Investigation and assessment of new amines for carbon dioxide capture:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | German |
| Published: |
Kaiserslautern
Technische Universität Kaiserslautern
2022
|
| Series: | Scientific report series
Volume 17 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | XXIV, 117 Seiten Diagramme 21 cm |
| ISBN: | 9783944433165 |
Staff View
MARC
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| 245 | 1 | 0 | |a Investigation and assessment of new amines for carbon dioxide capture |c Dan Vasiliu |
| 264 | 1 | |a Kaiserslautern |b Technische Universität Kaiserslautern |c 2022 | |
| 300 | |a XXIV, 117 Seiten |b Diagramme |c 21 cm | ||
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| 502 | |b Dissertation |c Technische Universität Kaiserslautern |d 2022 | ||
| 650 | 0 | 7 | |a Carbon dioxide capture and utilization |0 (DE-588)1107216192 |2 gnd |9 rswk-swf |
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Record in the Search Index
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|---|---|
| adam_text | CONTENTS
XV
CONTENTS
1
INTRODUCTION
1
2
SHORT-CUT
METHOD
FOR
ASSESSING
SOLVENTS
FOR
GAS
CLEANING
BY
REACTIVE
ABSORPTION
5
2.1
INTRODUCTION
......................................................................................................
5
2.2
NOVA
SHORT-CUT
METHOD
..................................................................................
6
2.2.1
ABSORBER
STEP
....................................................................................
9
2.2.2
DESORBER
STEP
....................................................................................
11
2.2.3
ENERGY
BALANCE
STEP
............................................................................
13
2.3
SOLSOFT
CORRELATION
OF
GAS
SOLUBILITY
DATA
..................................................
14
2.4
RESULTS
AND
DISCUSSION
.....................................................................................
15
2.4.1
APPLICATION
OF
THE
SOLSOFT
EQUATION
.............................................
16
2.4.2
STUDIES
WITH
THE
NOVA
METHOD
.........................................................
17
2.4.3
QREH*,
1*
AND
§*
AS
NEW
CRITERIA
FOR
ASSESSING
SOLVENTS
......................
23
3
THERMODYNAMIC
STUDY
OF
A
COMPLEX
SYSTEM
FOR
CARBON
CAPTURE:
BUTYLTRIACETONEDIAMINE
+
WATER
+
CARBON
DIOXIDE
25
3.1
INTRODUCTION
......................................................................................................
25
3.2
CHEMICAL
SYSTEM
..............................................................................................
27
3.3
CHEMICALS
.........................................................................................................
28
3.4
EXPERIMENTAL
...................................................................................................
29
3.4.1
AMINE
VAPOR
PRESSURE
..........................................................................
29
3.4.2
AMINE
PROTONATION
EQUILIBRIA
............................................................
29
3.4.3
LIQUID-LIQUID
EQUILIBRIA
.......................................................................
29
3.4.4
LIQUID
PHASE
SPECIATION
.......................................................................
30
3.4.5
EXPERIMENTS
WITH
FLOW
SATURATOR
......................................................
30
3.4.6
GAS
SOLUBILITY
BY
SYNTHETIC
METHOD
...................................................
32
3.4.7
GAS
SOLUBILITY
BY
HEADSPACE
GAS
CHROMATOGRAPHY
..........................
32
3.4.8
ANALYSIS
OF
PRECIPITATED
SOLIDS
............................................................
33
3.5
RESULTS
AND
DISCUSSION
.....................................................................................
33
3.5.1
AMINE
VAPOR
PRESSURE
..........................................................................
33
3.5.2
AMINE
PROTONATION
.............................................................................
35
XVI
CONTENTS
3.5.3
LIQUID-LIQUID
EQUILIBRIUM
....................................................................
37
3.5.4
CO2
SOLUBILITY
.....................................................................................
39
3.5.5
ANALYSIS
OF
SOLID
CRYSTALS
....................................................................
