Automated sample preparation: methods for GC-MS and LC-MS
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Weinheim
WILEY-VCH
[2022]
|
| Subjects: | |
| Online Access: | Kurzbeschreibung Inhaltsverzeichnis |
| Physical Description: | xvii, 459 Seiten Illustrationen, Diagramme (überwiegend farbig) |
| ISBN: | 9783527345076 3527345078 |
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MARC
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| 016 | 7 | |a 1222860198 |2 DE-101 | |
| 020 | |a 9783527345076 |c hbk. |9 978-3-527-34507-6 | ||
| 020 | |a 3527345078 |9 3-527-34507-8 | ||
| 024 | 3 | |a 9783527345076 | |
| 035 | |a (OCoLC)1296951665 | ||
| 035 | |a (DE-599)DNB1222860198 | ||
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| 100 | 1 | |a Hübschmann, Hans-Joachim |e Verfasser |0 (DE-588)1029246297 |4 aut | |
| 245 | 1 | 0 | |a Automated sample preparation |b methods for GC-MS and LC-MS |c Hans-Joachim Hübschmann |
| 264 | 1 | |a Weinheim |b WILEY-VCH |c [2022] | |
| 264 | 4 | |c © 2022 | |
| 300 | |a xvii, 459 Seiten |b Illustrationen, Diagramme (überwiegend farbig) | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a GC-MS |0 (DE-588)4414891-4 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Probenvorbereitung |0 (DE-588)4588977-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a LC-MS |0 (DE-588)4539813-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Automation |0 (DE-588)4003957-2 |2 gnd |9 rswk-swf |
| 653 | |a Chemical Analysis / Sample Preparation | ||
| 653 | |a Chemie | ||
| 653 | |a Chemische Analyse / Probenvorbereitung | ||
| 653 | |a Chemistry | ||
| 653 | |a Environmental Analysis | ||
| 653 | |a Food Chemistry | ||
| 653 | |a Food Science & Technology | ||
| 653 | |a Lebensmittelchemie | ||
| 653 | |a Lebensmittelforschung u. -technologie | ||
| 653 | |a Umweltanalytik | ||
| 653 | |a CH18: Chemische Analyse / Probenvorbereitung | ||
| 653 | |a CH21: Umweltanalytik | ||
| 653 | |a FO25: Lebensmittelchemie | ||
| 689 | 0 | 0 | |a GC-MS |0 (DE-588)4414891-4 |D s |
| 689 | 0 | 1 | |a LC-MS |0 (DE-588)4539813-6 |D s |
| 689 | 0 | 2 | |a Probenvorbereitung |0 (DE-588)4588977-6 |D s |
| 689 | 0 | 3 | |a Automation |0 (DE-588)4003957-2 |D s |
| 689 | 0 | |5 DE-604 | |
| 710 | 2 | |a Wiley-VCH |0 (DE-588)16179388-5 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-527-81752-8 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-527-81750-4 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, OBOOK |z 978-3-527-81751-1 |
| 856 | 4 | 2 | |m X:MVB |u http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34507-6/ |3 Kurzbeschreibung |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033035128&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-033035128 | ||
