Measurement uncertainty in analysis of plastics: evaluation by interlaboratory test results
Saved in:
| Main Authors: | , , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Munich
Hanser
[2022]
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXIX, 156 Seiten Illustrationen, Diagramme 25 cm |
| ISBN: | 9781569908129 1569908125 |
Staff View
MARC
| LEADER | 00000nam a22000008c 4500 | ||
|---|---|---|---|
| 001 | BV048295219 | ||
| 003 | DE-604 | ||
| 005 | 20221017 | ||
| 007 | t | ||
| 008 | 220622s2022 gw a||| |||| 00||| eng d | ||
| 015 | |a 22,N20 |2 dnb | ||
| 016 | 7 | |a 1257247484 |2 DE-101 | |
| 020 | |a 9781569908129 |c : circa EUR 99.99 (DE) (freier Preis), circa EUR 102.80 (AT) (freier Preis) |9 978-1-56990-812-9 | ||
| 020 | |a 1569908125 |9 1-56990-812-5 | ||
| 024 | 3 | |a 9781569908129 | |
| 028 | 5 | 2 | |a Bestellnummer: 559/00812 |
| 035 | |a (OCoLC)1317832039 | ||
| 035 | |a (DE-599)DNB1257247484 | ||
| 040 | |a DE-604 |b ger | ||
| 041 | 0 | |a eng | |
| 044 | |a gw |c XA-DE | ||
| 049 | |a DE-210 |a DE-91 |a DE-12 |a DE-83 | ||
| 084 | |a ZQ 3115 |0 (DE-625)158039: |2 rvk | ||
| 084 | |8 1\p |a 660 |2 23sdnb | ||
| 084 | |a WER 700 |2 stub | ||
| 100 | 1 | |a Wampfler, Bruno |e Verfasser |0 (DE-588)1261766768 |4 aut | |
| 245 | 1 | 0 | |a Measurement uncertainty in analysis of plastics |b evaluation by interlaboratory test results |c Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid |
| 264 | 1 | |a Munich |b Hanser |c [2022] | |
| 264 | 4 | |c © 2022 | |
| 300 | |a XXIX, 156 Seiten |b Illustrationen, Diagramme |c 25 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Kunststoff |0 (DE-588)4033676-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Messunsicherheit |0 (DE-588)4210374-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Chemische Analyse |0 (DE-588)4009840-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Messung |0 (DE-588)4038852-9 |2 gnd |9 rswk-swf |
| 653 | |a analytical results | ||
| 653 | |a data evaluation | ||
| 653 | |a dispersion of values | ||
| 653 | |a measurement errors | ||
| 653 | |a measurement models | ||
| 653 | |a measurement system design | ||
| 653 | |a standard deviation | ||
| 653 | |a statistical dispersion | ||
| 653 | |a uncertainty analysis | ||
| 653 | |a FBKTANAL: Werkstoffprüfung und Analytik | ||
| 653 | |a PLAS2022 | ||
| 653 | |a plastics technology | ||
| 653 | |a polymers | ||
| 653 | |a testing | ||
| 689 | 0 | 0 | |a Kunststoff |0 (DE-588)4033676-1 |D s |
| 689 | 0 | 1 | |a Chemische Analyse |0 (DE-588)4009840-0 |D s |
| 689 | 0 | 2 | |a Messunsicherheit |0 (DE-588)4210374-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Kunststoff |0 (DE-588)4033676-1 |D s |
| 689 | 1 | 1 | |a Messung |0 (DE-588)4038852-9 |D s |
| 689 | 1 | 2 | |a Messunsicherheit |0 (DE-588)4210374-5 |D s |
| 689 | 1 | |5 DE-604 | |
| 700 | 1 | |a Affolter, Samuel |d 1961- |e Verfasser |0 (DE-588)1261778448 |4 aut | |
| 700 | 1 | |a Ritter, Axel |d 1967- |e Verfasser |0 (DE-588)12156004X |4 aut | |
| 700 | 1 | |a Schmid, Manfred |e Verfasser |4 aut | |
| 710 | 2 | |a Hanser Publications |0 (DE-588)1064064051 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |t Measurement Uncertainty in Analysis of Plastics |b 1. Auflage |d München : Carl Hanser Verlag GmbH & Co. KG, 2022 |h Online-Ressource, 156 Seiten |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe |z 978-1-56990-813-6 |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033675113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-033675113 | ||
| 883 | 1 | |8 1\p |a vlb |d 20220511 |q DE-101 |u https://d-nb.info/provenance/plan#vlb | |
Record in the Search Index
| _version_ | 1804184132065951744 |
|---|---|
| adam_text | CONTENTS
PREFACE
.......................................................................................................