45
4
PILOT
PLANT
EXPERIMENTS
47
4.1
INTRODUCTION
.....................................................................................................
47
4.2
SOLVENT
.............................................................................................................
48
4.3
PILOT
PLANT
........................................................................................................
49
4.4
DATA
ACQUISITION
............................................................................................
50
4.5
SPECIFICATIONS
AND
RESULTS
..............................................................................
51
5
CONCLUSIONS
55
LITERATURE
66
APPENDIX
67
A
NOVA
SHORT-CUT
METHOD
67
A.L
FLOWCHART
.........................................................................................................
67
A.2
NUMERICAL
ASPECTS
...........................................................................................
67
A.3
DIFFERENTIABILITY
IN
CASE
CHANGE
POINTS
..........................................................
69
A.4
DISTRIBUTION
OF
ENERGY
TERMS
..........................................................................
71
A.5
RICH
AND
LEAN
LOADINGS
AND
CYCLIC
CAPACITY
..................................................
72
A.6
TOPOLOGY
............................................................................................................
73
B
SOLSOFT
EQUATION
75
B.L
CONVEXITY
OF
SOLSOFT
.....................................................................................
75
B.2
PHYSICO-CHEMICAL
BACKGROUND
OF
SOLSOFT
...................................................
76
B.3
ENTHALPY
OF
ABSORPTION
FROM
SOLSOFT:
WORKING
EQUATIONS
......................
78
B.4
ENTHALPY
OF
ABSORPTION
FROM
(EXTENDED)
SOLSOFT:
MATHEMATICAL
DERIVATION
.........................................................................
79
B.4.1
DIFFERENTIAL
ENTHALPY
OF
ABSORPTION
...................................................
79
B.4.
2
INTEGRAL
ENTHALPY
OF
ABSORPTION
.........................................................
82
B.4.
3
LIMITING
VALUES
AT
INFINITE
DILUTION
...................................................
84
B.5
GAS
SOLUBILITY
BY
SOFT
MODELS
..........................................................................
85
B.6
QUALITY
OF
SOLSOFT
FITS
..................................................................................
86
B.7
EXTENDED
SOLSOFT
EQUATION
..........................................................................
89
C
KINSOFT
EQUATION
93
C.1
EMPIRICAL
CORRELATION
OF
CO
2
LOADING
IN
FLOW
SATURATOR
............................
93
CONTENTS
XVII
D
ANALYSIS
OF
TOTAL
DISSOLVED
CO2
IN
LIQUID
PHASE
95
D.I
GAS
CHROMATOGRAPHIE
METHOD
.......................................................................
95
E
PILOT
PLANT
EXPERIMENTS
99
E.L
OVERVIEW
OF
THE
RESULTS
.................................................................................
99
E.2
DATA
PROCESSING
..................................................................................................
108
E.3
CHARACTERIZATION
OF
FLUID
FLOW
IN
THE
ABSORBER
................................................
109
E.4
UNCERTAINTY
ANALYSIS
..........................................................................................
110
F
SIMULATION
OF
CO
2
CAPTURE
WITH
MEA30
113
F.L
SPECIFICATIONS
.....................................................................................................
113
F.2
RESULTS
.................................................................................................................
115
|
| adam_txt |
CONTENTS
XV
CONTENTS
1
INTRODUCTION
1
2
SHORT-CUT
METHOD
FOR
ASSESSING
SOLVENTS
FOR
GAS
CLEANING
BY
REACTIVE
ABSORPTION
5
2.1
INTRODUCTION
.
5
2.2
NOVA
SHORT-CUT
METHOD
.
6
2.2.1
ABSORBER
STEP
.
9
2.2.2
DESORBER
STEP
.
11
2.2.3
ENERGY
BALANCE
STEP
.
13
2.3
SOLSOFT
CORRELATION
OF
GAS
SOLUBILITY
DATA
.
