Catalysis at surfaces:
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| Main Authors: | , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin ; Boston
De Gruyter
[2023]
|
| Series: | De Gruyter graduate
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XI, 695 Seiten Illustrationen, Diagramme |
| ISBN: | 9783110632477 |
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MARC
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| 015 | |a 23,N13 |2 dnb | ||
| 016 | 7 | |a 1284094111 |2 DE-101 | |
| 020 | |a 9783110632477 |c pbk. |9 978-3-11-063247-7 | ||
| 035 | |a (OCoLC)1395137141 | ||
| 035 | |a (DE-599)DNB1284094111 | ||
| 040 | |a DE-604 |b ger |e rda | ||
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| 084 | |a CHE 180 |2 stub | ||
| 084 | |8 1\p |a 540 |2 23sdnb | ||
| 084 | |a CHE 167 |2 stub | ||
| 100 | 1 | |a Grünert, Wolfgang |d 1949- |e Verfasser |0 (DE-588)142261165 |4 aut | |
| 245 | 1 | 0 | |a Catalysis at surfaces |c Wolfgang Grünert, Wolfgang Kleist, Martin Muhler |
| 264 | 1 | |a Berlin ; Boston |b De Gruyter |c [2023] | |
| 300 | |a XI, 695 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a De Gruyter graduate | |
| 650 | 0 | 7 | |a Katalyse |0 (DE-588)4029921-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Oberflächenreaktion |0 (DE-588)4140095-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Oberflächenchemie |0 (DE-588)4126166-5 |2 gnd |9 rswk-swf |
| 653 | |a Catalysis | ||
| 653 | |a Catalyst | ||
| 653 | |a Heterogene Katalyse | ||
| 653 | |a Heterogeneous Catalysis | ||
| 653 | |a Katalysator | ||
| 653 | |a Katalyse | ||
| 653 | |a Oberflächenchemie | ||
| 653 | |a Surface Chemistry | ||
| 653 | |a TB: Textbook | ||
| 689 | 0 | 0 | |a Katalyse |0 (DE-588)4029921-1 |D s |
| 689 | 0 | 1 | |a Oberflächenreaktion |0 (DE-588)4140095-1 |D s |
| 689 | 0 | 2 | |a Oberflächenchemie |0 (DE-588)4126166-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Kleist, Wolfgang |e Verfasser |0 (DE-588)1072788454 |4 aut | |
| 700 | 1 | |a Muhler, Martin |d 1961- |e Verfasser |0 (DE-588)143495577 |4 aut | |
| 710 | 2 | |a Walter de Gruyter GmbH & Co. KG |0 (DE-588)10095502-2 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-11-063248-4 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-11-063254-5 |
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| 883 | 1 | |8 1\p |a vlb |d 20230322 |q DE-101 |u https://d-nb.info/provenance/plan#vlb | |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-034359316 | |
Record in the Search Index
| _version_ | 1813532429492682752 |
|---|---|
| adam_text |
CONTENTS
PREFACE
-
V
1
1.1
1.2
1.3
1.4
1.4.1
1.4.2
1.4.3
1.5
1.6
INTRODUCTION
-
1
CATALYSIS,
REACTION
RATE,
AND
EQUILIBRIUM
-
1
CATALYST
AND
REACTANT
PHASES
-
2
CATALYSIS
AND
DAILY
LIFE
-
4
BASIC
CONCEPTS
OF
SURFACE
CATALYSIS
-
8
REACTION
RATE
-
8
ACTIVITY,
SELECTIVITY,
AND
STABILITY
-
11
CATALYST
AND
CATALYTIC
PROCESS
-
13
SURFACE
CATALYSIS:
AN
ART
OR
A
SCIENCE?
-
17
CATALYST
RESEARCH:
AN
OVERVIEW
-
23
REFERENCES
-
26
2
2.1
2.2
2.2.1
2.2.2
2.3
2.3.1
2.3.2
2.3.2.1
2.3.2.2
2.3.2.3
2.3.2.4
2.3.2.5
2.3.2.6
2.3.3
2.3.4
2.4
2.4.1
2.4.2
2.4.3
2.4.4
2.5
2.5.1
2.5.2
2.6
2.6.1
SURFACE
CATALYSIS:
THE
SCENE
AND
THE
PLAY
-
28
SOLIDS
-
28
SURFACES
-
38
SURFACE
STRUCTURES
-
38
