Chlorine, bromine and iodine NMR: Physico-chemical and biological applications
Gespeichert in:
| Hauptverfasser: | , |
|---|---|
| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Berlin [u.a.]
Springer
1976
|
| Schriftenreihe: | NMR.
12. |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIII, 368 S. graph. Darst. |
| ISBN: | 3540077251 0387077251 |
Internformat
MARC
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| 245 | 1 | 0 | |a Chlorine, bromine and iodine NMR |b Physico-chemical and biological applications |c Björn Lindman ; Sture Forsén |
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Datensatz im Suchindex
| _version_ | 1804115380079165440 |
|---|---|
| adam_text | Titel: Chlorine, bromine and iodine NMR
Autor: Lindman, Björn
Jahr: 1976
Table
of
Contents
1.
Introductory
Aspects.................
1.1
General
Properties
of
Halogens...
1.2
Static
Parameters................
1.2.1
Quadrupole
Splittings......
1.2.2
Nuclear
Shielding..........
1.2.3
Spin-Spin
Couplings........
1.3
Dynamic
Parameters...............
1.3.1
Quadrupolar
Relaxation.....
1.3.2
Other
Relaxation
Mechanisms
1.4
Chemical
Exchange
Effects........
1.5
Experimental
Aspects
2.
Relaxation
in
Molecules
or
Ions
With
Covalently
Bonded
Halogens..
2.1
Quadrupole
Relaxation........................................
2.1.1
General
Aspects........................................
2.1.2
On
the
Evaluation
of
the
Correlation
Time..............
2.1.3
Models
for
Molecular
Rotation
in
Liquids...............
2.1.4
Survey
of
Experimental
Results
and
Their
Interpretation
2.2
Other
Relaxation
Mechanisms..................................
3.
Shielding
Effects
in
Covalent
Halogen
Compounds....................
3.1
Theoretical
Aspects............................................
3.1.1
General
Considerations...................................
3.1.2
Approximate
Calculations
of
Nuclear
Shielding............
3.1.3
Correlations
Between
Electronic
Shielding
and
Quadrupolar
Coupling
Constants.......................................
3.1.4
Halide
Ion
Shielding
in
Crystals
and
Aqueous
Solutions...
3.2
Experimental
Data..............................................
3.3
Medium
Effects
on
Halogen
Shielding
Constants..................
3.3.1
General
Considerations...................................
3.3.2
Medium
Effects
on
Chlorine
Shielding
Values..............
4.
Scalar
Spin
Couplings...............................
4.1
General
Considerations..........................
4.2
Experimental
Data
on
Cl,
Br
and
I
Spin
Couplings
1
1
5
5
9
10
12
12
13
16
18
22
22
22
26
28
32
59
60
60
60
63
69
72
72
80
80
83
85
85
90
XII
Table
of
Contents
5.
Relaxation
of
Chloride,
Bromide
and
Iodide
Ions............................
103
5.
1
Quadrupole
Relaxation..................................................
103
5.1.1
General
Aspects..................................................
103
5.1.2
Halide
Ion
Quadrupole
Relaxation
in
Infinitely
Dilute
Aqueous
Solutions........................................................
106
5.
1.2.1
Experimental
Results.....................................
106
5.1.2.2
Electrostatic
Model......................................
108
5.1.2.3
Electronic
Distortion
Model..............................
112
5.1.3
Aqueous
Solutions
of
Alkali
Halides..............................
115
5.1.3.
1
Experimental
Concentration
Dependences...................
115
5.
1.3.2
Electrostatic
Model......................................
120
5.
1.3.3
Electronic
Distortion
Model..............................
125
5.
1.3.4
Water
Isotope
Effect.....................................
128
5.
1.3.5
Mixed
Alkali
Halide
Solutions............................
129
5.
1.3.6
Temperature
Dependence...................................
130
5.1.4
Aqueous
Solutions
of
Other
Inorganic
Halides.....................
135
5.
1.4.1
Hydrogen
Halides.........................................
135
5.1.4.2
Ammonium
Halides.........................................
135
5.1.4.3
Alkaline
Earth
Halides...................................
136
5.1.4.4
Other
Metal
Halides......................................
137
5.1.5
Aqueous
Solutions
Containing
Small
Hydrophobic
Ions
or
Molecules.
140
5.1.6
Halide
Ions
in
Surfactant
Systems................................
146
5.1.7
Halide
Ions
in
Mixed
Solvent
and
Non-Aqueous
Solutions...........
156
5.2
Relaxation
Rates
and
Chemical
Shifts
in
Paramagnetic
Systems...........
162
5.2.1
General
Comments....................
162
5.2.2
Experimental
Studies.............................................
164
5.3
Chemical
Exchange
of
Halide
Ions.......................................