VII
THE
AUTHORS
.............................................................................................
IX
ABOUT
THE
USE
OF THIS
BOOK
....................................................................
XIII
LIST
OF
ABBREVIATIONS
...............................................................................
XVII
EQUATION
SYMBOLS
....................................................................................
XXI
GLOSSARY
..................................................................................................
XXIII
1
INTRODUCTION
TO
MEASUREMENT
UNCERTAINTY
................................
1
1.1
MEASURING
-
WHAT
IS
IT?
..............................................................................
1
1.2
MEASUREMENT
UNCERTAINTY
IN
PLASTICS
TESTING
.........................................
4
1.3
INTERLABORATORY
COMPARISONS
......................................................................
5
1.3.1
TERMS
AND
PARAMETERS
...................................................................
6
1.3.2
CALCULATION
OF
THE
PARAMETERS
.........................................................
8
2
EVALUATION
OF
THE
MEASUREMENT
UNCERTAINTY
.............................
13
2.1
EXPLANATORY
EXAMPLE
..................................................................................
13
2.2
MODELING
APPROACH
ACCORDING
TO
GUM
...................................................
14
2.3
INTERLABORATORY
COMPARISONS
AND
THE
RANDOMNESS
OF
SYSTEMATIC
INFLUENCES
..........................................................................................
16
2.4
EVALUATION
OF
THE
MEASUREMENT
UNCERTAINTY
USING
INTERLABORATORY
COMPARISON
DATA
..............................................................................
19
2.4.1
BASIC
EQUATIONS
...............................................................................
19
2.4.2
ADDITIONAL
COMPONENTS
...................................................................
21
2.4.3
NOTES
REGARDING
THE
SYSTEMATIC
MEASUREMENT
ERROR
(BIAS)
....
22
2.5
CONCLUSION
OF
THE
EXPLANATORY
EXAMPLE
...................................................
23
2.6
CONTRIBUTION
OF
THE
SAMPLING
......................................................................
24
2.6.1
SAMPLING
AND
INTERLABORATORY
COMPARISON
...................................
25
2.6.2
EMPIRICAL
METHOD
.............................................................................
27
2.7
ESTIMATION
ALLOWED!
....................................................................................
28
3
UNCERTAINTY
DATA
IN
PRACTICAL
APPLICATION
..................................
31
3.1
ASSESSMENT
OF
MEASUREMENT
DATA
............................................................
31
3.1.1
INTRODUCTION
.....................................................................................
31
3.1.2
COMPARISON
OF
RESULTS
FROM
DIFFERENT
LABORATORIES
.....................
35
3.1.3
COMPARISON
OF
RESULTS
FROM
THE
SAME
LABORATORY
.......................
39
3.1.3.1
CRITICAL
DIFFERENCE
.............................................................
39
3.1.3.2
REFERENCE
MATERIALS
...........................................................
41
3.1.3.3
FAILURE
ANALYSIS
.................................................................
42
3.1.4
FURTHER
NOTES
ON
THE
EVALUATION
OF
MEASUREMENT
DATA
..............
44
3.2
REPORTING
UNCERTAINTY
................................................................................
45
3.3
EXPLANATIONS
TO
THE
PRECISION
DATA
PRESENTED
IN
THE
FOLLOWING
CHAPTERS
.......................................................................................................
46
4
THERMAL
ANALYSIS
..............................................................................
53
4.1
DIFFERENTIAL
SCANNING
CALORIMETRY
(DSC)
.................................................
53
4.1.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
53
4.1.2
INTERLABORATORY
COMPARISONS
-
SUMMARY
.....................................
55
4.1.3
GLASS
TRANSITION
TEMPERATURE
T
G
....................................................
56
4.1.4
CHANGE
OF
THE
SPECIFIC
HEAT
CAPACITY
AC
P
.....................................
59
4.1.5
CRYSTALLINITY
AND
MELTING
CHARACTERISTICS
OF
THERMOPLASTICS
...
60
4.1.6
CURING
REACTION
OF
EPOXY
RESINS
...................................................
61
4.2
OXIDATIVE
INDUCTION
TIME
AND
TEMPERATURE
.............................................
62
4.2.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
62
4.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.......................................
64
4.3
THERMOGRAVIMETRY
(TGA)
............................................................................
66
4.3.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
66
4.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
-
SUMMARY
...................
