ | 1804116370050252800 |
|---|---|
| adam_text | Physical Chemistry
of Surfaces
Second Edition
ARTHUR W ADAMSON
Department of Chemistry, University of Southern California
Los Angeles, California
INTERSCIENCE PUBL [SHERS
a division of John Wiley it Sons, New Ymh • Lomion • Sydney
Contents
I Capillarity 1
1 Surface Tension and Surface Free Energy 1
2 The Equal-ion of Young and Laplace 4
3 Some Experiments viih Soap Films 6
4 The Treatment of Capillary Rise 9
A Introductory Discussion 9
B Exact Solution to the Capillary Rise Problem 12
C Experimental Aspects of the Capillary Rise Method 17
D Variations in the Capillary Rise Method 18
5 The Maximum Bubble Pressure Method 18
0 The Drop Weight Met,hod 21
7 The Ring Method 24
8 Wilhelmy Slide Method 26
9 Methods Based on the Shape of Static Drops or Bubbles 28
A Sessile Drop or Bubble Method 28
B Pendant Drop Method 30
10 Dynamic Methods of Measuring Surface Tension 37
A Flow Methods 37
B Capillary Waves 40
11 Miscellaneous Methods of Surface Tension Measurement 41
12 Surface Tension Values as Obtained by Dif lerent Methods 42
13 Problems 46
General References 49
Textual References 49
II The Nature and Thermodynamics of Liquid Interfaces 53
1 One-Component Systems 53
A Surface Thermodynamic Quantities and the Temperature De
pendence of the Surface Free Energy 53
B The Total Surface Energy, E 56
C Change in Vapor Pressure for a Curved Surface 58
D Effect of Curvature on Surface Tension 60
E Effect, of Pressure on Surface Tension 60
F Effects of Other Variables 61
2 The Structural and Theoretical Treatment of Liquid Interlaces 62
A Further Development of the Thermodynamic Treatment of the
Surface Region 65
B Calculation of the Surface Energy and ] ree Energy of Liquids 67
3 Orientation at, Interfaces 70
xi
xii CONTENTS
4 The Surface Tension of Solutions 73
5 Thermodynamics of Binary Systems—the ribbs Equation 78
A Definition of Surface Excess 78
B The Gibbs Equation 80
C Alternate Methods of Locating the Dividing Surface 81
D Limiting Relationships between the V irions Surface Excess
Quantities 84
E The Thermodynamics of Surfaces Using the Concept of a Sur
face Phase 86
6 Verification of the Gibbs Equation—Direct Measurements of Sur
face Excess Quantities 87
A The Microtome Methods for Measuring V 88
B The Tracer Method for Measuring Surface Excess 89
C An Apparent Violation of the Gibbs Equation 92
7 Gibbs Monolayers 94
A The Two-Dimensional Ideal Gas Law 95
B Nonideal Two-Dimensional Gases 97
C The Osmotic Pressure Point of View 100
D Traube s Rule 101
E Some Further Comments on Gibbs Monolayers 102
8 Problems 193
General References 108
Textual References 108
III Surface Films on Liquid Substrates 113
1 Introduction 113
2 The Spreading of One Liquid on Another 117
A Criteria for Spreading 117
B Kinetics of Spreading Processes 122
C Lenses 123
3 Experimental Techniques for the Study of Monomolecular Films 123
A Measurement of ir 124
B Surface Potentials 128
C Surface Viscosities 131
D Optical Properties of Monolayers 136
E The Ultramicroscope 139
F Electron Microscopy and Diffraction 139
G Other Techniques 139
4 States of Monomolecular Films 141
5 Correspondence between v and a Three-Dimensional Pressure 14 5
6 Further Discussion of the States of Monoitiolecular Films 145
A Casebus Films 145
B The Liquid Expanded State 147
C Intermediate and L Films 150
D The Solid State 152
E Viscosities of Monolayers 153
F Effect of Changes in the Aqueous Sub rule 153
CONTENTS xiii
G General Correlations between Molecular Structure and tiie
Type of Film Formed 155
7 Mixed Films 157
8 Evaporation Kates through Monomoleculn r Films 1G0
9 Reactions in Monomolecular Films 164
A Kinetics of Reactions in Films 104