14
2.4
RESULTS
AND
DISCUSSION
.
15
2.4.1
APPLICATION
OF
THE
SOLSOFT
EQUATION
.
16
2.4.2
STUDIES
WITH
THE
NOVA
METHOD
.
17
2.4.3
QREH*,
1*
AND
§*
AS
NEW
CRITERIA
FOR
ASSESSING
SOLVENTS
.
23
3
THERMODYNAMIC
STUDY
OF
A
COMPLEX
SYSTEM
FOR
CARBON
CAPTURE:
BUTYLTRIACETONEDIAMINE
+
WATER
+
CARBON
DIOXIDE
25
3.1
INTRODUCTION
.
25
3.2
CHEMICAL
SYSTEM
.
27
3.3
CHEMICALS
.
28
3.4
EXPERIMENTAL
.
29
3.4.1
AMINE
VAPOR
PRESSURE
.
29
3.4.2
AMINE
PROTONATION
EQUILIBRIA
.
29
3.4.3
LIQUID-LIQUID
EQUILIBRIA
.
29
3.4.4
LIQUID
PHASE
SPECIATION
.
30
3.4.5
EXPERIMENTS
WITH
FLOW
SATURATOR
.
30
3.4.6
GAS
SOLUBILITY
BY
SYNTHETIC
METHOD
.
32
3.4.7
GAS
SOLUBILITY
BY
HEADSPACE
GAS
CHROMATOGRAPHY
.
32
3.4.8
ANALYSIS
OF
PRECIPITATED
SOLIDS
.
33
3.5
RESULTS
AND
DISCUSSION
.
33
3.5.1
AMINE
VAPOR
PRESSURE
.
33
3.5.2
AMINE
PROTONATION
.
35
XVI
CONTENTS
3.5.3
LIQUID-LIQUID
EQUILIBRIUM
.
37
3.5.4
CO2
SOLUBILITY
.
39
3.5.5
ANALYSIS
OF
SOLID
CRYSTALS
.
45
4
PILOT
PLANT
EXPERIMENTS
47
4.1
INTRODUCTION
.
47
4.2
SOLVENT
.
48
4.3
PILOT
PLANT
.
49
4.4
DATA
ACQUISITION
.
50
4.5
SPECIFICATIONS
AND
RESULTS
.
51
5
CONCLUSIONS
55
LITERATURE
66
APPENDIX
67
A
NOVA
SHORT-CUT
METHOD
67
A.L
FLOWCHART
.
67
A.2
NUMERICAL
ASPECTS
.
67
A.3
DIFFERENTIABILITY
IN
CASE
CHANGE
POINTS
.
69
A.4
DISTRIBUTION
OF
ENERGY
TERMS
.
71
A.5
RICH
AND
LEAN
LOADINGS
AND
CYCLIC
CAPACITY
.
72
A.6
TOPOLOGY
.
73
B
SOLSOFT
EQUATION
75
B.L
CONVEXITY
OF
SOLSOFT
.
75
B.2
PHYSICO-CHEMICAL
BACKGROUND
OF
SOLSOFT
.
76
B.3
ENTHALPY
OF
ABSORPTION
FROM
SOLSOFT:
WORKING
EQUATIONS
.
78
B.4
ENTHALPY
OF
ABSORPTION
FROM
(EXTENDED)
SOLSOFT:
MATHEMATICAL
DERIVATION
.
79
B.4.1
DIFFERENTIAL
ENTHALPY
OF
ABSORPTION
.
79
B.4.
2
INTEGRAL
ENTHALPY
OF
ABSORPTION
.
82
B.4.
3
LIMITING
VALUES
AT
INFINITE
DILUTION
.
84
B.5
GAS
SOLUBILITY
BY
SOFT
MODELS
.
85
B.6
QUALITY
OF
SOLSOFT
FITS
.
86
B.7
EXTENDED
SOLSOFT
EQUATION
.
