Chemical microscopy:
Gespeichert in:
| Hauptverfasser: | , , , |
|---|---|
| Format: | Buch |
| Sprache: | English German |
| Veröffentlicht: |
Amsterdam [u.a.]
Elsevier
1982
|
| Schriftenreihe: | Wilson and Wilson's Comprehensive analytical chemistry
16 |
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 513 S. Ill., graph. Darst. |
| ISBN: | 0444419500 |
Internformat
MARC
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| 003 | DE-604 | ||
| 005 | 20150728 | ||
| 007 | t | ||
| 008 | 890313s1982 ad|| |||| 00||| eng d | ||
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| 100 | 1 | |a Emons, Hans-Heinz |d 1930- |e Verfasser |0 (DE-588)1011452219 |4 aut | |
| 240 | 1 | 0 | |a Chemische Mikroskopie |
| 245 | 1 | 0 | |a Chemical microscopy |c [by H.-H. Emons ; H. Keune ; H.-H. Seyfarth] |
| 264 | 1 | |a Amsterdam [u.a.] |b Elsevier |c 1982 | |
| 300 | |a 513 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Wilson and Wilson's Comprehensive analytical chemistry |v 16 | |
| 650 | 4 | |a Chimie analytique | |
| 650 | 7 | |a Chimie analytique |2 ram | |
| 650 | 7 | |a Composés organiques |2 ram | |
| 650 | 4 | |a Microscopie chimique | |
| 650 | 4 | |a Chemical microscopy | |
| 650 | 4 | |a Chemistry, Organic | |
| 650 | 4 | |a Hot stage microscopes | |
| 700 | 1 | |a Keune, Hans |d 1923-2000 |e Verfasser |0 (DE-588)141830999 |4 aut | |
| 700 | 1 | |a Seyfarth, Hans H. |e Verfasser |4 aut | |
| 700 | 1 | 2 | |a Kuhnert-Brandstätter, Maria |d 1919-2011 |0 (DE-588)12251551X |4 aut |t Thermomicroscopy of organic compounds |
| 830 | 0 | |a Wilson and Wilson's Comprehensive analytical chemistry |v 16 |w (DE-604)BV000900805 |9 16 | |
| 856 | 4 | 2 | |m HEBIS Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000560455&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-000560455 | ||
| 249 | |a Thermomicroscopy of organic compounds |v [by Maria Kuhnert-Brandstätter] | ||
Datensatz im Suchindex
| _version_ | 1804115346688311296 |
|---|---|
| adam_text | Wilson and Wilson s
COMPREHENSIVE
ANALYTICAL
CHEMISTRY
Edited by
G SVEHLA, PH D,D SC ,FRSC
Reader in Analytical Chemistry
The Queen s University of Belfast
VOLUME XVI
Chemical Microscopy
Thermomicroscopy of Organic Compounds
ELSEVIER SCIENTIFIC PUBLISHING COMPANY
AMSTERDAM OXFORD NEW YORK
Contents
Glossary of selected microscopical terms 9
1 Introduction 13
2 Crystal optics of visible light 16
2 1 Passage of light through amorphous solids 16
2 2 Passage of light through crystalline solids 17
2 3 Observation by polarized light 20
231 Orthoscopic path of rays 20
232 Conoscopic path of rays 22
References 28
3 Microscopical equipment 30
3 1 Development and characteristics 30
3 2 Equipment for phase and interference microscopy 33
321 Equipment for phase microscopy (transmitted light) 33
322 Equipment for interference microscopy (transmitted light) 34
3 3 Equipment for varying the direction of transmission through the
specimen 37
331 The universal stage 37
332 The spindle stage 39
333 The Waldmann sphere 39
334 The goniomicroscope 40
3 4 Cold and hot stages 41
341 The cold stage 41
342 The hot stage 42
3 5 Other special-purpose microscopes and accessories 45
3 6 Light microscopy combined with other methods of measurement 48
3 7 Refractometers for microscopy 50
References 51
4 Sampling, pre-preparation and preparation of specimens 58
4 1 Sampling 58
4 2 Pre-preparation of specimens • 60
421 Substances durable in dry state 60
422 Substances of limited stability 66
4 3 Preparation of specimens 68
431 Static microscopy 68