SURFACE
CHEMISTRY
-
48
PARTICLE
ARCHITECTURE
IN
CATALYTIC
MATERIALS
-
52
SIZE,
POROSITY,
AND
STRUCTURAL
HETEROGENEITY
OF
CATALYST
PARTICLES
-
52
SUPPORTS
FOR
HETEROGENEOUS
CATALYSTS
-
55
SILICA
(SIO
2
)
----
56
ALUMINA
(AI
2
O
3
)
----
57
ALUMOSILICATES/ZEOLITES
----
59
METAL-ORGANIC
FRAMEWORKS
-
67
TITANIA,
ZIRCONIA,
CERIA
-
72
CARBON
MATERIALS
-
75
SUPPORT
AND
SUPPORTED
SPECIES
-
80
ALTERNATIVE
CATALYST
ARCHITECTURES
-
93
ADSORPTION
-
95
ADSORPTION
AND
DESORPTION:
PHENOMENA
AND
CLASSIFICATION
-
95
PHYSISORPTION
AND
CHEMISORPTION
-
97
DESCRIPTION
OF
EQUILIBRIA
IN
GAS-PHASE
ADSORPTION
-
102
DESCRIPTION
OF
EQUILIBRIA
IN
LIQUID-PHASE
ADSORPTION
-
105
SURFACE
REACTIONS
-
106
THERMAL
CATALYSIS
-
106
PHOTOCATALYSIS
-
113
REACTION
MECHANISMS
AND
REACTION
KINETICS
IN
THERMAL
CATALYSIS
-
115
REACTION
KINETICS
OF
SURFACE
PROCESSES
-
115
VIII
-
CONTENTS
2.6.2
2.7
2.8
2.8.1
2.8.2
2.8.3
2.8.4
INFLUENCES
OF
TRANSPORT
LIMITATIONS
ON
REACTION
RATES
-
121
ELECTROCHEMISTRY
AND
ELECTROCATALYSIS
-
133
REACTORS
FOR
SURFACE-CATALYTIC
REACTIONS
-
137
IDEAL
AND
REAL
REACTORS
-
137
REACTORS
FOR
THERMOCATALYTIC
PROCESSES
-
140
REACTORS
FOR
PHOTOCATALYTIC
PROCESSES
-
147
REACTORS
FOR
ELECTROCHEMICAL
CONVERSIONS
-
149
REFERENCES
-
150
3
3.1
3.1.1
3.1.1.1
3.1.1.2
3.1.1.3
3.1.1.4
3.1.1.5
3.1.1.6
3.1.2
3.1.3
TOOLS
OF
CATALYSIS
RESEARCH
-
158
CATALYST
PREPARATION
-
158
FORMATION
OF
SOLIDS
FROM
FLUID
PHASES
-
158
PRECIPITATION
AND
COPRECIPITATION
-
159
CRYSTALLIZATION:
SYNTHESIS
OF
ZEOLITES
AND
MOFS
----
165
SOL-GEL
TRANSITION
-
170
SOLIDIFICATION
OF
MELTS
-
173
SOLIDS
FROM
THE
GAS
PHASE
----
174
FLAME-BASED
SYNTHESIS
ROUTES
----
176
SHAPING
OF
CATALYST
PELLETS
-
177
DEPOSITION
OF
ACTIVE
COMPONENTS
ON
THE
INTERNAL
SURFACE
OF
POROUS
SUPPORTS
----
179
3.1.3.1
3.1.3.2
3.1.3.3
3.1.3.4
3.1.3.5
3.1.3.6
3.1.3.7
3.1.4
3.1.5
3.1.6
3.2
3.2.1
3.2.2
3.2.3
3.3
3.3.1
3.3.2
3.4
3.4.1
3.4.1.1
EQUILIBRIUM
ADSORPTION
AND
ION
EXCHANGE
-----180
IMPREGNATION
-
185
DEPOSITION-PRECIPITATION
-
187
ANCHORING,
GRAFTING,
AND
SURFACE
ORGANOMETALLIC
CHEMISTRY
-
188
DEPOSITION
OF
COLLOIDS
AND
MELT
INFILTRATION
----
192
DEPOSITION
OF
PRECURSORS
FROM
THE
GAS
PHASE
-----194
SOLID-STATE
METHODS
-----196
THERMAL
CONDITIONING
-
196
ACTIVATION
-
201
PREPARATION
OF
CATALYTICALLY
ACTIVE
ELECTRODES
-
203
RATE
MEASUREMENTS
IN
SURFACE
CATALYSIS
----
204
THERMAL
CATALYSIS
----
204
REACTORS
FOR
PHOTOCATALYTIC
RATE
MEASUREMENTS
-
219
MEASURING
ELECTROCHEMICAL
REACTION
RATES
----
222
APPLICATION-ORIENTED
CHARACTERIZATION
OF
SOLID
CATALYSTS
-
225
DENSITY
AND
POROSITY
OF
PARTICLES
AND
BEDS
-
225
STABILITY
TOWARD
MECHANICAL
STRESS
-
227
RESEARCH-ORIENTED
CHARACTERIZATION
OF
SOLID
CATALYSTS
-
228
ANALYSIS
OF
SURFACE
AREA
AND
POROSITY
-
228
CAPILLARY
PHENOMENA
IN
PORES
-
229
CONTENTS
-
IX
3.4.1.2
MEASURING
ADSORPTION
DATA
-
232
3.4.1.3
SPECIFIC
SURFACE
AREA:
THE
BET
METHOD
-
235
3.4.1.4
POROSITY
ANALYSIS
BY
PHYSISORPTION
-
237
3.4.1.5
POROSITY
ANALYSIS
BY
MERCURY
INTRUSION
-
239
3.4.1.6
ANALYSIS
OF
PARTICLE
DISPERSION
BY
CHEMISORPTION
-
240
3.4.2
THERMAL
ANALYSIS
AND
CALORIMETRY
-
242
3.4.2.1
STANDARD
METHODS:
DTA
AND
DTG
-
243
3.4.2.2
CALORIMETRY
IN
STATIONARY
AND
DYNAMIC
MODES
-
248
3.4.2.3
TEMPERATURE-PROGRAMMED
DESORPTION
(TPD)
AND
ADSORPTION
(TPA)
-
252
3.4.2.4
TEMPERATURE-PROGRAMMED