B Kinetics of Formation and Hydrolysis of lvsters 167
C Reactions at a Double Bond 170
D Other Chemical Read,ions 171
E Rate of Dissolving of Monolayers 172
10 Protein and Polymer Films 173
A Spreading Techniques 174
B Physical Properties of Protein Films 175
C Reactions of Protein Films 179
D Protein Films at Oil-Water Interfaces ISO
E Polymer Films 181
J1 Films at Liquid-Liquid Interfaces and oil Liquid Surfaces Other
than Water 182
12 Charged Films 184
A Equation of State of a Charged Film 184
B Interfacial Potentials 189
13 Capillar} Waves 191
14 Films Deposited on Solids 195
A Built-Up Films 195
B Monolayers 196
15 Problems 19S
General References 201
Textual References 201
IV Electrical Aspects of Surface Chemistry 209
1 Introduction 209
2 The Electrical Double Layer 210
3 The Stern Treatment of the Electrical Double Layer 214
4 The Free Energy of a Diffuse Double Layer 217
5 Repulsion between Two Plane Double La urs 218
6 The Nature of the Different Parts of the Double Layer 219
7 Further Treatment of the Stern and Diffuce Layers 222
8 The Zeta Potential 223
A Electrophoresis 224
B Electroosmosis 225
C Streaming Potential 227
D Sedimentation Potential 228
E Further Developments in the Theory of Elect rokinetic Phe
nomena 229
F General Observation on f Potentials—Stability of Colloids 229
9 Electrocapillarity 231
A Thermodynamics of the Electrocapillar- Effect 234
B Experimental Methods 237
xiv CONTENTS
C Results for the Mercury-Aqueous Solution Interface 2 3 9
IX Effect, of Uncharged Solutes and Changes of Solvent, 246
E Other Elect,rocapillary Systems 246
F The Potential Difference between Two Phases 247
10 Types of Potentials and the Meaning of Potential Differences When
Two Phases are Involved 247
A The Various Types of Potentials 247
B Volta Potentials, Surface Potential Differences, and the
Thermionic Work Function 250
C Electrochemical and Electrode Potentials 252
D Irreversible Electrode Phenomena 254
11 Problems 258
General References 260
Textual References 260
V Surfaces of Solids 263
1 Introduction 263
A The Surface Mobility of Solids—Sintering 263
B Effect of Past History on the Condition of Solid Surfaces 266
2 Thermodynamics of Crystals 268
A Surface Tension and Surface Free Energy 268
B The Equilibrium Shape of a Crystal 270
C The Kelvin Equation 272
3 Theoretical Estimates of Surface Energies and Free Energies 272
A Covalently Bonded Crystals 272
B Rare Gas Crystals 273
C Ionic Crystals 277
D Molecular Crystals 280
E Metals 280
4 Factors Affecting the Surface Energies and Surface Tensions of
Actual Crystals 281
A State of Subdivision 281
B Deviations from Ideal Considerations 282
C Dislocations 284
D Surface Heterogeneity 288
5 Experimental Estimates of Surface Energies and Free Energies 289
A Methods Depending on the Direct Manifestation of Surface
Tensional Forces 289
B Surface Energies and Free Energies from Heats of Solutions 292
C Relative Surface Tensions from Equilibrium Shapes of Crystals 294
D Dependence of Other Physical Properties on Surface Energy
Changes at a Solid Interface 295
6 Experimental Methods for Determining Surface Structure 297
A Low Energy Electron Diffraction 297
B Field Emission and Field Ion Microscopy 301
C Other Methods 307
7 Reactions of Solid Surfaces 307
8 Problems 310
CONTENTS xv
General References 312
Textual References 3 12
VI Long Range Forces 317
1 Forces between Atoms and Molecules 317
2 Qualitative Evidence for Long Range Fore s 322
A Evidence for Deep Surface Orientation 322
B Apparent Long Range Interaction between iYlacromolecules 323
C Entropy Considerations in the Case of Highly Asymmetric
Molecules 320
3 Long Range Forces 321)
A Dispersion or van der Waals Force 321)