432 Kinematic microscopy 81
References 88
5 Image recording and image analysis 91
5 1 Image recording 91
511 Photomicrography 91
512 Cinemicrography 94
513 Video techniques x 97
5 2 Image analysis 98
521 Visual image analysis 98
522 Automatic image analysis 98
5221 Differential automatic image analysis 100
5222 Integrating automatic image analysis 101
References 105
6 t Microscopical measurement of physical properties 107
6 1 Optical properties 107
611 Refractivity 107
6111 Becke line measurement 109
6112 Phase contrast measurement 121
6113 Universal stage measurements 123
6114 Special methods to determine rcfractive indices
612 Birefringence 130
613 Optic axial angle 138
6131 Estimation from isogyre curvature 139
6132 Measurement in special section planes 140
6133 Measurement with the universal stage 143
6134 Computation from the three principal refractive indices 147
6135 Optic axial dispersion 148
614 Optic sign 150
615 Extinction and extinction angle 151
616 Absorption and pleochroism 153
617 Other optical properties 156
6 2 Morphological properties 156
621 Grain, shape 158
622 Grain size and thickness 16 0
623 Surface 164
6 3 Volume and distribution analysis 166
631 Point counter (counting at constant in tervals) 166
632 Counting with no constant intervals 167
633 Errors of microscopical volume analysis 171
6 4 Thermal methods 174
641 Polymorphous inversion 174
642 Temperature of decomposition 176
643 Fusion temperature (melting point) ( 176
644 Examination of »solid-liquid« systems 179
6441 The temperature behaviour of graded mixtures 180
6442 Contact method 180
645 Microsublimation 184
646 Thermometry with the microscope 185
6 5 Ultramicroanalysis 186
6 6 Other physical properties 196
661 Solubility and etching behaviour 196
662 Microhardness 200
663 Cleavage, twinning, density, conductivity 201
References 203
7 Application examples 212
t
7 1 Phase analysis 218
711 Phase analysis by refractive index measurements 225
712 Determining fractions of different origin in a specimen , 230
713 Analysis of secondary and trace constituents 230
714 Special requirements for phase analyses of hygroscopic
and decomposing substances 238
715 Phase analysis in processes 240
7 2 Microstructure analysis 240
721 Structural interpretation of the optical indicatrix 242
722 Mixed* crystals 246
723 Real structure 249
724 Polymer structures 250
725 Disperse systems of submicroscopic particles
(imbibition method) 253
7 3 Phase transformations 257
731 Polymorphic transformation 257
732 Solid-state reactions 259
7321 Solid-solid reactions 259
7322 Decomposition reactions 259
733 Phase transformations via the liquid phase 268
734 Solid-liquid phase transitions 270
7341 Melting and solidification processes 270
7342 Dissolution processes 270
7343 Crystallization processes 272
7 4 Grain structure of aggregates 277
741 Orientation distribution 278
742 Phase distribution 279
743 Type of intergrowth 280
744 Textures 281
745 Special requirements for fabric analysis of decomposing
substances; measurement at high and low temperatures 1 287
References 288
8 Future trends in chemical microscopy 298
8 1 Standardization of measuring techniques, and automation
of data acquisition 298
8 2 Development in kinematic microscopy 299
8 3 Analysis of decomposing substances; measurement at high
and low temperatures 299
8 4 Higher accuracy and expanded possibilities of measurement 300
i
Annex Illustrations for main text 301
I
|
| any_adam_object | 1 |
| author | Emons, Hans-Heinz 1930- Keune, Hans 1923-2000 Seyfarth, Hans H. Kuhnert-Brandstätter, Maria 1919-2011 |