SURFACE
REACTION
(TPSR)
-
261
3.4.2.5
TEMPERATURE-PROGRAMMED
REDUCTION
(TPR),
OXIDATION
(TPO),
AND
SULFIDATION
(TPS)
-
263
3.4.3
SCATTERING
AND
DIFFRACTION
-
268
3.4.3.1
ELASTIC
AND
INELASTIC
SCATTERING
-
268
3.4.3.2
ELASTIC
SCATTERING
AT
ORDERED
ARRAYS:
DIFFRACTION
-
270
3.4.3.3
X-RAY
DIFFRACTION
(XRD)
-
279
3.4.3.4
OTHER
DIFFRACTION
AND
SCATTERING
TECHNIQUES
-
289
3.4.4
X-RAY
ABSORPTION
FINE
STRUCTURE
(XAFS)
-
293
3.4.4.1
FINE
STRUCTURE
IN
X-RAY
ABSORPTION
-
294
3.4.4.2
ACQUISITION
AND
INTERPRETATION
OF
X-RAY
ABSORPTION
SPECTRA
-
300
3.4.4.3
XAFS
IN
EXAMPLES
----
308
3.4.5
SURFACE
ANALYSIS
BY
PHOTOEMISSION
TECHNIQUES
-
312
3.4.5.1
PHOTOEMISSION
AND
SURFACE
SENSITIVITY
-
312
3.4.5.2
MEASURING
AND
ASSIGNING
PHOTOELECTRON
SPECTRA
-
315
3.4.5.3
SOURCES
OF
ANALYTICAL
INFORMATION
-
319
3.4.5.3.1
BINDING
ENERGIES
-
320
3.4.5.3.2
OPPORTUNITIES
BASED
ON
XPS
LINE
SHAPES
-
322
3.4.5.3.3
SURFACE
SENSITIVITY
AND
QUANTITATIVE
ANALYSIS
-
324
3.4.5.3.4
STRUCTURAL
SENSITIVITY
BY
COMBINING
XPS
AND
XAES
----
327
3.4.5.3.5
ULTRAVIOLET
PHOTOELECTRON
SPECTROSCOPY
-
328
3.4.5.4
XPS:
EXAMPLES
FOR
THE
INTERPRETATION
OF
SPECTRA
-
329
3.4.6
SURFACE
ANALYSIS
WITH
IONS:
SECONDARY
ION
MASS
SPECTROMETRY
(SIMS)
AND
LOW-ENERGY
ION
SCATTERING
(LEIS)
-
331
3.4.6.1
INTERACTIONS
BETWEEN
LOW-ENERGY
IONS
AND
SOLIDS
-
331
3.4.6.2
SECONDARY
ION
MASS
SPECTROMETRY
(SIMS)
-
333
3.4.6.3
LOW-ENERGY
ION
SCATTERING
(LEIS)
-----334
3.4.7
SPECTROSCOPY
OF
ELECTRONIC
TRANSITIONS:
ABSORPTION
OF
UV
AND
VISIBLE
LIGHT
----
341
3.4.7.1
ELECTRON
TRANSITIONS
AND
THEIR
DIAGNOSTIC
POTENTIAL
-
341
3.4.7.2
MEASURING
UV-VIS
SPECTRA
------
345
3.4.7.3
TYPICAL
APPLICATIONS
OF
UV-VIS
SPECTROSCOPY
IN
CATALYST
RESEARCH
-
351
3.4.8
VIBRATIONAL
SPECTROSCOPY
-
354
X
-
CONTENTS
3.4.8.1
VIBRATIONS
AND
VIBRATIONAL
SPECTRA
-
355
3.4.8.2
EXCITATION
PROCESSES
AND
SPECTROSCOPIES
-
360
3.4.83
MEASURING
IR
SPECTRA
OF
HETEROGENEOUS
CATALYSTS
-
362
3.4.8.4
IR
SPECTROSCOPY
WITH
CATALYSTS:
TYPICAL
APPLICATIONS
-
367
3.4.8.5
MEASURING
RAMAN
SPECTRA
OF
HETEROGENEOUS
CATALYSTS
-
376
3.4.8.6
RAMAN
SPECTROSCOPY
IN
CATALYSIS:
TYPICAL
APPLICATIONS
-
380
3.4.9
MAGNETIC
RESONANCE
SPECTROSCOPY
-
383
3.4.9.1
MAGNETISM
AND
MAGNETIC
RESONANCE
-
383
3.4.9.2
ELECTRON
PARAMAGNETIC
RESONANCE
SPECTROSCOPY
(EPR)
-
391
3.4.93
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
(NMR)
----
399
3.4.10
MDSSBAUER
SPECTROSCOPY
-
409
3.4.10.1
THE
MDSSBAUER
EFFECT
-----
409
3.4.10.2
SPECTROSCOPY
WITH
THE
MDSSBAUER
EFFECT
-
410
3.4.11
IMAGING
-
416
3.4.11.1
TRANSMISSION
ELECTRON
MICROSCOPY
(TEM)
-
418
3.4.11.2
SCANNING
ELECTRON
MICROSCOPY
(SEM)
-
430
3.4.11.3
SCANNING
PROBE
MICROSCOPY
-
434
3.4.12
ELECTROCHEMICAL
CHARACTERIZATION
TECHNIQUES
-----
439
3.5
COMPUTATIONAL
CHEMISTRY
IN
CATALYSIS
RESEARCH
-
443
3.5.1
WAVE
FUNCTION-BASED
QUANTUM
CHEMISTRY
AND
DENSITY
FUNCTIONAL
THEORY
-
444
3.5.2
CLUSTER
AND
PERIODIC
MODELS
-
449
3.53
QUANTUM
CHEMISTRY
IN
CATALYSIS
RESEARCH:
TYPICAL
APPLICATIONS
-
451
REFERENCES
-
460
4
A
CLOSE-UP
TO
SOME
IMPORTANT
ASPECTS
OF
SURFACE
CATALYSIS
-
475
4.1
A
PREFACE
-----
475
4.2
STRUCTURE
AND
ACTIVITY
------
477
4.2.1
THE
SABATIER
PRINCIPLE
------
477
4.2.2
ELECTRONIC
STRUCTURE
AND
CATALYTIC
ACTIVITY
ON
METAL
SURFACES
-
481
4.23
SPATIAL
STRUCTURE
AND
CATALYTIC
ACTIVITY
----
489
4.2.
