Plasma chromatography:
Gespeichert in:
| Format: | Buch |
|---|---|
| Sprache: | English |
| Veröffentlicht: |
New York u.a.
Plenum Pr.
1984
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | XIII, 259 S. Ill. |
| ISBN: | 0306414325 |
Internformat
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| 245 | 1 | 0 | |a Plasma chromatography |c ed. by Timothy W. Carr |
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| 650 | 4 | |a Chromatography | |
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Datensatz im Suchindex
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| adam_text | PLASMA CHROMATOGRAPHY EDITED BY TIMOTHY W. CARR IBM CORPORATION HOPEWELL
JUNCTION, NEW YORK PLENUM PRESS * NEW YORK AND LONDON CONTENTS 1.
INSTRUMENT DESIGN AND DESCRIPTION G. E. SPANGLER AND M. J. COHEN 1.
INTRODUCTION 1 2. EQUIPMENT DESCRIPTION 3 3. PERFORMANCE DESCRIPTION 9
3.1. GENERATION OF NEGATIVE SAMPLE IONS 9 3.2. ION EXTRACTION AND
SHUTTER GRID OPERATION 11 3.3. SEPARATION OF IONS BY MOBILITY 13 3.4.
GENERATION OF THE ION MOBILITY SPECTRUM (ION ARRIVAL TIME SPECTRUM)....
14 4. SPECTRAL INTERPRETATION 15 4.1. ION MOBILITY 15 4.2. REACTION
CHEMISTRY 17 5. THEORETICAL DESCRIPTION 19 5.1. REACTORTHEORY 19 5.2.
DRIFT THEORY 24 6. SAMPLE HANDLING 27 6.1. SAMPLE WIRE PROBE 28 6.2.
SYRINGE INJECTION 29 6.3. EXPONENTIAL DILUTION FLASK 30 6.4. CALIBRATED
STANDARD GENERATORS 31 6.5. INLET OVEN 31 6.6. AMBIENT AIR SAMPLING 31
7. PLASMA CHROMATOGRAPHY AS A GC PEAK IDENTIFIER 32 7.1. BACKGROUND OF
PC 34 7.2. PURE SAMPLE INTO PC 34 7.3. BACKGROUND OF GC 34 7.4. SAMPLE
INJECTION*FID RESPONSE 35 7.5. PC RESPONSE 36 8. PLASMA CHROMATOGRAPHY
AND MASS SPECTROMETRY 37 REFERENCES 39 2. ION MOBILITY: ITS ROLE IN
PLASMA CHROMATOGRAPHY E. A. MASON 1. INTRODUCTION 43 2. KINETIC THEORY
OF ION TRANSPORT 46 IX X CONTENTS 2.1. SUMMARY OF MAIN RESULTS 46 2.2.
ELEMENTARY DERIVATIONS 52 2.3. ION-MOLECULE FORCES AND MOBILITY 57 2.4.
INELASTIC COUISIONS AND NONSPHERICAL ION-MOLECULE INTERACTIONS 68 3.
APPLICATIONS TO PLASMA CHROMATOGRAPHY 69 3.1. CONSISTENCY WITH
DRIFT-TUBE DATA 69 3.2. COMPARISON WITH POLARIZATION LIMIT 69 3.3.
VARIATION OF ELECTRIC FIELD STRENGTH AND DRIFT-GAS PRESSURE 73 3.4.
VARIATION OF DRIFT GAS 73 3.5. MULTIPLY-CHARGED IONS 77 3.6.
MASS-MOBILITY CORRELATION 80 3.7. CORRELATION WITH VAPOR DIFFUSION
COEFFICIENTS 83 3.8. PULSE WIDTH AND SHAPE 84 3.9. ION-MOLECULE
REACTIONS IN THE DRIFT REGION 87 4. CONCLUDING REMARKS 89 REFERENCES 90
3. ATMOSPHERIC PRESSURE LONIZATION M. W. SIEGEL 1. INTRODUCTION 95 2.
RATE EQUATIONS DESCRIBING API 96 2.1. REAGENT ION PRODUCTION 97 2.2.