B Electrical Double Layer Interact ions 333
C Dipole-Induced Dipole Propagation 334
4 Experimental Verification of Long Range Forces 335
A Direct Measurement, of Long Range van der Waals At traction 335
B The Balance of Forces in a Soap Film 337
C Flocculation of Lyophobie Colloids 337
5 Problems 33!)
General References 342
Textual References 342
VII The Solid-Liquid Interface—Contact Angle—Nucleation 345
1 Introduction 345
2 Surface Free Energies from Solubility Changes 346
3 Surface Energy and Free Energy Difference: from Immersion and
Adsorption Studies 348
A Heat of Immersion 34S
B Surface Energy and Free Energy Changes from Adsorption
Studies 350
4 Contact, Angle Phenomena 352
A Contact Angles 352
B Measurement of Contact Angle 355
C Nonuniform Surfaces 357
D Hysteresis in Contact, Angle Measurements 35!)
E Results of Contact, Angle Measurement- 303
5 Some Theoretical Aspects of Contact Angle Phenomena 369
A Thermodynamics of the Young and Duple Equation 309
B Semiempirical Models for Contact Angle Phenomena 372
( The Formation of a New Phase—Nucleating and Crystal Growth 375
A Classical Nucleation Theory 375
B Results of Nucleat ion Studies 382
C Crystal Growth 385
D Some Further Remarks on Nucleat ion Theory 3S7
7 Problems 388
General References 391
Textual References 391
XVI CONTENTS
VIII The Solid-Liquid Interface Adsorption from Solution
1 Adsorption of Nonelectrolylies from Dilute Solution
A Adsorption Isotherms
B Qualitative Results of Adsorption Studies—Traube s Rule
C Multilayer Adsorption
2 Adsorption of Polymers
3 Surface Area Determination
4 Adsorption in Binary Liquid Systems
A Adsorption at the Solid-Solution Interface
B Interrelations bet,ween Adsorption at Different Interfaces
C Heat of Adsorption at the Solid-Solution Interface
5 Adsorption of Electrolytes
A Stern Layer Adsorption
B Counterfoil Adsorption—Ion Exchange
6 Problems
General References
Textual References
IX Friction arid Lubrication ; Adhesion
1 Introduction
2 Friction between Unlubricatod Surfaces
A Amontons Law
B Nature of the Contact between Two Solid Surfaces
C Role of Shearing and Plowing; Explanai ion of Amontons Law
D Static and Stick-Slip Friction
3 Two Special Cases of Friction
A Use of Skid Marks to Estimate Vehicle Speeds
B Ice and Snow
4 Metallic Friction—Effect, of Oxide Films
5 Friction between Nonmetals
A Relatively Isotropic Crystals
B Layer Crystals
C Plastics
G Some Further Aspects of Friction
7 Friction between Lubricated Surfaces
A Boundary Lubrication
B The Mechanism of Boundary Lubrication
8 Adhesion
A Ideal Adhesion
B Practical Adhesion
9 Problems
General References
Textual References
X Wetting, Flotation, and Detergency
1 Introduction
2 Wetting
A Wetting as a Contact Angle Phenomenon
B Wetting as a Capillary Action Phenomenon
39S
40-
41S
42
43
43
43
43
43S
44~
46S
47?
CONTENTS xvii
3 Water Repellcncy 476
4 Flotation 47S
A The Role of Contact Angle in Flotation 47!)