168
5.3.1
General
Considerations...........................................
168
5.3.2
Effects
of
Different
Isotopes....................................
174
5.3.3
Exchange
Rates
Accessible
for
Study..............................
177
5.3.4
Ligand
Exchange
Mechanisms
in
Inorganic
Halide
Complexes.........
178
5.3.5
Experimental
Studies
of
Halide
Ion
Exchange:
Systems
Involving
Halogen
Molecules................................................
180
5.3.6
Experimental
Studies
of
Halide
Ion
Exchange:
Metal-Halide
Com¬
plexes...........................................................
188
6.
Shielding
of
Halide
Ions...................................................
204
6.1
Absolute
Shielding
Values
of
Ions
in
Aqueous
Solutions.................
204
6.1.1
Theoretical
Calculations
of
Shieldings
in
Alkali
Halide
Crystals.
205
6.1.2
Estimates
of
Absolute
Ion
Shieldings
from
Relaxation
Rates
and
Solvent
Isotope
Shifts...........................................
211
6.1.3
Molecular
Beam
and
Atomic
Beam
Data..............................
213
6.1.4
Discussion
of
the
Absolute
Shielding
Values
in
Table
6.1.........
213
6.2
Shielding
in
Aqueous
Alkali
Halide
Solutions...........................
214
6.3
Shielding
in
Other
Aqueous
Solutions...................................
222
6.4
Shielding
in
Mixed
Solvent
and
Non-Aqueous
Solution....................
225
6.5
Water
Solvent
Isotope
Effect
on
Shielding..............................
229
7.
Quadrupole
Splittings
in
Liquid
Crystals...................................
233
7.1
General
Aspects
on
Static
Quadrupole
Effects
of
Mesomorphous
Systems...
233
7.2
Halogen
Quadrupole
Splittings
of
Covalent
Compounds
in
Liquid
Crystals.
240
7.3
Quadrupole
Splittings
of
Halide
Ions
in
Amphiphilic
Mesophases...:.....
242
Table
of
Contents
XIII
8.
Halide
Ions
in
Biological
Systems.........................................
249
8.1
General
Principles......................................•.............
249
8.1.1
Introduction...................................................
249
8.1.2
Quadrupolar
Relaxation
of
I
=
3/2
Nuclei.......................
250
8.1.3
Chemical
Exchange
of
a
Spin
I
=
3/2
Nucleus....................
252
8.1.4
The
Influence
of
Chemical
Exchange
on
the
Correlation
Time
x
c
..
256
8.1.5
Effects
of
Internal
Motion
at
the
Macromolecular
Binding
Site..
258
8.1.6
Halide
Exchange
in
Multi-Site
Systems..........................
259
8.1.7
General
Types
of
Biological
Halide
NMR
Studies
and
Parameters
Attainable.....................................................
262
8.1.8
Evaluation
of
Rate
Parameters.............
263
8.1.9
Determination
of
Binding
Constants
and
Related
Parameters......
265
8.1.10
Competition
Experiments
Between
Different
Ligands..............
271
8.1.11
Evaluation
of
Rotational
Correlation
Times.....................
273
8.2
Small
Molecules
or
Ions
of
Biological
Interest........................
276
8.3
Polypeptides........................
281
8.4
Proteins..................................,...........................
286
8.4.1
Carbonic
Anhydrase.................
286
8.4.2
Alcohol
Dehydrogenase..........................................
290
8.4.3
Alkaline
Phosphatase...........................................
295
8.4.4
Serum
Albumin..................................................
298
8.4.5
Hemoglobin.....................................................
304
8.4.6
Other
Proteins.................................................
315
8.5
Miscellaneous
Systems.................................................
324
9.
Studies
of
the
Perchlorate
Ion............................................
326
9.1
Introduction..........................................................
326
9.2
Shielding.............................................................
327
9.3
Quadrupole
Effects....................................................
329
10.
Recent
Work...............................................................
338
11.
References................................................................
344
12.
Subject
Index.............................................................
