Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Berlin
[2021?]
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Item Description: | Tag der mündlichen Prüfung: 03.12.2021 |
| Physical Description: | viii, 209 Seiten Illustrationen, Diagramme (farbig) |
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MARC
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| 100 | 1 | |a Hein, Dennis Matthias |e Verfasser |0 (DE-588)1260385647 |4 aut | |
| 245 | 1 | 0 | |a Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |c von Dennis Matthias Hein |
| 264 | 1 | |a Berlin |c [2021?] | |
| 300 | |a viii, 209 Seiten |b Illustrationen, Diagramme (farbig) | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 500 | |a Tag der mündlichen Prüfung: 03.12.2021 | ||
| 502 | |b Dissertation |c Humboldt-Universität Berlin |d 2021 | ||
| 546 | |a Zusammenfassung englisch und deutsch | ||
| 650 | 0 | 7 | |a Photoelektronenspektroskopie |0 (DE-588)4174491-3 |2 gnd |9 rswk-swf |
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| 689 | 0 | 2 | |a Edelmetall |0 (DE-588)4013531-7 |D s |
| 689 | 0 | |5 DE-604 | |
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| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-033670790 | |
Record in the Search Index
| _version_ | 1814162805152022528 |
|---|---|
| adam_text |
CONTENT
ABSTRACT
.
I
ZUSAMMENFASSUNG
.
III
LIST
OF
ABBREVIATIONS
.
V
CONTENT
.
VII
1
INTRODUCTION
AND
MOTIVATION
.
1
1.1
THESIS
OUTLINE
.
6
2
X-RAY
PHOTOELECTRON
SPECTROSCOPY
AND
ABSORPTION
.
9
2.1
X-RAY
RADIATION
AND
ABSORPTION
.
9
2.2
PHOTOIONIZATION
PROCESS
.
11
2.3
PHOTOELECTRON
DETECTION
.
13
2.4
AUGER-ELECTRON
AND
RESONANT
PHOTOELECTRON
SPECTROSCOPY
.
15
2.5
X-RAY
FLUORESCENCE
.
20
3
EXPERIMENTAL
METHODS
.
23
3.1
CHALLENGES
TO
STUDY
SOLID-LIQUID
INTERFACES
WITH
XPS
.
23
3.2
SOL
3
PES
.
26
3.2.1
ELECTRON
ENERGY
ANALYZER:
SCIENTAOMICRON
R4000
HIPP-2
.27
3.2.2
DIFFERENTIAL
PUMPING
STAGE
.
29
3.2.3
INTERACTION
CHAMBER
.30
3.2.4
EASI
EXPERIMENTAL
SETUP
.
32
3.3
LIQUID
JET
XPS
.
33
3.4
NEAR-AMBIENT
PRESSURE
XPS
OF
ADSORBED
FHO-SOLID
INTERFACE
.36
3.5
OPERANDO
FLOW-CELL
-
FREE-STANDING
GRAPHENE
ON
SI3N4
.39
3.5.1
GRAPHENE
HARVESTING
.42
3.5.2
FLOW-CELL
ALIGNMENT
IN
THE
SOL
3
PES
INTERACTION
CHAMBER
.47
3.6
TFY
AND
TEY
MEASUREMENTS
WITH
THE
LIXEDROM
SETUP
.48
3.7
SYNCHROTRON
LIGHT
SOURCE
AND
BEAMLINES
.
50
3.7.1
BESSY
II
AND
UNDULATOR
U49/2
.
50
3.7.2
BEAMLINES
U49/2-PGM
1
AND
P04
XUV
.
51
4
ADDITIONAL
CHARACTERIZATION
METHODS
.
55
4.1
ELECTROCHEMICAL
CHARACTERIZATION:
CYCLOVOLTAMMETRY
.
55
4.2
SCANNING
ELECTRON
MICROSCOPY
AND
ENERGY
DISPERSIVE
X-RAY
ANALYSIS
.
58
4.3
DYNAMIC
LIGHT
SCATTERING
AND
LASER
DOPPLER
VELOCIMETRY
.60
5
WATER-INDUCED
REVERSIBLE
PHASE
CHANGE
OF
COO
X
NANOPARTICLES
.
63
5.1
COBALT
OXIDE
AS
A
CATALYST
.