B Flotation of Metallic Minerals 484
C Flotation of :oninetallic; Minerals 487
5 Detergency 48!)
A General Aspects of Soil Removal 489
B Properties of Colloidal Electrolyte Solnt ions 491
C Factors in Detergent Action 495
D Adsorption of Detergents on Fabrics 497
E Detergents in Commercial Use 498
6 Problems 499
General References 501
Textual References 501
XI Emulsions and Foams 505
1 Introduction 505
2 Emulsions—General Properties 506
3 Factors Determining Emulsion Stability 50S
A Macroscopic Theories of Emulsion Stabilization SOS
B Specific Chemical and Structural Effect- 510
C Long Range Forces its a Factor in Emulsion Stability 512
D Stabilization of Emulsions by Solid Panicles 514
4 The Ageing and Inversion of Emulsions 515
A Flocculation and Coagulation Kinetics 515
B Inversion and Breaking of Emulsions 517
5 Spontaneous Emulsification—Micellar Emulsions 519
6 Serniempirical Treatments of Emulsion Stability 520
A Hydrophile-Lipophile Balance 520
B Other Treatments 522
7 Practical Aspects of Emulsions 522
8 Foams—The Structure of Foams 523
9 Foam Drainage 526
A Drainage of Single Films 526
B Drainage of Foams 528
10 The Stability of Foams 52!)
11 Foaming Agents and Foams of Practical Importance 531
12 Problems 532
General References 533
Textual References 533
XII The Solid-Gas Interface—General Considerations 537
1 Introduction 537
2 The Surface Area of Solids 53S
A The Meaning of Surface Area 53S
B Methods Requiring Knowledge of the Surface Free Energy or
Total Energy 541
C Rate of Dissolving 543
XVI11 CONTENTS
D Surface Areas from ( he Electrical Potential of an Adsorbed
Layer 545
E The Mercury Porosimeter 546
F Other Methods of Surface Area Estimation 549
3 The Structural and Chemical Nature of Solid Surfaces 55 1
4 The Nature of the Solid-Adsorbate Complex 552
A Effect of Adsorption on Adsorbate Properties 552
B Effect, of the Adsorbate on the Adsorbent, 558
C The Adsorbate-Adsorbent Bond 560
5 Problems 561
General References 561
Textual References 562
XIII Adsorption of Gases and Vapors on Solids 565
i
1 Introduction 565
2 The Adsorption Time 568
3 The Langmuir Adsorption Isotherm 569
A Kinetic Derivation 57(1
B Statistical Thermodynamic Derivation 572
C Adsorption Entropies 575
D Lateral Interaction 57,8
E Experimental Applications of the Langmuir liquation 580
4 Experimental Procedures 581
5 The BET and Related Isotherms 584
A Derivation of the BET Equation 584
B Properties of the BET Equation 586
C Modifications of (he BET Equation 588
6 Isotherms Based on the Equation of State ef the Adsorbed Film 589
A Types of Force-Area Diagrams from Adsorption Isotherms 590
B Adsorption Isotherms from Two-Dimensional Equations of
State 590
7 The Potential Theory 595
A The Polanyi Treatment 595
B Correspondence between the Potential Theory and that of a
Two-Dimensional Film 598
C Isotherms Based on an Assumed Variation of Potential with
Distance 51)8
D The Polarization Model 600
8 Comparison of the Surface Areas from the Various Multilayer
Models—The Characteristic Isotherm 602
9 Surface Areas from Submonolayer Adsorption 605
10 Adsorption Steps and Phase Transformations 607
11 Thermodynamics of Adsorption 60!)
A Theoretical Considerations 60!)
B Experimental Heats and Entropies of Adsorption 615
12 Critical Comparison of (he Various Model-; for Adsorption 620
CONTENTS xix
A The Liuigmuir-BET Model G20
B Two-Dimensional Equation of State Treatments G22
C The Potential Model 622
13 Adsorption 011 Heterogeneous Surfaces 625
A Site Energy Distributions 625
B Thermodynamics of Adsorption on Heterogeneous Surfaces 632
]4 Hate of Adsorption 634
15 Adsorption on Porous Solids—Hysteresis 634
A Molecular Sieves 634
B Capillar} Condensation 637
1G Problems 641
General References 643
Textual References 644
XIV Chemisorption and Catalysis 649
1 Introduction 649
2 Chemisorption Isotherms 051)
A Variable Heat of Adsorption 650
B Effect of Site and Adsorbate Coordination Number 654
C Adsorption Thermodynamics 656
3 Kinetics of Chemisorption 656
A Activation Energies 656
B Rates of Adsorption 660
C Rates of Desorption 663
D Flash Desorption Studies 664
E Other Kinetic Techniques 665
4 Surface Mobility 666
5 The Chemisorption Bond 66S
A The Localized Bond Approach 668
B Metals 671
C Semiconductors 674
D Acid-Base Systems 676
6 Mechanisms of Heterogeneous Catalysis 678
A Adsorption or Desorption as the Rate-D tennining Step 678
B Reaction within the Adsorbed Film as I,lie Rate-Determining
Step 680
7 Influence of the Adsorption Isotherm 011 the- Kinetics of Hetero
geneous Catalysis 682
A Unimolecular Surface Reactions 683
B Bimolecular Surface Reactions 685
C Effect of Isotherm Complexities 686
8 Mechanisms of a Few Catalyzed Reactions 686
A Ammonia Synthesis 686
B Fisclier-Tropsch Type React,ions 688
C Hydrogenation of Ethylene 690
ID Catalytic Cracking of Hydrocarbons and Related Reactions 691
9 Problems 692
XX CONTENTS
V
General References 594
Textual References 094
Author Index 69!)