SAMPLE ION PRODUCTION 99 2.3. SAMPLE MOLECULE DEPLETION 100 2.4. SUMMARY
OF PROCESSES 102 3. APPLICATION OF RATE EQUATIONS TO A 63 NI API SOURCE
102 3.1. PRIMARY LONIZATION 102 3.2. DIFFUSION 102 3.3. RECOMBINATION
103 3.4. REAGENT ION DENSITY 103 3.5. SAMPLE ION DENSITY 104 3.6. SAMPLE
ION CURRENT 105 3.7. FLOW RATE OPTIMIZATION 105 3.8. SOURCE RADIUS
OPTIMIZATION 108 3.9. MEANING OF SMALL SAMPLE LIMIT 108 3.10. SAMPLE
QUANTITY VS. SAMPLE CONCENTRATION 109 4. SUMMARY, CONCLUSIONS, AND
THOUGHTS ON FUTURE WORK 110 NOTATION 110 REFERENCES AND NOTES 112 4.
CHARACTERIZATION OF ISOMERS BY PLASMA CHROMATOGRAPHY D. F. HAGEN 1.
INTRODUCTION 115 2. SAMPLING REQUIREMENTS AND DATA ACQUISITION 116
CONTENTS XI 2. 1. SAMPLING INTERFACES 116 2.2. SAMPLE SIZE*REACTANT ION
LEVEL 118 2.3. DERIVATIVE STABILIZATION 119 2.4. TIMING FACTORS 120 3.
MOLECULAR ION CHARACTERISTICS 121 3.1. ION BEHAVIOR 121 3.2.
REARRANGEMENTS OF MOLECULAR IONS 124 3.3. ION MOLECULE, SIZE-MASS
RELATIONSHIPS 126 4. AROMATIC POSITIONAL ISOMERS 131 4.1. SUBSTITUTED
TOLUENES AND CHLOROBENZOATE ESTER HOMOLOGS 131 4.2. PHTHALATE ESTER
HOMOLOGS 132 4.3. TRISUBSTITUTED BENZENE ISOMERE 133 4.4. ISOMERIC
PERFLUIDONES AND METHOXYPERFLUIDONES 134 4.5. BRANCHED CHAIN ISOMERS 135
5. CIS-TRANS ISOMERS 135 6. POLYNUCLEAR AROMATICS 137 7. AROMATIC
NITROGEN COMPOUNDS 138 7.1. DIPYRIDYLS, PHENYL PYRIDINES 138 7.2.
NAPHTHALENE RELATED NITROGEN ISOMERS 139 7.3. PICOLINE-PYRAZINE ISOMERS
140 8. CONCLUDING REMARKS 140 REFERENCES 141 5. PLASMA CHROMATOGRAPHY AS
A GAS CHROMATOGRAPHIE DETECTION METHOD HERBERT H. HILL AND MICHAEL A.
BAIM 1. AMBIENT PRESSURE LONIZATION DETECTORS FOR GAS CHROMATOGRAPHY 144
2. SAMPLE INTRODUCTION 145 3. QUALITATIVE ANALYSIS 148 3.1. MOVING
SECOND GATE METHOD 149 3.2. SINGLE-SCAN METHOD 150 3.3. SIGNAL AVERAGING
METHOD 150 3.4. QUALITATIVE GC DETECTION 150 4. CONTINUOUS MOBILITY
MONITORING 157 5. QUANTITATIVE ANALYSIS 161 5.1. CALIBRATION GRAPHS 161
5.2. PRECISION 162 5.3. ACCURACY 162 6. INTERFERENCES 163 6.1. OVERLOAD
164 6.2. SOLVENT EFFECTS 165 6.3. COLUMN BLEED 166 6.4. MATRIX
INTERFERENCE 168 6.5. RESIDENCE TIME 170 7. A DETECTOR FOR CAPILLARY
CHROMATOGRAPHY 171 REFERENCES 175 XII CONTENTS 6. ANALYSIS OF TOXIC
VAPORS BY PLASMA CHROMATOGRAPHY R. J. DAM 1. THE ROLE OF PLASMA
CHROMATOGRAPHY IN TOXIC GAS MONITORING 177 1.1. INTRODUCTION 177 1.2.
ADVANTAGES OF PLASMA CHROMATOGRAPHY 178 1.3. DISADVANTAGES OF PLASMA
CHROMATOGRAPHY 180 1.4. SELECTING SUITABLE PC MONITORING APPLICATIONS
183 1.5. PC MONITOR DEVELOPMENT PROGRAM AT DU PONT 183 2. PLASMA
CHROMATOGRAPH CALIBRATION 184 2.1. REQUIREMENTS OF A CALIBRATION
TECHNIQUE 184 2.2. BASIC CONCEPTS AND THEORY 185 2.3. CALIBRATION
APPARATUS AND METHODS 189 2.4. CALIBRATION EXAMPLE 193 3. SAMPLING
SYSTEMS 194 3.1. DESIGN GOALS 194 3.2. SYSTEM DESCRIPTION 196 3.3.
