Calibration in analytical science: methods and procedures
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
[2023]
|
| Subjects: | |
| Online Access: | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34846-6/ Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | xi, 372 Seiten Illustrationen, Diagramme 25 cm, 896 g |
| ISBN: | 9783527348466 3527348468 |
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Record in the Search Index
| _version_ | 1804185387363467264 |
|---|---|
| adam_text | CONTENTS
PREFACE
IX
1
CALIBRATION
FUNDAMENTALS
1
1.1
ANALYTICAL
CONTEXT
1
1.2
PRINCIPLES
OF
ANALYTICAL
CALIBRATION
2
1.3
CALIBRATION
STANDARDS
AND
MODELS
5
1.4
CALIBRATION
PROCEDURES
AND
METHODS
7
1.5
CALIBRATION
IN
THE
CONTEXT
OF
MEASUREMENT
ERRORS
8
1.5.1
UNCONTROLLED
ANALYTICAL
EFFECTS
9
1.5.2
ELIMINATION
AND
COMPENSATION
OF
UNCONTROLLED
EFFECTS
11
1.6
CALIBRATION
IN
QUALITATIVE
ANALYSIS
14
1.7
CALIBRATION
IN
QUANTITATIVE
ANALYSIS
18
1.8
GENERAL
RULES
FOR
CORRECT
CALIBRATION
22
REFERENCES
24
2
CALIBRATION-FREE
ANALYSIS
25
2.1
NOVEL
APPROACH
25
2.2
EMPIRICAL
CALIBRATION
26
2.3
THEORETICAL
CALIBRATION
30
2.3.1
FIXED
MODELS
30
2.3.2
FLEXIBLE
MODELS
36
REFERENCES
45
3
CALIBRATION
METHODS
IN
QUALITATIVE
ANALYSIS
47
3.1
CLASSIFICATION
47
3.2
EXTERNAL
CALIBRATION
METHODS
49
3.2.1
EXTERNAL
STANDARD
METHOD
49
3.2.2
REFERENCE
SAMPLE
METHOD
59
3.3
INTERNAL
CALIBRATION
METHODS
71
3.3.1
INTERNAL
STANDARD
METHOD
71
3.3.2
INDIRECT
METHOD
75
3.4
STANDARD
ADDITION
METHOD
80
REFERENCES
83
VI
CONTENTS
4
INTRODUCTION
TO
EMPIRICAL
CALIBRATION
IN
QUANTITATIVE
ANALYSIS
85
4.1
4.2
4.3
4.4
CLASSIFICATION
85
FORMULATION
OF
MODEL
FUNCTIONS
86
EXAMINATION
OF
INTERFERENCE
EFFECT
93
MATHEMATICAL
MODELING
OF
REAL
FUNCTION
98
REFERENCES
100
5
5.1
5.1.1
5.1.1.1
5.1.2
5.2
5.2.1
5.2.2
COMPARATIVE
CALIBRATION
METHODS
103
EXTERNAL
CALIBRATION
METHODS
103
EXTERNAL
STANDARD
METHOD
103
MODIFIED
PROCEDURES
110
DILUTION
METHOD
115
INTERNAL
CALIBRATION METHODS
125
INTERNAL
STANDARD
METHOD
125
INDIRECT
METHOD
133
REFERENCES
141
6
6.1
6.2
6.2.1
6.2.1.1
6.2.2
6.2.3
6.3
6.4
6.4.1
6.4.2
6.4.2.1
ADDITIVE
CALIBRATION
METHODS
143
BASIC
ASPECTS
143
STANDARD
ADDITION
METHOD
144
EXTRAPOLATIVE
VARIANT
144
MODIFIED
PROCEDURES
155
INTERPOLATE
VARIANTS
162
INDICATIVE
VARIANT
167
TITRATION
172
ISOTOPE
DILUTION
METHOD
180
RADIOMETRIC
ISOTOPE
DILUTION
182
ISOTOPE
DILUTION
MASS
SPECTROMETRY
189
MODIFIED
PROCEDURES
197
REFERENCES
199
7
7.1
7.1.1
7.1.2
7.2
CALIBRATION
IN