4
PROMOTING
ACTIVITY
-
498
4.3
STRUCTURE
AND
SELECTIVITY
-----
504
4.3.1
SIDE
PRODUCTS
AND
STRATEGIES
-
504
4.3.2
SHAPE
SELECTIVITY
-
510
43.3
SELECTIVE
OXIDATION
IN
THE
GAS
PHASE
-
512
4.3.4
SELECTIVE
HYDROGENATION
-
519
4.3.5
PROMOTING
SELECTIVITY
-
523
4.4
STABILITY,
REGENERATION,
AND
REACTIVATION
-
525
4.4.1
MECHANISMS
OF
CATALYST
DEACTIVATION
-
526
4.4.1.1
POISONING
AND
FOULING
----
527
4.4.1.2
LOSS
OF
ACTIVE
COMPONENT
-
531
CONTENTS
-
XI
4.4.13
4.4.1.4
4.4.2
4.4.3
4.5
4.5.1
4.5.2
THERMAL
EFFECTS
-
532
MECHANICAL
DEGRADATION
-
534
PREVENTING
CATALYST
DECAY/PROMOTING
STABILITY
-
535
REGENERATION
OF
CATALYSTS
AND
THE
END
OF
THEIR
LIFE
CYCLE
-
540
TYPES
OF
REACTION
MECHANISMS
-
542
GETTING
INSIGHT
INTO
SURFACE
PROCESSES
-
542
REACTION
TYPES
AND
CATALYTIC
MECHANISMS:
CATALYSIS
ON
BRONSTED
SITES,
WITH
NUCLEOPHILIC
OXYGEN,
AND
VIA
METAL-CARBON
BONDS
-
545
4.5.2.1
4.5.2.2
4.5.23
4.5.3
4.5.4
4.5.5
4.5.6
4.6
4.7
4.8
4.9
4.9.1
4.9.2
REACTIONS
CATALYZED
BY
SOLID
BRONSTED
ACIDS
-
545
ALLYLIC
OXIDATION
OF
PROPENE
-
554
MECHANISMS
INVOLVING
METAL-CARBON
BONDS
-
559
SITE
ISOLATION
AND
CATALYTIC
MECHANISM
-
565
MECHANISMS
DEPENDING
ON
TRANSPORT
STEPS
----
574
MECHANISMS
INVOLVING
POOLS
OF
SECONDARY
SPECIES
-
580
THE
MULTIPLICITY
OF
SITES
AND
MECHANISMS
-
581
MICROKINETIC
MODELING
-
590
HETEROGENEOUS
CATALYSIS
IN
LIQUIDS:
WHAT
IS
SPECIAL?
-
594
STRUCTURE
AND
PERFORMANCE
IN
PHOTOCATALYSIS
-
601
STRUCTURE
AND
PERFORMANCE
IN
ELECTROCATALYSIS
-
606
ELECTROCATALYTIC
REACTION
MECHANISMS
-
606
RECENT
TOPICS
OF
ELECTROCATALYSIS
-
612
REFERENCES
-
616
5
WITH
CATALYSIS
INTO
THE
ANTHROPOCENE
AGE:
STRATEGIES
AND
A
LOOK
AHEAD
-
631
REFERENCES
-
641
APPENDIX
-
643
INDEX
-
673 |
| adam_txt |
CONTENTS
PREFACE
-
V
1
1.1
1.2
1.3
1.4
1.4.1
1.4.2
1.4.3
1.5
1.6
INTRODUCTION
-
1
CATALYSIS,
REACTION
RATE,
AND
EQUILIBRIUM
-
1
CATALYST
AND
REACTANT
PHASES
-
2
CATALYSIS
AND
DAILY
LIFE
-
4
BASIC
CONCEPTS
OF
SURFACE
CATALYSIS
-
8
REACTION
RATE
-
8
ACTIVITY,
SELECTIVITY,
AND
STABILITY
-
11
CATALYST
AND
CATALYTIC
PROCESS
-
13
SURFACE
CATALYSIS:
AN
ART
OR
A
SCIENCE?