67
4.3.3
CONTENT
OF
PLASTICIZER
.......................................................................
68
4.3.4
CONTENT
OF
CARBON
BLACK
.................................................................
69
4.3.5
ASH
CONTENT
.....................................................................................
69
4.4
DYNAMIC
MECHANICAL
ANALYSIS
(DMA)
.....................................................
70
4.4.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
70
4.4.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.......................................
72
4.5
EXAMPLES
OF
THERMAL
ANALYSIS
.................................................................
75
4.5.1
ADHESIVES:
COMPARISON
OF
TWO
SAMPLES
......................................
75
4.5.2
OIT:
COMPARISON
OF
THE
VALUES
OF
TWO
LABORATORIES
.....................
79
5
DETERMINATION
OF
THE
MOLECULAR
WEIGHT
......................................
83
5.1
SIZE
EXCLUSION
CHROMATOGRAPHY
(SEC)
.....................................................
83
5.1.1
PRINCIPLE
OF
MEASUREMENT
..............................................................
83
5.1.2
SEC
IN
ORGANIC
PHASE
....................................................................
85
5.1.3
SEC
IN
AQUEOUS
PHASE
....................................................................
87
5.1.4
HIGH
TEMPERATURE
SEC
..................................................................
87
5.1.5
POLYDISPERSITY
..................................................................................
88
5.2
MELT
MASS-FLOW
RATE
(MFR)
..........................................
88
5.2.1
PRINCIPLE
OF
MEASUREMENT
..............................................................
88
5.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
......................................
89
5.3
SOLUTION
VISCOSITY
.......................................................................................
90
5.3.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
90
5.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
......................................
91
5.4
EXAMPLES
TO
THE
DETERMINATION
OF
THE
MOLECULAR
WEIGHT
......................
92
5.4.1
MFR:
TESTING
THE
SAMPLE
FOR
SPECIFICATION
AND
INHOMOGENEITY
.
92
5.4.2
INTRINSIC
VISCOSITY
[Q]
-
ESTIMATION
OF
THE
STANDARD
UNCERTAINTY
94
6
QUANTIFICATION
OF
MAIN
AND
SECONDARY
COMPONENTS
...............
99
6.1
ELEMENTS
.......................................................................................................
99
6.1.1
HALOGENS
...........................................................................................
99
6.1.1.1
PRINCIPLE
OF
MEASUREMENT
.................................................
100
6.1.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
..........................
101
6.1.2
SULFUR
.................................................................................................
101
6.1.2.1
PRINCIPLE
OF
MEASUREMENT
.................................................
102
6.1.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
..........................
102
6.1.3
NITROGEN
...........................................................................................
103
6.1.3.1
PRINCIPLE
OF
MEASUREMENT
.................................................
103
6.1.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
..........................
103
6.2
COMPOUNDS
..................................................................................................
104
6.2.1
PLASTICIZER
.........................................................................................
104
6.2.1.1
PRINCIPLE
OF
MEASUREMENT
.................................................
104
6.2.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
...........................
105
6.2.2
VINYL
ACETATE
CONTENT
IN
ETHYLENE-VINYL
ACETATE
COPOLYMERS
..
106
6.2.2.1
PRINCIPLE
OF
MEASUREMENT
.................................................
106
6.2.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
...........................
107
6.2.3
WATER
.................................................................................................
108
6.2.3.1
PRINCIPLE
OF
MEASUREMENT
.................................................
108
6.2.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
..........................
109
6.3
ASH
................................................................................................................
110
6.3.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
110
6.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.......................................
110
6.4
EXAMPLES
FOR
QUANTITATIVE
DETERMINATION
.............................................................................................
112
6.4.1
PLASTICIZER:
EXTRACTION
VERSUS
TGA
.................................................
112
6.4.2
BROMINE:
XRF
VERSUS
TITRIMETRY
...................................................
114
7
QUANTIFICATION
OF
TRACE
COMPONENTS
...........................................
119
7.1
ELEMENTS:
METALLOIDS,
HEAVY
METALS
AND
BROMINE
..................................
119
7.1.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
119
7.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.......................................
121
7.2
STABILIZERS
....................................................................................................
124
7.2.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
125
7.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.......................................
127
7.3
RESIDUAL
SOLVENTS
........................................................................................
129
7.3.1
PRINCIPLE
OF
MEASUREMENT
...............................................................
129
7.3.2
SAMPLE
PREPARATION
.........................................................................
130
7.3.3
RESULTS
OF
INTERLABORATORY
COMPARISONS
........................................