NONEQUILIBRIUM
CONDITIONS
203
FLOW
INJECTION
ANALYSIS
203
MANIPULATION
TECHNIQUES
205
GRADIENT
TECHNIQUE
212
KINETIC
ANALYSIS
220
REFERENCES
231
8
8.1
8.1.1
8.1.2
8.1.3
8.2
COMPLEX
CALIBRATION
APPROACHES
233
EXTRAPOLATIVE
METHODS
233
EXTRAPOLATIVE
INDIRECT
METHOD
234
EXTRAPOLATIVE
INTERNAL
STANDARD
METHOD
239
EXTRAPOLATIVE
DILUTION
METHOD
244
MIXED
METHODS
252
CONTENTS
VII
INDEX
367
8.3
8.3.1
8.3.1.1
8.3.1.2
8.3.2
8.3.2.1
8.3.3
COMBINED
METHODS
256
INTEGRATED
CALIBRATION
METHODS
256
SIMPLE
INTEGRATED
METHOD
256
COMPLEMENTARY
DILUTION
METHOD
261
GENERALIZED
CALIBRATION
STRATEGY
270
VERSATILE
FLOW
INJECTION
CALIBRATION
MODULE
276
STANDARD
DILUTION
ANALYSIS
280
REFERENCES
286
9
CALIBRATION
APPROACHES
FOR
DETECTION
AND
EXAMINATION
OF
INTERFERENCE
EFFECTS
289
9.1
9.2
INTRODUCTION
289
SIMPLE
PROCEDURES
FOR DETECTION
AND
EXAMINATION
OF
INTERFERENCE
EFFECTS
290
9.3
9.3.1
9.3.2
9.3.3
DETECTION
AND
COMPENSATION
OF
ADDITIVE
INTERFERENCE
EFFECT
295
INTERPOLATIVE
PROCEDURE
297
EXTRAPOLATIVE
PROCEDURE
301
INTEGRATED
PROCEDURE
308
REFERENCES
311
10
CALIBRATION-BASED
PROCEDURES
FOR
CORRECTION
OF
PREPARATIVE
EFFECTS
313
10.1
10.2
10.3
10.3.1
10.3.2
10.3.3
10.3.4
INTRODUCTION
313
SPECIFIC
PROCEDURES
314
SURROGATE
RECOVERY
METHOD
316
RELIABILITY
OF
THE
METHOD
318
INTERPRETATIONS
OF
THE
METHOD
321
RECOVERY
VS.
INTERFERENCE
EFFECT
324
RECOVERY
VS.
SPECIATION
EFFECT
329
REFERENCES
333
11
11.1
11.2
11.3
11.4
CALIBRATION-RELATED
APPLICATIONS
OF
EXPERIMENTAL
PLANS
335
INTRODUCTION
335
EXAMINATION
OF
INTERFERENCE
EFFECTS
337
MODELING
OF
REAL
FUNCTIONS
342
MULTICOMPONENT
ANALYSIS
347
REFERENCES
356
12
FINAL
REMARKS
359
REFERENCES
365
|
| adam_txt |
CONTENTS
PREFACE
IX
1
CALIBRATION
FUNDAMENTALS
1
1.1
ANALYTICAL
CONTEXT
1
1.2
PRINCIPLES
OF
ANALYTICAL
CALIBRATION
2
1.3
CALIBRATION
STANDARDS
AND
MODELS
5
1.4
CALIBRATION
PROCEDURES
AND
METHODS
7
1.5
CALIBRATION
IN
THE
CONTEXT
OF
MEASUREMENT
ERRORS
8
1.5.1
UNCONTROLLED
ANALYTICAL
EFFECTS
9
1.5.2
ELIMINATION
AND
COMPENSATION
OF
UNCONTROLLED
EFFECTS
11
1.6
CALIBRATION
IN
QUALITATIVE
ANALYSIS
14
1.7
CALIBRATION
IN
QUANTITATIVE
ANALYSIS
18
1.8
GENERAL
RULES
FOR
CORRECT
CALIBRATION
22
REFERENCES
24
2
"
CALIBRATION-FREE
"
ANALYSIS
25
2.1
NOVEL
APPROACH
25
2.2
EMPIRICAL
CALIBRATION
26
2.3
THEORETICAL
CALIBRATION
30
2.3.1
FIXED
MODELS
30
2.3.2
FLEXIBLE
MODELS
36
REFERENCES
45
3
CALIBRATION
METHODS
IN
QUALITATIVE
ANALYSIS
47
3.1
CLASSIFICATION
47
3.2
EXTERNAL
CALIBRATION
METHODS
49
3.2.1
EXTERNAL
STANDARD