-
17
CATALYST
RESEARCH:
AN
OVERVIEW
-
23
REFERENCES
-
26
2
2.1
2.2
2.2.1
2.2.2
2.3
2.3.1
2.3.2
2.3.2.1
2.3.2.2
2.3.2.3
2.3.2.4
2.3.2.5
2.3.2.6
2.3.3
2.3.4
2.4
2.4.1
2.4.2
2.4.3
2.4.4
2.5
2.5.1
2.5.2
2.6
2.6.1
SURFACE
CATALYSIS:
THE
SCENE
AND
THE
PLAY
-
28
SOLIDS
-
28
SURFACES
-
38
SURFACE
STRUCTURES
-
38
SURFACE
CHEMISTRY
-
48
PARTICLE
ARCHITECTURE
IN
CATALYTIC
MATERIALS
-
52
SIZE,
POROSITY,
AND
STRUCTURAL
HETEROGENEITY
OF
CATALYST
PARTICLES
-
52
SUPPORTS
FOR
HETEROGENEOUS
CATALYSTS
-
55
SILICA
(SIO
2
)
----
56
ALUMINA
(AI
2
O
3
)
----
57
ALUMOSILICATES/ZEOLITES
----
59
METAL-ORGANIC
FRAMEWORKS
-
67
TITANIA,
ZIRCONIA,
CERIA
-
72
CARBON
MATERIALS
-
75
SUPPORT
AND
SUPPORTED
SPECIES
-
80
ALTERNATIVE
CATALYST
ARCHITECTURES
-
93
ADSORPTION
-
95
ADSORPTION
AND
DESORPTION:
PHENOMENA
AND
CLASSIFICATION
-
95
PHYSISORPTION
AND
CHEMISORPTION
-
97
DESCRIPTION
OF
EQUILIBRIA
IN
GAS-PHASE
ADSORPTION
-
102
DESCRIPTION
OF
EQUILIBRIA
IN
LIQUID-PHASE
ADSORPTION
-
105
SURFACE
REACTIONS
-
106
THERMAL
CATALYSIS
-
106
PHOTOCATALYSIS
-
113
REACTION
MECHANISMS
AND
REACTION
KINETICS
IN
THERMAL
CATALYSIS
-
115
REACTION
KINETICS
OF
SURFACE
PROCESSES
-
115
VIII
-
CONTENTS
2.6.2
2.7
2.8
2.8.1
2.8.2
2.8.3
2.8.4
INFLUENCES
OF
TRANSPORT
LIMITATIONS
ON
REACTION
RATES
-
121
ELECTROCHEMISTRY
AND
ELECTROCATALYSIS
-
133
REACTORS
FOR
SURFACE-CATALYTIC
REACTIONS
-
137
IDEAL
AND
REAL
REACTORS
-
137
REACTORS
FOR
THERMOCATALYTIC
PROCESSES
-
140
REACTORS
FOR
PHOTOCATALYTIC
PROCESSES
-
147
REACTORS
FOR
ELECTROCHEMICAL
CONVERSIONS
-
149
REFERENCES
-
150
3
3.1
3.1.1
3.1.1.1
3.1.1.2
3.1.1.3
3.1.1.4
3.1.1.5
3.1.1.6
3.1.2
3.1.3
TOOLS
OF
CATALYSIS
RESEARCH
-
158
CATALYST
PREPARATION
-
158
FORMATION
OF
SOLIDS
FROM
FLUID
PHASES
-
158
PRECIPITATION
AND
COPRECIPITATION
-
159
CRYSTALLIZATION:
SYNTHESIS
OF
ZEOLITES
AND
MOFS
----
165
SOL-GEL
TRANSITION
-
170
SOLIDIFICATION
OF
MELTS
-
173
SOLIDS
FROM
THE
GAS
PHASE
----
174
FLAME-BASED
SYNTHESIS
ROUTES
----
176
SHAPING
OF
CATALYST
PELLETS
-
177
DEPOSITION
OF
ACTIVE
COMPONENTS
ON
THE
INTERNAL
SURFACE
OF
POROUS
SUPPORTS
----
179
3.1.3.1
3.1.3.2
3.1.3.3
3.1.3.4
3.1.3.5
3.1.3.6
3.1.3.7
3.1.4
3.1.5
3.1.6
3.2
3.2.1
3.2.2
3.2.3
3.3
3.3.1
3.3.2
3.4
3.4.1
3.4.1.1
EQUILIBRIUM
ADSORPTION
AND
ION
EXCHANGE
-----180
IMPREGNATION
-
185
DEPOSITION-PRECIPITATION
-
187
ANCHORING,
GRAFTING,
AND
SURFACE
ORGANOMETALLIC
CHEMISTRY
-
188
DEPOSITION
OF
COLLOIDS
AND
MELT
INFILTRATION
----
192
DEPOSITION
OF
PRECURSORS
FROM
THE
GAS
PHASE
-----194
SOLID-STATE
METHODS
-----196
THERMAL
CONDITIONING
-
196
ACTIVATION
-
201
PREPARATION
OF
CATALYTICALLY
ACTIVE
ELECTRODES
-
203
RATE
MEASUREMENTS
IN
SURFACE
CATALYSIS
----
204
THERMAL
CATALYSIS
----
204
REACTORS
FOR
PHOTOCATALYTIC
RATE
MEASUREMENTS
-
219
MEASURING
ELECTROCHEMICAL