131
7.4
EXAMPLES
OF
QUANTITATIVE
TRACE
ANALYSIS
...................................................
132
7.4.1
CORRECTION
OF
THE
LEAD
CONTENT
.......................................................
132
7.4.2
MINI-INTERLABORATORY
TEST
(THREE
PARTICIPANTS)
..............................
134
8
SUMMARY
...........................................................................................
139
8.1
DATA
OVERVIEW
..............................................................................................
140
8.2
REPRODUCIBILITY
PRECISION
............................................................................
143
8.3
REPEATABILITY
PRECISION
................................................................................
144
8.4
BETWEEN-LABORATORY
EFFECTS
........................................................................
145
8.5
REPORTINGUNCERTAINTY
................................................................................
147
INDEX
..........................................................................................................
149
|
| adam_txt |
CONTENTS
PREFACE
.
VII
THE
AUTHORS
.
IX
ABOUT
THE
USE
OF THIS
BOOK
.
XIII
LIST
OF
ABBREVIATIONS
.
XVII
EQUATION
SYMBOLS
.
XXI
GLOSSARY
.
XXIII
1
INTRODUCTION
TO
MEASUREMENT
UNCERTAINTY
.
1
1.1
MEASURING
-
WHAT
IS
IT?
.
1
1.2
MEASUREMENT
UNCERTAINTY
IN
PLASTICS
TESTING
.
4
1.3
INTERLABORATORY
COMPARISONS
.
5
1.3.1
TERMS
AND
PARAMETERS
.
6
1.3.2
CALCULATION
OF
THE
PARAMETERS
.
8
2
EVALUATION
OF
THE
MEASUREMENT
UNCERTAINTY
.
13
2.1
EXPLANATORY
EXAMPLE
.
13
2.2
MODELING
APPROACH
ACCORDING
TO
GUM
.
14
2.3
INTERLABORATORY
COMPARISONS
AND
THE
RANDOMNESS
OF
SYSTEMATIC
INFLUENCES
.
16
2.4
EVALUATION
OF
THE
MEASUREMENT
UNCERTAINTY
USING
INTERLABORATORY
COMPARISON
DATA
.
19
2.4.1
BASIC
EQUATIONS
.
19
2.4.2
ADDITIONAL
COMPONENTS
.
21
2.4.3
NOTES
REGARDING
THE
SYSTEMATIC
MEASUREMENT
ERROR
(BIAS)
.
22
2.5
CONCLUSION
OF
THE
EXPLANATORY
EXAMPLE
.
23
2.6
CONTRIBUTION
OF
THE
SAMPLING
.
24
2.6.1
SAMPLING
AND
INTERLABORATORY
COMPARISON
.
25
2.6.2
EMPIRICAL
METHOD
.
27
2.7
ESTIMATION
ALLOWED!
.
28
3
UNCERTAINTY
DATA
IN
PRACTICAL
APPLICATION
.
31
3.1
ASSESSMENT
OF
MEASUREMENT
DATA
.
31
3.1.1
INTRODUCTION
.
31
3.1.2
COMPARISON
OF
RESULTS
FROM
DIFFERENT
LABORATORIES
.
35
3.1.3
COMPARISON
OF
RESULTS
FROM
THE
SAME
LABORATORY
.
39
3.1.3.1
CRITICAL
DIFFERENCE
.
39
3.1.3.2
REFERENCE
MATERIALS
.
41
3.1.3.3
FAILURE
ANALYSIS
.
42
3.1.4
FURTHER
NOTES
ON
THE
EVALUATION
OF
MEASUREMENT
DATA
.
44
3.2
REPORTING
UNCERTAINTY
.
45
3.3
EXPLANATIONS
TO
THE
PRECISION
DATA
PRESENTED
IN
THE
FOLLOWING
CHAPTERS
.
46
4
THERMAL
ANALYSIS
.
53
4.1
DIFFERENTIAL
SCANNING
CALORIMETRY
(DSC)
.
53
4.1.1
PRINCIPLE
OF
MEASUREMENT
.
53
4.1.2
INTERLABORATORY
COMPARISONS
-
SUMMARY
.
55
4.1.3
GLASS
TRANSITION
TEMPERATURE
T
G
.
56
4.1.4
CHANGE
OF
THE
SPECIFIC
HEAT
CAPACITY
AC
P
.
59
4.1.5
CRYSTALLINITY
AND
MELTING
CHARACTERISTICS
OF
THERMOPLASTICS
.
60
4.1.6
CURING
REACTION
OF
EPOXY
RESINS
.