METHOD
49
3.2.2
REFERENCE
SAMPLE
METHOD
59
3.3
INTERNAL
CALIBRATION
METHODS
71
3.3.1
INTERNAL
STANDARD
METHOD
71
3.3.2
INDIRECT
METHOD
75
3.4
STANDARD
ADDITION
METHOD
80
REFERENCES
83
VI
CONTENTS
4
INTRODUCTION
TO
EMPIRICAL
CALIBRATION
IN
QUANTITATIVE
ANALYSIS
85
4.1
4.2
4.3
4.4
CLASSIFICATION
85
FORMULATION
OF
MODEL
FUNCTIONS
86
EXAMINATION
OF
INTERFERENCE
EFFECT
93
MATHEMATICAL
MODELING
OF
REAL
FUNCTION
98
REFERENCES
100
5
5.1
5.1.1
5.1.1.1
5.1.2
5.2
5.2.1
5.2.2
COMPARATIVE
CALIBRATION
METHODS
103
EXTERNAL
CALIBRATION
METHODS
103
EXTERNAL
STANDARD
METHOD
103
MODIFIED
PROCEDURES
110
DILUTION
METHOD
115
INTERNAL
CALIBRATION METHODS
125
INTERNAL
STANDARD
METHOD
125
INDIRECT
METHOD
133
REFERENCES
141
6
6.1
6.2
6.2.1
6.2.1.1
6.2.2
6.2.3
6.3
6.4
6.4.1
6.4.2
6.4.2.1
ADDITIVE
CALIBRATION
METHODS
143
BASIC
ASPECTS
143
STANDARD
ADDITION
METHOD
144
EXTRAPOLATIVE
VARIANT
144
MODIFIED
PROCEDURES
155
INTERPOLATE
VARIANTS
162
INDICATIVE
VARIANT
167
TITRATION
172
ISOTOPE
DILUTION
METHOD
180
RADIOMETRIC
ISOTOPE
DILUTION
182
ISOTOPE
DILUTION
MASS
SPECTROMETRY
189
MODIFIED
PROCEDURES
197
REFERENCES
199
7
7.1
7.1.1
7.1.2
7.2
CALIBRATION
IN
NONEQUILIBRIUM
CONDITIONS
203
FLOW
INJECTION
ANALYSIS
203
MANIPULATION
TECHNIQUES
205
GRADIENT
TECHNIQUE
212
KINETIC
ANALYSIS
220
REFERENCES
231
8
8.1
8.1.1
8.1.2
8.1.3
8.2
COMPLEX
CALIBRATION
APPROACHES
233
EXTRAPOLATIVE
METHODS
233
EXTRAPOLATIVE
INDIRECT
METHOD
234
EXTRAPOLATIVE
INTERNAL
STANDARD
METHOD
239
EXTRAPOLATIVE
DILUTION
METHOD
244
MIXED
METHODS
252
CONTENTS
VII
INDEX
367
8.3
8.3.1
8.3.1.1
8.3.1.2
8.3.2
8.3.2.1
8.3.3
COMBINED
METHODS
256
INTEGRATED
CALIBRATION
METHODS
256
SIMPLE
INTEGRATED
METHOD
256
COMPLEMENTARY
DILUTION
METHOD
261
GENERALIZED
CALIBRATION
STRATEGY
270
VERSATILE
FLOW
INJECTION
CALIBRATION
MODULE
276
STANDARD
DILUTION
ANALYSIS
280
REFERENCES
286
9
CALIBRATION
APPROACHES
FOR
DETECTION
AND
EXAMINATION
OF
INTERFERENCE
EFFECTS
289
9.1
9.2
INTRODUCTION
289
SIMPLE
PROCEDURES
FOR DETECTION
AND
EXAMINATION
OF
INTERFERENCE
EFFECTS
290
9.3
9.3.1
9.3.2
9.3.3
DETECTION
AND
COMPENSATION
OF
ADDITIVE
INTERFERENCE
EFFECT
295
INTERPOLATIVE
PROCEDURE
297
EXTRAPOLATIVE
PROCEDURE
301
INTEGRATED
PROCEDURE
308
REFERENCES
311
10
CALIBRATION-BASED
PROCEDURES
FOR
CORRECTION
OF
PREPARATIVE
EFFECTS
313
10.1
10.2
10.3
10.3.1
10.3.2
10.3.3
10.3.4
INTRODUCTION
313
SPECIFIC
PROCEDURES
314
SURROGATE
RECOVERY
METHOD
316
RELIABILITY
OF
THE
METHOD
318
INTERPRETATIONS
OF
THE
METHOD
321
RECOVERY
VS.