REACTION
RATES
----
222
APPLICATION-ORIENTED
CHARACTERIZATION
OF
SOLID
CATALYSTS
-
225
DENSITY
AND
POROSITY
OF
PARTICLES
AND
BEDS
-
225
STABILITY
TOWARD
MECHANICAL
STRESS
-
227
RESEARCH-ORIENTED
CHARACTERIZATION
OF
SOLID
CATALYSTS
-
228
ANALYSIS
OF
SURFACE
AREA
AND
POROSITY
-
228
CAPILLARY
PHENOMENA
IN
PORES
-
229
CONTENTS
-
IX
3.4.1.2
MEASURING
ADSORPTION
DATA
-
232
3.4.1.3
SPECIFIC
SURFACE
AREA:
THE
BET
METHOD
-
235
3.4.1.4
POROSITY
ANALYSIS
BY
PHYSISORPTION
-
237
3.4.1.5
POROSITY
ANALYSIS
BY
MERCURY
INTRUSION
-
239
3.4.1.6
ANALYSIS
OF
PARTICLE
DISPERSION
BY
CHEMISORPTION
-
240
3.4.2
THERMAL
ANALYSIS
AND
CALORIMETRY
-
242
3.4.2.1
STANDARD
METHODS:
DTA
AND
DTG
-
243
3.4.2.2
CALORIMETRY
IN
STATIONARY
AND
DYNAMIC
MODES
-
248
3.4.2.3
TEMPERATURE-PROGRAMMED
DESORPTION
(TPD)
AND
ADSORPTION
(TPA)
-
252
3.4.2.4
TEMPERATURE-PROGRAMMED
SURFACE
REACTION
(TPSR)
-
261
3.4.2.5
TEMPERATURE-PROGRAMMED
REDUCTION
(TPR),
OXIDATION
(TPO),
AND
SULFIDATION
(TPS)
-
263
3.4.3
SCATTERING
AND
DIFFRACTION
-
268
3.4.3.1
ELASTIC
AND
INELASTIC
SCATTERING
-
268
3.4.3.2
ELASTIC
SCATTERING
AT
ORDERED
ARRAYS:
DIFFRACTION
-
270
3.4.3.3
X-RAY
DIFFRACTION
(XRD)
-
279
3.4.3.4
OTHER
DIFFRACTION
AND
SCATTERING
TECHNIQUES
-
289
3.4.4
X-RAY
ABSORPTION
FINE
STRUCTURE
(XAFS)
-
293
3.4.4.1
FINE
STRUCTURE
IN
X-RAY
ABSORPTION
-
294
3.4.4.2
ACQUISITION
AND
INTERPRETATION
OF
X-RAY
ABSORPTION
SPECTRA
-
300
3.4.4.3
XAFS
IN
EXAMPLES
----
308
3.4.5
SURFACE
ANALYSIS
BY
PHOTOEMISSION
TECHNIQUES
-
312
3.4.5.1
PHOTOEMISSION
AND
SURFACE
SENSITIVITY
-
312
3.4.5.2
MEASURING
AND
ASSIGNING
PHOTOELECTRON
SPECTRA
-
315
3.4.5.3
SOURCES
OF
ANALYTICAL
INFORMATION
-
319
3.4.5.3.1
BINDING
ENERGIES
-
320
3.4.5.3.2
OPPORTUNITIES
BASED
ON
XPS
LINE
SHAPES
-
322
3.4.5.3.3
SURFACE
SENSITIVITY
AND
QUANTITATIVE
ANALYSIS
-
324
3.4.5.3.4
STRUCTURAL
SENSITIVITY
BY
COMBINING
XPS
AND
XAES
----
327
3.4.5.3.5
ULTRAVIOLET
PHOTOELECTRON
SPECTROSCOPY
-
328
3.4.5.4
XPS:
EXAMPLES
FOR
THE
INTERPRETATION
OF
SPECTRA
-
329
3.4.6
SURFACE
ANALYSIS
WITH
IONS:
SECONDARY
ION
MASS
SPECTROMETRY
(SIMS)
AND
LOW-ENERGY
ION
SCATTERING
(LEIS)
-
331
3.4.6.1
INTERACTIONS
BETWEEN
LOW-ENERGY
IONS
AND
SOLIDS
-
331
3.4.6.2
SECONDARY
ION
MASS
SPECTROMETRY
(SIMS)
-
333
3.4.6.3
LOW-ENERGY
ION
SCATTERING
(LEIS)
-----334
3.4.7
SPECTROSCOPY
OF
ELECTRONIC
TRANSITIONS:
ABSORPTION
OF
UV
AND
VISIBLE
LIGHT
----
341
3.4.7.1
ELECTRON
TRANSITIONS
AND
THEIR
DIAGNOSTIC
POTENTIAL
-
341
3.4.7.2
MEASURING
UV-VIS
SPECTRA
------
345
3.4.7.3
TYPICAL
APPLICATIONS
OF
UV-VIS
SPECTROSCOPY
IN
CATALYST
RESEARCH
-
351
3.4.8
VIBRATIONAL
SPECTROSCOPY
-
354
X
-
CONTENTS
3.4.8.1
VIBRATIONS
AND
VIBRATIONAL
SPECTRA
-
355
3.4.8.2
EXCITATION
PROCESSES
AND
SPECTROSCOPIES
-
360
3.4.83
MEASURING
IR
SPECTRA
OF
HETEROGENEOUS