61
4.2
OXIDATIVE
INDUCTION
TIME
AND
TEMPERATURE
.
62
4.2.1
PRINCIPLE
OF
MEASUREMENT
.
62
4.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
64
4.3
THERMOGRAVIMETRY
(TGA)
.
66
4.3.1
PRINCIPLE
OF
MEASUREMENT
.
66
4.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
-
SUMMARY
.
67
4.3.3
CONTENT
OF
PLASTICIZER
.
68
4.3.4
CONTENT
OF
CARBON
BLACK
.
69
4.3.5
ASH
CONTENT
.
69
4.4
DYNAMIC
MECHANICAL
ANALYSIS
(DMA)
.
70
4.4.1
PRINCIPLE
OF
MEASUREMENT
.
70
4.4.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
72
4.5
EXAMPLES
OF
THERMAL
ANALYSIS
.
75
4.5.1
ADHESIVES:
COMPARISON
OF
TWO
SAMPLES
.
75
4.5.2
OIT:
COMPARISON
OF
THE
VALUES
OF
TWO
LABORATORIES
.
79
5
DETERMINATION
OF
THE
MOLECULAR
WEIGHT
.
83
5.1
SIZE
EXCLUSION
CHROMATOGRAPHY
(SEC)
.
83
5.1.1
PRINCIPLE
OF
MEASUREMENT
.
83
5.1.2
SEC
IN
ORGANIC
PHASE
.
85
5.1.3
SEC
IN
AQUEOUS
PHASE
.
87
5.1.4
HIGH
TEMPERATURE
SEC
.
87
5.1.5
POLYDISPERSITY
.
88
5.2
MELT
MASS-FLOW
RATE
(MFR)
.
88
5.2.1
PRINCIPLE
OF
MEASUREMENT
.
88
5.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
89
5.3
SOLUTION
VISCOSITY
.
90
5.3.1
PRINCIPLE
OF
MEASUREMENT
.
90
5.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
91
5.4
EXAMPLES
TO
THE
DETERMINATION
OF
THE
MOLECULAR
WEIGHT
.
92
5.4.1
MFR:
TESTING
THE
SAMPLE
FOR
SPECIFICATION
AND
INHOMOGENEITY
.
92
5.4.2
INTRINSIC
VISCOSITY
[Q]
-
ESTIMATION
OF
THE
STANDARD
UNCERTAINTY
94
6
QUANTIFICATION
OF
MAIN
AND
SECONDARY
COMPONENTS
.
99
6.1
ELEMENTS
.
99
6.1.1
HALOGENS
.
99
6.1.1.1
PRINCIPLE
OF
MEASUREMENT
.
100
6.1.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
101
6.1.2
SULFUR
.
101
6.1.2.1
PRINCIPLE
OF
MEASUREMENT
.
102
6.1.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
102
6.1.3
NITROGEN
.
103
6.1.3.1
PRINCIPLE
OF
MEASUREMENT
.
103
6.1.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
103
6.2
COMPOUNDS
.
104
6.2.1
PLASTICIZER
.
104
6.2.1.1
PRINCIPLE
OF
MEASUREMENT
.
104
6.2.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
105
6.2.2
VINYL
ACETATE
CONTENT
IN
ETHYLENE-VINYL
ACETATE
COPOLYMERS
.
106
6.2.2.1
PRINCIPLE
OF
MEASUREMENT
.
106
6.2.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
107
6.2.3
WATER
.
108
6.2.3.1
PRINCIPLE
OF
MEASUREMENT
.
108
6.2.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
109
6.3
ASH
.
110
6.3.1
PRINCIPLE
OF
MEASUREMENT
.
110
6.3.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
110
6.4
EXAMPLES
FOR
QUANTITATIVE
DETERMINATION
.
112
6.4.1
PLASTICIZER:
EXTRACTION
VERSUS
TGA
.
112
6.4.2
BROMINE:
XRF
VERSUS
TITRIMETRY
.
114
7
QUANTIFICATION
OF
TRACE
COMPONENTS
.
119
7.1
ELEMENTS:
METALLOIDS,
HEAVY
METALS
AND
BROMINE
.
119
7.1.1
PRINCIPLE
OF
MEASUREMENT
.
119
7.1.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
121
7.2
STABILIZERS
.
124
7.2.1
PRINCIPLE
OF
MEASUREMENT
.
125
7.2.2
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
127
7.3
RESIDUAL
SOLVENTS
.
129
7.3.1
PRINCIPLE
OF
MEASUREMENT
.