INTERFERENCE
EFFECT
324
RECOVERY
VS.
SPECIATION
EFFECT
329
REFERENCES
333
11
11.1
11.2
11.3
11.4
CALIBRATION-RELATED
APPLICATIONS
OF
EXPERIMENTAL
PLANS
335
INTRODUCTION
335
EXAMINATION
OF
INTERFERENCE
EFFECTS
337
MODELING
OF
REAL
FUNCTIONS
342
MULTICOMPONENT
ANALYSIS
347
REFERENCES
356
12
FINAL
REMARKS
359
REFERENCES
365 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Kościelniak, Paweł 1952- |
| author_GND | (DE-588)1290453551 |
| author_facet | Kościelniak, Paweł 1952- |
| author_role | aut |
| author_sort | Kościelniak, Paweł 1952- |
| author_variant | p k pk |
| building | Verbundindex |
| bvnumber | BV049072097 |
| classification_rvk | VG 5100 VG 5170 VG 5171 |
| ctrlnum | (OCoLC)1387594049 (DE-599)DNB1267209011 |
| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV049072097 |
| illustrated | Illustrated |
| index_date | 2024-07-03T22:27:28Z |
| indexdate | 2024-07-10T09:54:25Z |
| institution | BVB |
| institution_GND | (DE-588)16179388-5 |
| isbn | 9783527348466 3527348468 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-034334028 |
| oclc_num | 1387594049 |
| open_access_boolean | |
| owner | DE-703 DE-19 DE-BY-UBM |
| owner_facet | DE-703 DE-19 DE-BY-UBM |
| physical | xi, 372 Seiten Illustrationen, Diagramme 25 cm, 896 g |
| publishDate | 2023 |
| publishDateSearch | 2023 |
| publishDateSort | 2023 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Kościelniak, Paweł 1952- Verfasser (DE-588)1290453551 aut Calibration in analytical science methods and procedures Paweł Kościelniak Weinheim Wiley-VCH [2023] xi, 372 Seiten Illustrationen, Diagramme 25 cm, 896 g txt rdacontent n rdamedia nc rdacarrier Kalibrieren Messtechnik (DE-588)4198763-9 gnd rswk-swf Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Analytical Chemistry Analytische Chemie Chemie Chemistry Drug QA/Analysis Physics Physik Qualitätssicherung / Analyse in der Pharmazie CH10: Analytische Chemie CH66: Qualitätssicherung / Analyse in der Pharmazie PH00: Allg. Physik Qualitätssicherung Kalibrieren Messtechnik (DE-588)4198763-9 s Analytische Chemie (DE-588)4129906-1 s DE-604 Wiley-VCH (DE-588)16179388-5 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-527-83110-4 Erscheint auch als Online-Ausgabe, EPUB 978-3-527-83112-8 Erscheint auch als Online-Ausgabe 978-3-527-83111-1 X:MVB http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34846-6/ B:DE-101 application/pdf https://d-nb.info/1267209011/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034334028&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p dnb 20230623 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Kościelniak, Paweł 1952- Calibration in analytical science methods and procedures Kalibrieren Messtechnik (DE-588)4198763-9 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| subject_GND | (DE-588)4198763-9 (DE-588)4129906-1 |
| title | Calibration in analytical science methods and procedures |
| title_auth | Calibration in analytical science methods and procedures |
| title_exact_search | Calibration in analytical science methods and procedures |
| title_exact_search_txtP | Calibration in analytical science methods and procedures |
| title_full | Calibration in analytical science methods and procedures Paweł Kościelniak |
| title_fullStr | Calibration in analytical science methods and procedures Paweł Kościelniak |
| title_full_unstemmed | Calibration in analytical science methods and procedures Paweł Kościelniak |
| title_short | Calibration in analytical science |
| title_sort | calibration in analytical science methods and procedures |
| title_sub | methods and procedures |
| topic | Kalibrieren Messtechnik (DE-588)4198763-9 gnd Analytische Chemie (DE-588)4129906-1 gnd |
| topic_facet | Kalibrieren Messtechnik Analytische Chemie |
| url | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34846-6/ https://d-nb.info/1267209011/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=034334028&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT koscielniakpaweł calibrationinanalyticalsciencemethodsandprocedures AT wileyvch calibrationinanalyticalsciencemethodsandprocedures |
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