| author_GND | (DE-588)1011452219 (DE-588)141830999 (DE-588)12251551X |
| author_facet | Emons, Hans-Heinz 1930- Keune, Hans 1923-2000 Seyfarth, Hans H. Kuhnert-Brandstätter, Maria 1919-2011 |
| author_role | aut aut aut aut |
| author_sort | Emons, Hans-Heinz 1930- |
| author_variant | h h e hhe h k hk h h s hh hhs m k b mkb |
| building | Verbundindex |
| bvnumber | BV000908912 |
| callnumber-first | Q - Science |
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| callnumber-subject | QD - Chemistry |
| ctrlnum | (OCoLC)8917256 (DE-599)BVBBV000908912 |
| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV000908912 |
| illustrated | Illustrated |
| indexdate | 2024-07-09T15:21:09Z |
| institution | BVB |
| isbn | 0444419500 |
| language | English German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-000560455 |
| oclc_num | 8917256 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-188 |
| owner_facet | DE-19 DE-BY-UBM DE-188 |
| physical | 513 S. Ill., graph. Darst. |
| publishDate | 1982 |
| publishDateSearch | 1982 |
| publishDateSort | 1982 |
| publisher | Elsevier |
| record_format | marc |
| series | Wilson and Wilson's Comprehensive analytical chemistry |
| series2 | Wilson and Wilson's Comprehensive analytical chemistry |
| spelling | Emons, Hans-Heinz 1930- Verfasser (DE-588)1011452219 aut Chemische Mikroskopie Chemical microscopy [by H.-H. Emons ; H. Keune ; H.-H. Seyfarth] Amsterdam [u.a.] Elsevier 1982 513 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Wilson and Wilson's Comprehensive analytical chemistry 16 Chimie analytique Chimie analytique ram Composés organiques ram Microscopie chimique Chemical microscopy Chemistry, Organic Hot stage microscopes Keune, Hans 1923-2000 Verfasser (DE-588)141830999 aut Seyfarth, Hans H. Verfasser aut Kuhnert-Brandstätter, Maria 1919-2011 (DE-588)12251551X aut Thermomicroscopy of organic compounds Wilson and Wilson's Comprehensive analytical chemistry 16 (DE-604)BV000900805 16 HEBIS Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000560455&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Thermomicroscopy of organic compounds [by Maria Kuhnert-Brandstätter] |
| spellingShingle | Emons, Hans-Heinz 1930- Keune, Hans 1923-2000 Seyfarth, Hans H. Kuhnert-Brandstätter, Maria 1919-2011 Chemical microscopy Wilson and Wilson's Comprehensive analytical chemistry Chimie analytique Chimie analytique ram Composés organiques ram Microscopie chimique Chemical microscopy Chemistry, Organic Hot stage microscopes |
| title | Chemical microscopy |
| title_alt | Chemische Mikroskopie Thermomicroscopy of organic compounds |
| title_auth | Chemical microscopy |
| title_exact_search | Chemical microscopy |
| title_full | Chemical microscopy [by H.-H. Emons ; H. Keune ; H.-H. Seyfarth] |
| title_fullStr | Chemical microscopy [by H.-H. Emons ; H. Keune ; H.-H. Seyfarth] |
| title_full_unstemmed | Chemical microscopy [by H.-H. Emons ; H. Keune ; H.-H. Seyfarth] |
| title_short | Chemical microscopy |
| title_sort | chemical microscopy |
| topic | Chimie analytique Chimie analytique ram Composés organiques ram Microscopie chimique Chemical microscopy Chemistry, Organic Hot stage microscopes |
| topic_facet | Chimie analytique Composés organiques Microscopie chimique Chemical microscopy Chemistry, Organic Hot stage microscopes |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000560455&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV000900805 |
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