63
5.2
PREPARATION
OF
COO
X
NPS
ON
SI(
111)
.66
5.3
PEY-XAS
UNDER
HIGH
VACUUM
AND
NEAR-AMBIENT
PRESSURE
CONDITIONS
.67
5.3.1
HIGH
VACUUM
.68
5.3.2
NAP
CONDITIONS
.69
5.4
RESONANT
AUGER
SPECTRA
UNDER
NEAR-AMBIENT
PRESSURE
CONDITIONS
.
71
5.4.1
NEAR
AMBIENT
PRESSURE
XPS
OF
SIO
X
/SI(
111)
.
72
5.5
RESONANT-PES
AT
HIGH
VACUUM
VERSUS
NEAR-AMBIENT
PRESSURE
.
75
5.5.1
X-RAY
RADIATION
EFFECTS
AND
SAMPLE
CONTAMINATION
.77
6
NICKEL-FERRITE
NANOPARTICLES
AS
A
PROMISING
OER
CATALYST
.
81
6.1
CHARACTERIZATION
OF
NICKEL-FERRITE
NPS
-
XRD,
RAMAN
AND
TEM
.
85
6.2
PEY-XAS
AND
XPS
OF
NICKEL-FERRITE
NPS
.90
6.3
LIQUID
MICROJET
XPS
OF
STABILIZED
NICKEL-FERRITE
NPS
-
RESULTS
AND
LIMITATIONS
.
99
6.3.1
STABILIZATION
OF
THE
NANOPARTICLE
SUSPENSION
-
ZETA
POTENTIAL,
PARTICLE
SIZE
.99
6.3.2
LIQUID
MICROJET
XPS
-
FE
AND
NI
LA-EDGE
AND
RESONANT
XPS
.
103
6.3.3
LIQUID-MICROJET
XPS
AT
THE
OXYGEN
K-EDGE
.
109
6.4
WATER-INDUCED
FORMATION
OF
FE
2+
ON
THE
SURFACE
OF
NICKEL-FERRITE
NPS
.
112
6.4.1
IRON
LA-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
112
6.4.2
NICKEL
LA-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
118
6.4.3
NEAR
AMBIENT
PRESSURE
XPS
-
CIS
AND
O
IS
.
120
6.4.4
OXYGEN
K-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
122
6.5
CATALYTIC
OER
ACTIVITY
OF
NICKEL-FERRITE
NPS
.
127
6.6
OPERANDO
PHOTON-IN
PHOTON-OUT
SPECTROSCOPY
-
THE
WAY
TO
GO?
.
131
7
OPERANDO
(RESONANT)
PHOTOELECTRON
SPECTROSCOPY
-
ROADMAP
AND
LIMITATIONS
.
137
7.1
IN-SITU
ELECTROCHEMICAL
DEPOSITION
AND
CHARACTERIZATION
OF
FENI
X
O
Y
.
138
7.2
OPERANDO
OXYGEN
EVOLUTION
REACTION
VERSUS
GRAPHENE
OXIDATION
.
146
7.3
ALTERNATIVE
FLOW-CELL
CONCEPT
-
THE
IONOMER
APPROACH
.
154
8
SUMMARY
AND
OUTLOOK
.
159
8.1
UPCOMING
PROJECTS
.
161
8.2
PROJECTS
BEYOND
THE
SCOPE
OF
MY
DOCTORAL
PROJECT
.
163
9
REFERENCE
.
165
10
APPENDIX
.
197
PUBLICATIONS
.205
ACKNOWLEDGEMENTS
.
207
SELBSTANDIGKEITSERKLARUNG
GEMAB
§
7
ABSATZ
4
.
209
VIII |
| adam_txt |
CONTENT
ABSTRACT
.
I
ZUSAMMENFASSUNG
.
III
LIST
OF
ABBREVIATIONS
.
V
CONTENT
.
VII
1
INTRODUCTION
AND
MOTIVATION
.
1
1.1
THESIS
OUTLINE
.
6
2
X-RAY
PHOTOELECTRON
SPECTROSCOPY
AND
ABSORPTION
.
9
2.1
X-RAY
RADIATION
AND
ABSORPTION
.
9
2.2
PHOTOIONIZATION
PROCESS
.
11
2.3
PHOTOELECTRON
DETECTION
.
13
2.4
AUGER-ELECTRON
AND
RESONANT
PHOTOELECTRON
SPECTROSCOPY
.
15
2.5
X-RAY
FLUORESCENCE
.
20
3
EXPERIMENTAL
METHODS
.
23
3.1
CHALLENGES
TO
STUDY
SOLID-LIQUID
INTERFACES
WITH
XPS
.
23
3.2
SOL
3
PES
.