MEASURING SYSTEM PERFORMANCE 198 3.4. SYSTEM ENCLOSURE 201 4. INSTRUMENT
CONTROL AND DATA PROCESSING 201 4.1. GENERAL CONSIDERATIONS 201 4.2.
PLASMA CHROMATOGRAPH DATA ACQUISITION 203 4.3. INSTRUMENT CONTROL AND
HARDWARE STATUS MONITORING 204 4.4. SOFTWARE 205 5. TOXIC MONITORING
APPLICATIONS 208 5.1. WORKPLACE CHARACTERIZATION IMPROVED 209 5.2.
INSTRUMENT PROVEN RELIABLE 211 5.3. MAINTENANCE PROCEDURA 212 5.4.
FUTURE WORK 213 REFERENCES 213 7. ANALYSIS OF SEMICONDUCTOR DEVICES AND
MICROELECTRONIC PACKAGES BY PLASMA CHROMATOGRAPHY/MASS SPECTROSCOPY T.
W. CARR 1. INTRODUCTION 215 2. ANALYSIS OF ORGANIC SURFACE CONTAMINANTS
216 2.1. INTRODUCTION 216 2.2. EXPERIMENTAL DISCUSSION 216 2.3.
DISCUSSION OF SURFACE ANALYSIS 219 3. ANALYSIS OF WATER IN SEALED
ELECTRONIC PACKAGES 225 3.1. INTRODUCTION 225 3.2. NEGATIVE ION
MEASUREMENTS 225 3.3. POSITIVE ION MEASUREMENTS 228 4. ANALYSIS OF
HEADSPACE VAPOR OF SEALED PACKAGES 229 5. PLASMA CHROMATOGRAPHY AS A
PROCESS MONITOR 231 6. EXTENSION OF PC/MS TO SMALL-AREA SURFACE ANALYSIS
. 233 CONTENTS * 7. CONCLUSION 234 REFERENCES 234 8. INSTRUMENT DESIGN
AND AUTOMATION ROGER F. WERNLUND 1. INTRODUCTION 237 2. HARDWARE 240
2.1. CENTRAL PROCESSING UNIT (CPU) 240 2.2. PERIPHERALS 242 2.3.
INTERFACING 243 3. SOFTWARE 244 3.1. BASIC DATA ACQUISITION 244 3.2.
BASIC DATA STORAGE AND RETRIEVAL 245 3.3. BASIC DATA REDUCTION 245 3.4.
HIGHER LEVEL COMMAND STRUCTURE 247 SUBJECT INDEX 257 AUTHOR INDEX 257
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| illustrated | Illustrated |
| indexdate | 2024-07-09T15:12:47Z |
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| spelling | Plasma chromatography ed. by Timothy W. Carr New York u.a. Plenum Pr. 1984 XIII, 259 S. Ill. txt rdacontent n rdamedia nc rdacarrier Spectroscopie du plasma Chromatography Ion mobility spectroscopy Plasma chemistry Plasmaspektroskopie (DE-588)4046265-1 gnd rswk-swf (DE-588)4143413-4 Aufsatzsammlung gnd-content Plasmachromatographie gnd rswk-swf Plasmachromatographie f DE-604 Plasmaspektroskopie (DE-588)4046265-1 s Carr, Timothy W. Sonstige oth GBV Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=000219394&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Plasma chromatography Spectroscopie du plasma Chromatography Ion mobility spectroscopy Plasma chemistry Plasmaspektroskopie (DE-588)4046265-1 gnd |
| subject_GND | (DE-588)4046265-1 (DE-588)4143413-4 |
| title | Plasma chromatography |
| title_auth | Plasma chromatography |
| title_exact_search | Plasma chromatography |
| title_full | Plasma chromatography ed. by Timothy W. Carr |
| title_fullStr | Plasma chromatography ed. by Timothy W. Carr |
| title_full_unstemmed | Plasma chromatography ed. by Timothy W. Carr |
| title_short | Plasma chromatography |
| title_sort | plasma chromatography |
| topic | Spectroscopie du plasma Chromatography Ion mobility spectroscopy Plasma chemistry Plasmaspektroskopie (DE-588)4046265-1 gnd |
| topic_facet | Spectroscopie du plasma Chromatography Ion mobility spectroscopy Plasma chemistry Plasmaspektroskopie Aufsatzsammlung Plasmachromatographie |
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