CATALYSTS
-
362
3.4.8.4
IR
SPECTROSCOPY
WITH
CATALYSTS:
TYPICAL
APPLICATIONS
-
367
3.4.8.5
MEASURING
RAMAN
SPECTRA
OF
HETEROGENEOUS
CATALYSTS
-
376
3.4.8.6
RAMAN
SPECTROSCOPY
IN
CATALYSIS:
TYPICAL
APPLICATIONS
-
380
3.4.9
MAGNETIC
RESONANCE
SPECTROSCOPY
-
383
3.4.9.1
MAGNETISM
AND
MAGNETIC
RESONANCE
-
383
3.4.9.2
ELECTRON
PARAMAGNETIC
RESONANCE
SPECTROSCOPY
(EPR)
-
391
3.4.93
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
(NMR)
----
399
3.4.10
MDSSBAUER
SPECTROSCOPY
-
409
3.4.10.1
THE
MDSSBAUER
EFFECT
-----
409
3.4.10.2
SPECTROSCOPY
WITH
THE
MDSSBAUER
EFFECT
-
410
3.4.11
IMAGING
-
416
3.4.11.1
TRANSMISSION
ELECTRON
MICROSCOPY
(TEM)
-
418
3.4.11.2
SCANNING
ELECTRON
MICROSCOPY
(SEM)
-
430
3.4.11.3
SCANNING
PROBE
MICROSCOPY
-
434
3.4.12
ELECTROCHEMICAL
CHARACTERIZATION
TECHNIQUES
-----
439
3.5
COMPUTATIONAL
CHEMISTRY
IN
CATALYSIS
RESEARCH
-
443
3.5.1
WAVE
FUNCTION-BASED
QUANTUM
CHEMISTRY
AND
DENSITY
FUNCTIONAL
THEORY
-
444
3.5.2
CLUSTER
AND
PERIODIC
MODELS
-
449
3.53
QUANTUM
CHEMISTRY
IN
CATALYSIS
RESEARCH:
TYPICAL
APPLICATIONS
-
451
REFERENCES
-
460
4
A
CLOSE-UP
TO
SOME
IMPORTANT
ASPECTS
OF
SURFACE
CATALYSIS
-
475
4.1
A
PREFACE
-----
475
4.2
STRUCTURE
AND
ACTIVITY
------
477
4.2.1
THE
SABATIER
PRINCIPLE
------
477
4.2.2
ELECTRONIC
STRUCTURE
AND
CATALYTIC
ACTIVITY
ON
METAL
SURFACES
-
481
4.23
SPATIAL
STRUCTURE
AND
CATALYTIC
ACTIVITY
----
489
4.2.
4
PROMOTING
ACTIVITY
-
498
4.3
STRUCTURE
AND
SELECTIVITY
-----
504
4.3.1
SIDE
PRODUCTS
AND
STRATEGIES
-
504
4.3.2
SHAPE
SELECTIVITY
-
510
43.3
SELECTIVE
OXIDATION
IN
THE
GAS
PHASE
-
512
4.3.4
SELECTIVE
HYDROGENATION
-
519
4.3.5
PROMOTING
SELECTIVITY
-
523
4.4
STABILITY,
REGENERATION,
AND
REACTIVATION
-
525
4.4.1
MECHANISMS
OF
CATALYST
DEACTIVATION
-
526
4.4.1.1
POISONING
AND
FOULING
----
527
4.4.1.2
LOSS
OF
ACTIVE
COMPONENT
-
531
CONTENTS
-
XI
4.4.13
4.4.1.4
4.4.2
4.4.3
4.5
4.5.1
4.5.2
THERMAL
EFFECTS
-
532
MECHANICAL
DEGRADATION
-
534
PREVENTING
CATALYST
DECAY/PROMOTING
STABILITY
-
535
REGENERATION
OF
CATALYSTS
AND
THE
END
OF
THEIR
LIFE
CYCLE
-
540
TYPES
OF
REACTION
MECHANISMS
-
542
GETTING
INSIGHT
INTO
SURFACE
PROCESSES
-
542
REACTION
TYPES
AND
CATALYTIC
MECHANISMS:
CATALYSIS
ON
BRONSTED
SITES,
WITH
NUCLEOPHILIC
OXYGEN,
AND
VIA
METAL-CARBON
BONDS
-
545
4.5.2.1
4.5.2.2
4.5.23
4.5.3
4.5.4
4.5.5
4.5.6
4.6
4.7
4.8
4.9
4.9.1
4.9.2
REACTIONS
CATALYZED
BY
SOLID
BRONSTED
ACIDS
-
545
ALLYLIC
OXIDATION
OF
PROPENE
-
554
MECHANISMS
INVOLVING
METAL-CARBON
BONDS
-
559
SITE
ISOLATION
AND
CATALYTIC
MECHANISM
-
565
MECHANISMS
DEPENDING
ON
TRANSPORT
STEPS
----
574
MECHANISMS
INVOLVING
POOLS
OF
SECONDARY
SPECIES
-
580
THE
MULTIPLICITY
OF
SITES
AND
MECHANISMS
-
581
MICROKINETIC
MODELING
-
590
HETEROGENEOUS
CATALYSIS
IN
LIQUIDS:
WHAT
IS
SPECIAL?