129
7.3.2
SAMPLE
PREPARATION
.
130
7.3.3
RESULTS
OF
INTERLABORATORY
COMPARISONS
.
131
7.4
EXAMPLES
OF
QUANTITATIVE
TRACE
ANALYSIS
.
132
7.4.1
CORRECTION
OF
THE
LEAD
CONTENT
.
132
7.4.2
MINI-INTERLABORATORY
TEST
(THREE
PARTICIPANTS)
.
134
8
SUMMARY
.
139
8.1
DATA
OVERVIEW
.
140
8.2
REPRODUCIBILITY
PRECISION
.
143
8.3
REPEATABILITY
PRECISION
.
144
8.4
BETWEEN-LABORATORY
EFFECTS
.
145
8.5
REPORTINGUNCERTAINTY
.
147
INDEX
.
149 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Wampfler, Bruno Affolter, Samuel 1961- Ritter, Axel 1967- Schmid, Manfred |
| author_GND | (DE-588)1261766768 (DE-588)1261778448 (DE-588)12156004X |
| author_facet | Wampfler, Bruno Affolter, Samuel 1961- Ritter, Axel 1967- Schmid, Manfred |
| author_role | aut aut aut aut |
| author_sort | Wampfler, Bruno |
| author_variant | b w bw s a sa a r ar m s ms |
| building | Verbundindex |
| bvnumber | BV048295219 |
| classification_rvk | ZQ 3115 |
| classification_tum | WER 700 |
| ctrlnum | (OCoLC)1317832039 (DE-599)DNB1257247484 |
| discipline | Werkstoffwissenschaften Mess-/Steuerungs-/Regelungs-/Automatisierungstechnik / Mechatronik |
| discipline_str_mv | Werkstoffwissenschaften Mess-/Steuerungs-/Regelungs-/Automatisierungstechnik / Mechatronik |
| format | Book |
| fullrecord | <?xml version="1.0" encoding="UTF-8"?><collection xmlns="http://www.loc.gov/MARC21/slim"><record><leader>03228nam a22007818c 4500</leader><controlfield tag="001">BV048295219</controlfield><controlfield tag="003">DE-604</controlfield><controlfield tag="005">20221017 </controlfield><controlfield tag="007">t</controlfield><controlfield tag="008">220622s2022 gw a||| |||| 00||| eng d</controlfield><datafield tag="015" ind1=" " ind2=" "><subfield code="a">22,N20</subfield><subfield code="2">dnb</subfield></datafield><datafield tag="016" ind1="7" ind2=" "><subfield code="a">1257247484</subfield><subfield code="2">DE-101</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">9781569908129</subfield><subfield code="c">: circa EUR 99.99 (DE) (freier Preis), circa EUR 102.80 (AT) (freier Preis)</subfield><subfield code="9">978-1-56990-812-9</subfield></datafield><datafield tag="020" ind1=" " ind2=" "><subfield code="a">1569908125</subfield><subfield code="9">1-56990-812-5</subfield></datafield><datafield tag="024" ind1="3" ind2=" "><subfield code="a">9781569908129</subfield></datafield><datafield tag="028" ind1="5" ind2="2"><subfield code="a">Bestellnummer: 559/00812</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(OCoLC)1317832039</subfield></datafield><datafield tag="035" ind1=" " ind2=" "><subfield code="a">(DE-599)DNB1257247484</subfield></datafield><datafield tag="040" ind1=" " ind2=" "><subfield code="a">DE-604</subfield><subfield code="b">ger</subfield></datafield><datafield tag="041" ind1="0" ind2=" "><subfield code="a">eng</subfield></datafield><datafield tag="044" ind1=" " ind2=" "><subfield code="a">gw</subfield><subfield code="c">XA-DE</subfield></datafield><datafield tag="049" ind1=" " ind2=" "><subfield code="a">DE-210</subfield><subfield code="a">DE-91</subfield><subfield code="a">DE-12</subfield><subfield code="a">DE-83</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">ZQ 3115</subfield><subfield code="0">(DE-625)158039:</subfield><subfield code="2">rvk</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="8">1\p</subfield><subfield code="a">660</subfield><subfield code="2">23sdnb</subfield></datafield><datafield tag="084" ind1=" " ind2=" "><subfield code="a">WER 700</subfield><subfield code="2">stub</subfield></datafield><datafield tag="100" ind1="1" ind2=" "><subfield code="a">Wampfler, Bruno</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)1261766768</subfield><subfield code="4">aut</subfield></datafield><datafield tag="245" ind1="1" ind2="0"><subfield code="a">Measurement uncertainty in analysis of plastics</subfield><subfield code="b">evaluation by interlaboratory test results</subfield><subfield code="c">Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid</subfield></datafield><datafield tag="264" ind1=" " ind2="1"><subfield code="a">Munich</subfield><subfield code="b">Hanser</subfield><subfield code="c">[2022]</subfield></datafield><datafield tag="264" ind1=" " ind2="4"><subfield code="c">© 2022</subfield></datafield><datafield tag="300" ind1=" " ind2=" "><subfield code="a">XXIX, 156 Seiten</subfield><subfield code="b">Illustrationen, Diagramme</subfield><subfield code="c">25 cm</subfield></datafield><datafield tag="336" ind1=" " ind2=" "><subfield code="b">txt</subfield><subfield