26
3.2.1
ELECTRON
ENERGY
ANALYZER:
SCIENTAOMICRON
R4000
HIPP-2
.27
3.2.2
DIFFERENTIAL
PUMPING
STAGE
.
29
3.2.3
INTERACTION
CHAMBER
.30
3.2.4
EASI
EXPERIMENTAL
SETUP
.
32
3.3
LIQUID
JET
XPS
.
33
3.4
NEAR-AMBIENT
PRESSURE
XPS
OF
ADSORBED
FHO-SOLID
INTERFACE
.36
3.5
OPERANDO
FLOW-CELL
-
FREE-STANDING
GRAPHENE
ON
SI3N4
.39
3.5.1
GRAPHENE
HARVESTING
.42
3.5.2
FLOW-CELL
ALIGNMENT
IN
THE
SOL
3
PES
INTERACTION
CHAMBER
.47
3.6
TFY
AND
TEY
MEASUREMENTS
WITH
THE
LIXEDROM
SETUP
.48
3.7
SYNCHROTRON
LIGHT
SOURCE
AND
BEAMLINES
.
50
3.7.1
BESSY
II
AND
UNDULATOR
U49/2
.
50
3.7.2
BEAMLINES
U49/2-PGM
1
AND
P04
XUV
.
51
4
ADDITIONAL
CHARACTERIZATION
METHODS
.
55
4.1
ELECTROCHEMICAL
CHARACTERIZATION:
CYCLOVOLTAMMETRY
.
55
4.2
SCANNING
ELECTRON
MICROSCOPY
AND
ENERGY
DISPERSIVE
X-RAY
ANALYSIS
.
58
4.3
DYNAMIC
LIGHT
SCATTERING
AND
LASER
DOPPLER
VELOCIMETRY
.60
5
WATER-INDUCED
REVERSIBLE
PHASE
CHANGE
OF
COO
X
NANOPARTICLES
.
63
5.1
COBALT
OXIDE
AS
A
CATALYST
.
63
5.2
PREPARATION
OF
COO
X
NPS
ON
SI(
111)
.66
5.3
PEY-XAS
UNDER
HIGH
VACUUM
AND
NEAR-AMBIENT
PRESSURE
CONDITIONS
.67
5.3.1
HIGH
VACUUM
.68
5.3.2
NAP
CONDITIONS
.69
5.4
RESONANT
AUGER
SPECTRA
UNDER
NEAR-AMBIENT
PRESSURE
CONDITIONS
.
71
5.4.1
NEAR
AMBIENT
PRESSURE
XPS
OF
SIO
X
/SI(
111)
.
72
5.5
RESONANT-PES
AT
HIGH
VACUUM
VERSUS
NEAR-AMBIENT
PRESSURE
.
75
5.5.1
X-RAY
RADIATION
EFFECTS
AND
SAMPLE
CONTAMINATION
.77
6
NICKEL-FERRITE
NANOPARTICLES
AS
A
PROMISING
OER
CATALYST
.
81
6.1
CHARACTERIZATION
OF
NICKEL-FERRITE
NPS
-
XRD,
RAMAN
AND
TEM
.
85
6.2
PEY-XAS
AND
XPS
OF
NICKEL-FERRITE
NPS
.90
6.3
LIQUID
MICROJET
XPS
OF
STABILIZED
NICKEL-FERRITE
NPS
-
RESULTS
AND
LIMITATIONS
.
99
6.3.1
STABILIZATION
OF
THE
NANOPARTICLE
SUSPENSION
-
ZETA
POTENTIAL,
PARTICLE
SIZE
.99
6.3.2
LIQUID
MICROJET
XPS
-
FE
AND
NI
LA-EDGE
AND
RESONANT
XPS
.
103
6.3.3
LIQUID-MICROJET
XPS
AT
THE
OXYGEN
K-EDGE
.
109
6.4
WATER-INDUCED
FORMATION
OF
FE
2+
ON
THE
SURFACE
OF
NICKEL-FERRITE
NPS
.
112
6.4.1
IRON
LA-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
112
6.4.2
NICKEL
LA-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
118
6.4.3
NEAR
AMBIENT
PRESSURE
XPS
-
CIS
AND
O
IS
.
120
6.4.4
OXYGEN
K-EDGE
PEY-XAS
UNDER
HIGH
VACUUM
AND
NAP
CONDITIONS
.
122
6.5
CATALYTIC
OER
ACTIVITY
OF
NICKEL-FERRITE
NPS
.