89
C
KINSOFT
EQUATION
93
C.1
EMPIRICAL
CORRELATION
OF
CO
2
LOADING
IN
FLOW
SATURATOR
.
93
CONTENTS
XVII
D
ANALYSIS
OF
TOTAL
DISSOLVED
CO2
IN
LIQUID
PHASE
95
D.I
GAS
CHROMATOGRAPHIE
METHOD
.
95
E
PILOT
PLANT
EXPERIMENTS
99
E.L
OVERVIEW
OF
THE
RESULTS
.
99
E.2
DATA
PROCESSING
.
108
E.3
CHARACTERIZATION
OF
FLUID
FLOW
IN
THE
ABSORBER
.
109
E.4
UNCERTAINTY
ANALYSIS
.
110
F
SIMULATION
OF
CO
2
CAPTURE
WITH
MEA30
113
F.L
SPECIFICATIONS
.
113
F.2
RESULTS
.
115 |
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| author | Vasiliu, Dan 1982- |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV049352354 |
| illustrated | Not Illustrated |
| index_date | 2024-07-03T22:50:11Z |
| indexdate | 2024-07-10T10:02:21Z |
| institution | BVB |
| isbn | 9783944433165 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-034612675 |
| oclc_num | 1378730546 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | XXIV, 117 Seiten Diagramme 21 cm |
| publishDate | 2022 |
| publishDateSearch | 2022 |
| publishDateSort | 2022 |
| publisher | Technische Universität Kaiserslautern |
| record_format | marc |
| series | Scientific report series |
| series2 | Scientific report series |
| spelling | Vasiliu, Dan 1982- Verfasser (DE-588)1281120359 aut Investigation and assessment of new amines for carbon dioxide capture Dan Vasiliu Kaiserslautern Technische Universität Kaiserslautern 2022 XXIV, 117 Seiten Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Scientific report series Volume 17 Dissertation Technische Universität Kaiserslautern 2022 Carbon dioxide capture and utilization (DE-588)1107216192 gnd rswk-swf Amine (DE-588)4001705-9 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Carbon dioxide capture and utilization (DE-588)1107216192 s Amine (DE-588)4001705-9 s DE-604 Scientific report series Volume 17 (DE-604)BV040983565 17 B:DE-101 application/pdf https://d-nb.info/1280651083/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034612675&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p dnb 20230224 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Vasiliu, Dan 1982- Investigation and assessment of new amines for carbon dioxide capture Scientific report series Carbon dioxide capture and utilization (DE-588)1107216192 gnd Amine (DE-588)4001705-9 gnd |
| subject_GND | (DE-588)1107216192 (DE-588)4001705-9 (DE-588)4113937-9 |
| title | Investigation and assessment of new amines for carbon dioxide capture |
| title_auth | Investigation and assessment of new amines for carbon dioxide capture |
| title_exact_search | Investigation and assessment of new amines for carbon dioxide capture |
| title_exact_search_txtP | Investigation and assessment of new amines for carbon dioxide capture |
| title_full | Investigation and assessment of new amines for carbon dioxide capture Dan Vasiliu |
| title_fullStr | Investigation and assessment of new amines for carbon dioxide capture Dan Vasiliu |
| title_full_unstemmed | Investigation and assessment of new amines for carbon dioxide capture Dan Vasiliu |
| title_short | Investigation and assessment of new amines for carbon dioxide capture |
| title_sort | investigation and assessment of new amines for carbon dioxide capture |
| topic | Carbon dioxide capture and utilization (DE-588)1107216192 gnd Amine (DE-588)4001705-9 gnd |
| topic_facet | Carbon dioxide capture and utilization Amine Hochschulschrift |
| url | https://d-nb.info/1280651083/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034612675&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV040983565 |
| work_keys_str_mv | AT vasiliudan investigationandassessmentofnewaminesforcarbondioxidecapture |
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