code="2">rdacontent</subfield></datafield><datafield tag="337" ind1=" " ind2=" "><subfield code="b">n</subfield><subfield code="2">rdamedia</subfield></datafield><datafield tag="338" ind1=" " ind2=" "><subfield code="b">nc</subfield><subfield code="2">rdacarrier</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Kunststoff</subfield><subfield code="0">(DE-588)4033676-1</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Messunsicherheit</subfield><subfield code="0">(DE-588)4210374-5</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Chemische Analyse</subfield><subfield code="0">(DE-588)4009840-0</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="650" ind1="0" ind2="7"><subfield code="a">Messung</subfield><subfield code="0">(DE-588)4038852-9</subfield><subfield code="2">gnd</subfield><subfield code="9">rswk-swf</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">analytical results</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">data evaluation</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">dispersion of values</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">measurement errors</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">measurement models</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">measurement system design</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">standard deviation</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">statistical dispersion</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">uncertainty analysis</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">FBKTANAL: Werkstoffprüfung und Analytik</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">PLAS2022</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">plastics technology</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">polymers</subfield></datafield><datafield tag="653" ind1=" " ind2=" "><subfield code="a">testing</subfield></datafield><datafield tag="689" ind1="0" ind2="0"><subfield code="a">Kunststoff</subfield><subfield code="0">(DE-588)4033676-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="1"><subfield code="a">Chemische Analyse</subfield><subfield code="0">(DE-588)4009840-0</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2="2"><subfield code="a">Messunsicherheit</subfield><subfield code="0">(DE-588)4210374-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="0" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="689" ind1="1" ind2="0"><subfield code="a">Kunststoff</subfield><subfield code="0">(DE-588)4033676-1</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="1"><subfield code="a">Messung</subfield><subfield code="0">(DE-588)4038852-9</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2="2"><subfield code="a">Messunsicherheit</subfield><subfield code="0">(DE-588)4210374-5</subfield><subfield code="D">s</subfield></datafield><datafield tag="689" ind1="1" ind2=" "><subfield code="5">DE-604</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Affolter, Samuel</subfield><subfield code="d">1961-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)1261778448</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Ritter, Axel</subfield><subfield code="d">1967-</subfield><subfield code="e">Verfasser</subfield><subfield code="0">(DE-588)12156004X</subfield><subfield code="4">aut</subfield></datafield><datafield tag="700" ind1="1" ind2=" "><subfield code="a">Schmid, Manfred</subfield><subfield code="e">Verfasser</subfield><subfield code="4">aut</subfield></datafield><datafield tag="710" ind1="2" ind2=" "><subfield code="a">Hanser Publications</subfield><subfield code="0">(DE-588)1064064051</subfield><subfield code="4">pbl</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe</subfield><subfield code="t">Measurement Uncertainty in Analysis of Plastics</subfield><subfield code="b">1. Auflage</subfield><subfield code="d">München : Carl Hanser Verlag GmbH & Co. KG, 2022</subfield><subfield code="h">Online-Ressource, 156 Seiten</subfield></datafield><datafield tag="776" ind1="0" ind2="8"><subfield code="i">Erscheint auch als</subfield><subfield code="n">Online-Ausgabe</subfield><subfield code="z">978-1-56990-813-6</subfield></datafield><datafield tag="856" ind1="4" ind2="2"><subfield code="m">DNB Datenaustausch</subfield><subfield code="q">application/pdf</subfield><subfield code="u">http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033675113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA</subfield><subfield code="3">Inhaltsverzeichnis</subfield></datafield><datafield tag="999" ind1=" " ind2=" "><subfield code="a">oai:aleph.bib-bvb.de:BVB01-033675113</subfield></datafield><datafield tag="883" ind1="1" ind2=" "><subfield code="8">1\p</subfield><subfield code="a">vlb</subfield><subfield code="d">20220511</subfield><subfield code="q">DE-101</subfield><subfield code="u">https://d-nb.info/provenance/plan#vlb</subfield></datafield></record></collection> |