127
6.6
OPERANDO
PHOTON-IN
PHOTON-OUT
SPECTROSCOPY
-
THE
WAY
TO
GO?
.
131
7
OPERANDO
(RESONANT)
PHOTOELECTRON
SPECTROSCOPY
-
ROADMAP
AND
LIMITATIONS
.
137
7.1
IN-SITU
ELECTROCHEMICAL
DEPOSITION
AND
CHARACTERIZATION
OF
FENI
X
O
Y
.
138
7.2
OPERANDO
OXYGEN
EVOLUTION
REACTION
VERSUS
GRAPHENE
OXIDATION
.
146
7.3
ALTERNATIVE
FLOW-CELL
CONCEPT
-
THE
IONOMER
APPROACH
.
154
8
SUMMARY
AND
OUTLOOK
.
159
8.1
UPCOMING
PROJECTS
.
161
8.2
PROJECTS
BEYOND
THE
SCOPE
OF
MY
DOCTORAL
PROJECT
.
163
9
REFERENCE
.
165
10
APPENDIX
.
197
PUBLICATIONS
.205
ACKNOWLEDGEMENTS
.
207
SELBSTANDIGKEITSERKLARUNG
GEMAB
§
7
ABSATZ
4
.
209
VIII |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Hein, Dennis Matthias |
| author_GND | (DE-588)1260385647 |
| author_facet | Hein, Dennis Matthias |
| author_role | aut |
| author_sort | Hein, Dennis Matthias |
| author_variant | d m h dm dmh |
| building | Verbundindex |
| bvnumber | BV048290785 |
| ctrlnum | (OCoLC)1294932348 (DE-599)DNB1250440270 |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV048290785 |
| illustrated | Illustrated |
| index_date | 2024-07-03T20:03:33Z |
| indexdate | 2024-10-28T13:01:12Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033670790 |
| oclc_num | 1294932348 |
| open_access_boolean | |
| owner | DE-11 DE-706 |
| owner_facet | DE-11 DE-706 |
| physical | viii, 209 Seiten Illustrationen, Diagramme (farbig) |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| record_format | marc |
| spelling | Hein, Dennis Matthias Verfasser (DE-588)1260385647 aut Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting von Dennis Matthias Hein Berlin [2021?] viii, 209 Seiten Illustrationen, Diagramme (farbig) txt rdacontent n rdamedia nc rdacarrier Tag der mündlichen Prüfung: 03.12.2021 Dissertation Humboldt-Universität Berlin 2021 Zusammenfassung englisch und deutsch Photoelektronenspektroskopie (DE-588)4174491-3 gnd rswk-swf Wasserstofferzeugung (DE-588)4189271-9 gnd rswk-swf Edelmetall (DE-588)4013531-7 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Wasserstofferzeugung (DE-588)4189271-9 s Photoelektronenspektroskopie (DE-588)4174491-3 s Edelmetall (DE-588)4013531-7 s DE-604 B:DE-101 application/pdf https://d-nb.info/1250440270/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033670790&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hein, Dennis Matthias Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting Photoelektronenspektroskopie (DE-588)4174491-3 gnd Wasserstofferzeugung (DE-588)4189271-9 gnd Edelmetall (DE-588)4013531-7 gnd |
| subject_GND | (DE-588)4174491-3 (DE-588)4189271-9 (DE-588)4013531-7 (DE-588)4113937-9 |
| title | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |
| title_auth | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |
| title_exact_search | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |
| title_exact_search_txtP | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |
| title_full | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting von Dennis Matthias Hein |
| title_fullStr | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting von Dennis Matthias Hein |
| title_full_unstemmed | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting von Dennis Matthias Hein |
| title_short | Photoelectron spectroscopy of transition metal oxide-electrolyte interfaces relevant for catalytic water splitting |
| title_sort | photoelectron spectroscopy of transition metal oxide electrolyte interfaces relevant for catalytic water splitting |
| topic | Photoelektronenspektroskopie (DE-588)4174491-3 gnd Wasserstofferzeugung (DE-588)4189271-9 gnd Edelmetall (DE-588)4013531-7 gnd |
| topic_facet | Photoelektronenspektroskopie Wasserstofferzeugung Edelmetall Hochschulschrift |
| url | https://d-nb.info/1250440270/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033670790&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT heindennismatthias photoelectronspectroscopyoftransitionmetaloxideelectrolyteinterfacesrelevantforcatalyticwatersplitting |
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