Subject Index 721
|
| any_adam_object | 1 |
| author | Adamson, Arthur W. |
| author_facet | Adamson, Arthur W. |
| author_role | aut |
| author_sort | Adamson, Arthur W. |
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| building | Verbundindex |
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| ctrlnum | (OCoLC)250140023 (DE-599)BVBBV001930494 |
| dewey-full | 541/.3453 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541/.3453 |
| dewey-search | 541/.3453 |
| dewey-sort | 3541 43453 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik Chemie |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV001930494 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:37:25Z |
| institution | BVB |
| isbn | 0470007931 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-001258291 |
| oclc_num | 250140023 |
| open_access_boolean | |
| owner | DE-355 DE-BY-UBR DE-210 DE-11 DE-188 |
| owner_facet | DE-355 DE-BY-UBR DE-210 DE-11 DE-188 |
| physical | XX, 747 S. Ill., graph. Darst. |
| publishDate | 1967 |
| publishDateSearch | 1967 |
| publishDateSort | 1967 |
| publisher | Interscience Publ. |
| record_format | marc |
| spelling | Adamson, Arthur W. Verfasser aut Physical chemistry of surfaces Arthur W. Adamson 2. ed. New York Interscience Publ. 1967 XX, 747 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Chimie physique et théorique Chemistry, Physical Chemistry, Physical and theoretical Surface Properties Surface chemistry Oberflächenphysik (DE-588)4134881-3 gnd rswk-swf Oberflächenchemie (DE-588)4126166-5 gnd rswk-swf Physikalische Chemie (DE-588)4045959-7 gnd rswk-swf Oberfläche (DE-588)4042907-6 gnd rswk-swf Oberflächenchemie (DE-588)4126166-5 s DE-604 Oberflächenphysik (DE-588)4134881-3 s Oberfläche (DE-588)4042907-6 s Physikalische Chemie (DE-588)4045959-7 s 1\p DE-604 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001258291&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Adamson, Arthur W. Physical chemistry of surfaces Chimie physique et théorique Chemistry, Physical Chemistry, Physical and theoretical Surface Properties Surface chemistry Oberflächenphysik (DE-588)4134881-3 gnd Oberflächenchemie (DE-588)4126166-5 gnd Physikalische Chemie (DE-588)4045959-7 gnd Oberfläche (DE-588)4042907-6 gnd |
| subject_GND | (DE-588)4134881-3 (DE-588)4126166-5 (DE-588)4045959-7 (DE-588)4042907-6 |
| title | Physical chemistry of surfaces |
| title_auth | Physical chemistry of surfaces |
| title_exact_search | Physical chemistry of surfaces |
| title_full | Physical chemistry of surfaces Arthur W. Adamson |
| title_fullStr | Physical chemistry of surfaces Arthur W. Adamson |
| title_full_unstemmed | Physical chemistry of surfaces Arthur W. Adamson |
| title_short | Physical chemistry of surfaces |
| title_sort | physical chemistry of surfaces |
| topic | Chimie physique et théorique Chemistry, Physical Chemistry, Physical and theoretical Surface Properties Surface chemistry Oberflächenphysik (DE-588)4134881-3 gnd Oberflächenchemie (DE-588)4126166-5 gnd Physikalische Chemie (DE-588)4045959-7 gnd Oberfläche (DE-588)4042907-6 gnd |
| topic_facet | Chimie physique et théorique Chemistry, Physical Chemistry, Physical and theoretical Surface Properties Surface chemistry Oberflächenphysik Oberflächenchemie Physikalische Chemie Oberfläche |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=001258291&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT adamsonarthurw physicalchemistryofsurfaces |