| id | DE-604.BV048295219 |
| illustrated | Illustrated |
| index_date | 2024-07-03T20:04:54Z |
| indexdate | 2024-07-10T09:34:28Z |
| institution | BVB |
| institution_GND | (DE-588)1064064051 |
| isbn | 9781569908129 1569908125 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033675113 |
| oclc_num | 1317832039 |
| open_access_boolean | |
| owner | DE-210 DE-91 DE-BY-TUM DE-12 DE-83 |
| owner_facet | DE-210 DE-91 DE-BY-TUM DE-12 DE-83 |
| physical | XXIX, 156 Seiten Illustrationen, Diagramme 25 cm |
| publishDate | 2022 |
| publishDateSearch | 2022 |
| publishDateSort | 2022 |
| publisher | Hanser |
| record_format | marc |
| spelling | Wampfler, Bruno Verfasser (DE-588)1261766768 aut Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid Munich Hanser [2022] © 2022 XXIX, 156 Seiten Illustrationen, Diagramme 25 cm txt rdacontent n rdamedia nc rdacarrier Kunststoff (DE-588)4033676-1 gnd rswk-swf Messunsicherheit (DE-588)4210374-5 gnd rswk-swf Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Messung (DE-588)4038852-9 gnd rswk-swf analytical results data evaluation dispersion of values measurement errors measurement models measurement system design standard deviation statistical dispersion uncertainty analysis FBKTANAL: Werkstoffprüfung und Analytik PLAS2022 plastics technology polymers testing Kunststoff (DE-588)4033676-1 s Chemische Analyse (DE-588)4009840-0 s Messunsicherheit (DE-588)4210374-5 s DE-604 Messung (DE-588)4038852-9 s Affolter, Samuel 1961- Verfasser (DE-588)1261778448 aut Ritter, Axel 1967- Verfasser (DE-588)12156004X aut Schmid, Manfred Verfasser aut Hanser Publications (DE-588)1064064051 pbl Erscheint auch als Online-Ausgabe Measurement Uncertainty in Analysis of Plastics 1. Auflage München : Carl Hanser Verlag GmbH & Co. KG, 2022 Online-Ressource, 156 Seiten Erscheint auch als Online-Ausgabe 978-1-56990-813-6 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033675113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20220511 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Wampfler, Bruno Affolter, Samuel 1961- Ritter, Axel 1967- Schmid, Manfred Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results Kunststoff (DE-588)4033676-1 gnd Messunsicherheit (DE-588)4210374-5 gnd Chemische Analyse (DE-588)4009840-0 gnd Messung (DE-588)4038852-9 gnd |
| subject_GND | (DE-588)4033676-1 (DE-588)4210374-5 (DE-588)4009840-0 (DE-588)4038852-9 |
| title | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results |
| title_auth | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results |
| title_exact_search | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results |
| title_exact_search_txtP | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results |
| title_full | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid |
| title_fullStr | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid |
| title_full_unstemmed | Measurement uncertainty in analysis of plastics evaluation by interlaboratory test results Bruno Wampfler, Samuel Affolter, Axel Ritter, Manfred Schmid |
| title_short | Measurement uncertainty in analysis of plastics |
| title_sort | measurement uncertainty in analysis of plastics evaluation by interlaboratory test results |
| title_sub | evaluation by interlaboratory test results |
| topic | Kunststoff (DE-588)4033676-1 gnd Messunsicherheit (DE-588)4210374-5 gnd Chemische Analyse (DE-588)4009840-0 gnd Messung (DE-588)4038852-9 gnd |
| topic_facet | Kunststoff Messunsicherheit Chemische Analyse Messung |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033675113&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT wampflerbruno measurementuncertaintyinanalysisofplasticsevaluationbyinterlaboratorytestresults AT affoltersamuel measurementuncertaintyinanalysisofplasticsevaluationbyinterlaboratorytestresults AT ritteraxel measurementuncertaintyinanalysisofplasticsevaluationbyinterlaboratorytestresults AT schmidmanfred measurementuncertaintyinanalysisofplasticsevaluationbyinterlaboratorytestresults AT hanserpublications measurementuncertaintyinanalysisofplasticsevaluationbyinterlaboratorytestresults |