-
594
STRUCTURE
AND
PERFORMANCE
IN
PHOTOCATALYSIS
-
601
STRUCTURE
AND
PERFORMANCE
IN
ELECTROCATALYSIS
-
606
ELECTROCATALYTIC
REACTION
MECHANISMS
-
606
RECENT
TOPICS
OF
ELECTROCATALYSIS
-
612
REFERENCES
-
616
5
WITH
CATALYSIS
INTO
THE
ANTHROPOCENE
AGE:
STRATEGIES
AND
A
LOOK
AHEAD
-
631
REFERENCES
-
641
APPENDIX
-
643
INDEX
-
673 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Grünert, Wolfgang 1949- Kleist, Wolfgang Muhler, Martin 1961- |
| author_GND | (DE-588)142261165 (DE-588)1072788454 (DE-588)143495577 |
| author_facet | Grünert, Wolfgang 1949- Kleist, Wolfgang Muhler, Martin 1961- |
| author_role | aut aut aut |
| author_sort | Grünert, Wolfgang 1949- |
| author_variant | w g wg w k wk m m mm |
| building | Verbundindex |
| bvnumber | BV049097728 |
| classification_rvk | VE 7040 VE 7041 VE 7000 |
| classification_tum | CHE 180 CHE 167 |
| ctrlnum | (OCoLC)1395137141 (DE-599)DNB1284094111 |
| discipline | Chemie / Pharmazie Physik Chemie |
| discipline_str_mv | Chemie / Pharmazie Physik Chemie |
| format | Book |
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| id | DE-604.BV049097728 |
| illustrated | Illustrated |
| index_date | 2024-07-03T22:31:48Z |
| indexdate | 2024-10-21T14:01:39Z |
| institution | BVB |
| institution_GND | (DE-588)10095502-2 |
| isbn | 9783110632477 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-034359316 |
| oclc_num | 1395137141 |
| open_access_boolean | |
| owner | DE-29T DE-91G DE-BY-TUM DE-19 DE-BY-UBM DE-11 DE-20 DE-1051 |
| owner_facet | DE-29T DE-91G DE-BY-TUM DE-19 DE-BY-UBM DE-11 DE-20 DE-1051 |
| physical | XI, 695 Seiten Illustrationen, Diagramme |
| publishDate | 2023 |
| publishDateSearch | 2023 |
| publishDateSort | 2023 |
| publisher | De Gruyter |
| record_format | marc |
| series2 | De Gruyter graduate |
| spelling | Grünert, Wolfgang 1949- Verfasser (DE-588)142261165 aut Catalysis at surfaces Wolfgang Grünert, Wolfgang Kleist, Martin Muhler Berlin ; Boston De Gruyter [2023] XI, 695 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier De Gruyter graduate Katalyse (DE-588)4029921-1 gnd rswk-swf Oberflächenreaktion (DE-588)4140095-1 gnd rswk-swf Oberflächenchemie (DE-588)4126166-5 gnd rswk-swf Catalysis Catalyst Heterogene Katalyse Heterogeneous Catalysis Katalysator Katalyse Oberflächenchemie Surface Chemistry TB: Textbook Katalyse (DE-588)4029921-1 s Oberflächenreaktion (DE-588)4140095-1 s Oberflächenchemie (DE-588)4126166-5 s DE-604 Kleist, Wolfgang Verfasser (DE-588)1072788454 aut Muhler, Martin 1961- Verfasser (DE-588)143495577 aut Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-11-063248-4 Erscheint auch als Online-Ausgabe, EPUB 978-3-11-063254-5 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034359316&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20230322 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Grünert, Wolfgang 1949- Kleist, Wolfgang Muhler, Martin 1961- Catalysis at surfaces Katalyse (DE-588)4029921-1 gnd Oberflächenreaktion (DE-588)4140095-1 gnd Oberflächenchemie (DE-588)4126166-5 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4140095-1 (DE-588)4126166-5 |
| title | Catalysis at surfaces |
| title_auth | Catalysis at surfaces |
| title_exact_search | Catalysis at surfaces |
| title_exact_search_txtP | Catalysis at surfaces |
| title_full | Catalysis at surfaces Wolfgang Grünert, Wolfgang Kleist, Martin Muhler |
| title_fullStr | Catalysis at surfaces Wolfgang Grünert, Wolfgang Kleist, Martin Muhler |
| title_full_unstemmed | Catalysis at surfaces Wolfgang Grünert, Wolfgang Kleist, Martin Muhler |
| title_short | Catalysis at surfaces |
| title_sort | catalysis at surfaces |
| topic | Katalyse (DE-588)4029921-1 gnd Oberflächenreaktion (DE-588)4140095-1 gnd Oberflächenchemie (DE-588)4126166-5 gnd |
| topic_facet | Katalyse Oberflächenreaktion Oberflächenchemie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034359316&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT grunertwolfgang catalysisatsurfaces AT kleistwolfgang catalysisatsurfaces AT muhlermartin catalysisatsurfaces AT walterdegruytergmbhcokg catalysisatsurfaces |