360
|
| any_adam_object | 1 |
| author | Lindman, Björn Forsén, Sture |
| author_facet | Lindman, Björn Forsén, Sture |
| author_role | aut aut |
| author_sort | Lindman, Björn |
| author_variant | b l bl s f sf |
| building | Verbundindex |
| bvnumber | BV000949954 |
| callnumber-first | Q - Science |
| callnumber-label | QC490 |
| callnumber-raw | QC490 |
| callnumber-search | QC490 |
| callnumber-sort | QC 3490 |
| callnumber-subject | QC - Physics |
| classification_rvk | UM 3500 VG 9500 |
| ctrlnum | (OCoLC)2373457 (DE-599)BVBBV000949954 |
| dewey-full | 538.3 546/.73 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 538 - Magnetism 546 - Inorganic chemistry |
| dewey-raw | 538.3 546/.73 |
| dewey-search | 538.3 546/.73 |
| dewey-sort | 3538.3 |
| dewey-tens | 530 - Physics 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Physik |
| format | Book |
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| id | DE-604.BV000949954 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:21:41Z |
| institution | BVB |
| isbn | 3540077251 0387077251 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000579636 |
| oclc_num | 2373457 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-91G DE-BY-TUM DE-703 DE-355 DE-BY-UBR DE-20 DE-83 DE-188 |
| owner_facet | DE-19 DE-BY-UBM DE-91G DE-BY-TUM DE-703 DE-355 DE-BY-UBR DE-20 DE-83 DE-188 |
| physical | XIII, 368 S. graph. Darst. |
| psigel | TUB-nveb |
| publishDate | 1976 |
| publishDateSearch | 1976 |
| publishDateSort | 1976 |
| publisher | Springer |
| record_format | marc |
| series | NMR. |
| series2 | NMR. |
| spelling | Lindman, Björn Verfasser aut Chlorine, bromine and iodine NMR Physico-chemical and biological applications Björn Lindman ; Sture Forsén Berlin [u.a.] Springer 1976 XIII, 368 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier NMR. 12. Halogens Spectra Nuclear magnetic resonance spectroscopy Chlorisotop (DE-588)4147795-9 gnd rswk-swf Iodisotop (DE-588)4162277-7 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 gnd rswk-swf Bromisotop (DE-588)4146647-0 gnd rswk-swf Iod (DE-588)4162271-6 gnd rswk-swf Brom (DE-588)4146635-4 gnd rswk-swf Chlor (DE-588)4147748-0 gnd rswk-swf NMR-Spektroskopie (DE-588)4075421-2 s Iodisotop (DE-588)4162277-7 s DE-604 Bromisotop (DE-588)4146647-0 s Chlorisotop (DE-588)4147795-9 s Iod (DE-588)4162271-6 s Brom (DE-588)4146635-4 s Chlor (DE-588)4147748-0 s Forsén, Sture Verfasser aut NMR. 12. (DE-604)BV002321940 12. HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000579636&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lindman, Björn Forsén, Sture Chlorine, bromine and iodine NMR Physico-chemical and biological applications NMR. Halogens Spectra Nuclear magnetic resonance spectroscopy Chlorisotop (DE-588)4147795-9 gnd Iodisotop (DE-588)4162277-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Bromisotop (DE-588)4146647-0 gnd Iod (DE-588)4162271-6 gnd Brom (DE-588)4146635-4 gnd Chlor (DE-588)4147748-0 gnd |
| subject_GND | (DE-588)4147795-9 (DE-588)4162277-7 (DE-588)4075421-2 (DE-588)4146647-0 (DE-588)4162271-6 (DE-588)4146635-4 (DE-588)4147748-0 |
| title | Chlorine, bromine and iodine NMR Physico-chemical and biological applications |
| title_auth | Chlorine, bromine and iodine NMR Physico-chemical and biological applications |
| title_exact_search | Chlorine, bromine and iodine NMR Physico-chemical and biological applications |
| title_full | Chlorine, bromine and iodine NMR Physico-chemical and biological applications Björn Lindman ; Sture Forsén |
| title_fullStr | Chlorine, bromine and iodine NMR Physico-chemical and biological applications Björn Lindman ; Sture Forsén |
| title_full_unstemmed | Chlorine, bromine and iodine NMR Physico-chemical and biological applications Björn Lindman ; Sture Forsén |
| title_short | Chlorine, bromine and iodine NMR |
| title_sort | chlorine bromine and iodine nmr physico chemical and biological applications |
| title_sub | Physico-chemical and biological applications |
| topic | Halogens Spectra Nuclear magnetic resonance spectroscopy Chlorisotop (DE-588)4147795-9 gnd Iodisotop (DE-588)4162277-7 gnd NMR-Spektroskopie (DE-588)4075421-2 gnd Bromisotop (DE-588)4146647-0 gnd Iod (DE-588)4162271-6 gnd Brom (DE-588)4146635-4 gnd Chlor (DE-588)4147748-0 gnd |
| topic_facet | Halogens Spectra Nuclear magnetic resonance spectroscopy Chlorisotop Iodisotop NMR-Spektroskopie Bromisotop Iod Brom Chlor |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000579636&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV002321940 |
| work_keys_str_mv | AT lindmanbjorn chlorinebromineandiodinenmrphysicochemicalandbiologicalapplications AT forsensture chlorinebromineandiodinenmrphysicochemicalandbiologicalapplications |