| 883 | 1 | |8 1\p |a vlb |d 20201205 |q DE-101 |u https://d-nb.info/provenance/plan#vlb | |
Record in the Search Index
| _version_ | 1804183115268096000 |
|---|---|
| adam_text | VII
CONTENTS
FOREWORD
XIII
PREFACE
XV
1
INTRODUCTION
1
1.1
A
PERSPECTIVE
ON
HUMAN
PERFORMANCE
2
REFERENCES
5
2
THE
ANALYTICAL
PROCESS
7
2.1
LABORATORY
LOGISTICS
7
2.1.1
ANALYTICAL
BENEFITS
OF
INSTRUMENTAL
WORKFLOWS
9
2.1.1.1
DATA
QUALITY
11
2.1.1.2
TURNKEY
OPERATION
11
2.1.1.3
GREEN
ANALYTICAL
CHEMISTRY
11
2.1.1.4
PRODUCTIVITY
12
2.1.2
STANDARD
OPERATION
PROCEDURE
13
2.1.3
ECONOMICAL
ASPECTS
15
REFERENCES
16
3
WORKFLOW
CONCEPTS
19
3.1
SAMPLE
PREPARATION
WORKFLOW
DESIGN
19
3.1.1
TRANSFER
OF
STANDARD
METHODS
TO
AUTOMATED
WORKFLOWS
20
3.1.2
METHOD
TRANSLATION
21
3.1.2.1
SKETCHING
THE
AUTOMATED
WORKFLOW
22
3.1.2.2
ROBOTIC
SYSTEM
CONFIGURATION
22
3.1.3
ONLINE
OR
OFFLINE
CONFIGURATION
25
3.2
INSTRUMENTAL
CONCEPTS
25
3.2.1
WORKSTATIONS
25
3.2.2
REVOLVING
TRAY
AUTOSAMPLERS
26
3.2.3
SELECTIVE
COMPLIANCE
ARTICULATED
ROBOTS
28
3.2.4
CARTESIAN
ROBOTS
28
3.2.5
MULTIPLE
AXIS
ROBOTS
32
3.2.6
COLLABORATIVE
ROBOTS
33
VIII
CONTENTS
3.3
3.3.1
3.3.2
3.3.3
3.3.4
3.3.5
3.3.6
3.3.6.1
3.3.6.2
3.4
3.4.1
3.4.2
3.4.3
3.5
3.5.1
3.5.2
3.5.3
3.6
SAMPLE
PROCESSING
35
SEQUENTIAL
SAMPLE
PREPARATION
35
PREP-AHEAD
MODE
35
INCUBATION
OVERLAPPING
36
BATCH
PROCESSING
36
PARALLEL
PROCESSING
WORKFLOWS
38
SAMPLE
IDENTIFICATION
38
BARCODES
38
RADIO-FREQUENCY
IDENTIFICATION
CHIPS
40
TOOL
CHANGE
41
MANUAL
TOOL
CHANGE
41
AUTOMATED
TOOL
CHANGE
42
TOOL
IDENTIFICATION
44
OBJECT
TRANSPORT
46
MAGNETIC
TRANSPORT
46
GRIPPER
TRANSPORT
48
NEEDLE
TRANSPORT
50
VIAL
DECAPPING
50
REFERENCES
52
4
4.1
4.1.1
4.1.2
4.1.2.1
4.1.2.2
4.1.2.3
4.1.2.4
4.1.2.5
4.1.2.6
4.1.3
4.1.4
4.1.4.1
4.1.4.2
4.1.4.3
4.1.4.4
4.1.4.5
4.1.4.6
4.1.4.7
4.1.4.8
4.1.4.9
4.1.4.10
4.1.5
4.1.6
4.2
ANALYTICAL
ASPECTS
55
LIQUID
HANDLING
55
ABOUT
DROPS
AND
DROPLETS
55
SYRINGES
56
PRECISION
AND
ACCURACY
57
SYRINGE
NEEDLES
58
SYRINGE
NEEDLE
POINT
STYLES
59
SYRINGE
PLUNGER
TYPES
60
SYRINGE
TERMINATION
61
OPERATIONAL
PARAMETERS
62
VIAL
BOTTOM
SENSING
66
PIPETTING
67
AIR
DISPLACEMENT
PIPETTES
68
POSITIVE
DISPLACEMENT
PIPETS
69
PIPETTING
MODES
69
ASPIRATION
71
DISPENSING
73
LIQUID-LEVEL
DETECTION
74
LIQUID
CLASSES
75
PIPET
TIPS
75
FUNCTIONAL
PIPET
TIPS
78
PIPET
TIP
MATERIALS
81
DILUTOR/DISPENSER
OPERATION
82
FLOW
CELL
SAMPLING
84
SOLID
MATERIALS
HANDLING
85
CONTENTS
IX
4.2.1
WORKFLOWS
WITH
SOLID
MATERIALS
86
4.2.2
AUTOMATED
SOLIDS
DOSING
BY
POWDER
DISPENSING
86
4.3
WEIGHING
88
4.4
EXTRACTION
90
4.4.1
LIQUID
EXTRACTION
91
4.4.2
PRESSURIZED
FLUID
EXTRACTION
92
4.4.2.1
SOLVENTS
AND
EXTRACTION
93
4.4.2.2
MINIATURIZATION
AND
AUTOMATION
94
4.4.2.3
IN-CELL
CLEAN-UP
96
4.4.2.4
INTERNATIONAL
STANDARD
METHODS
97
4.4.3
LIQUID/LIQUID
EXTRACTION
97
4.4.4
DISPERSIVE
LIQUID/LIQUID
MICRO-EXTRACTION
100
4.4.4.1
AUTOMATED
DLLME
WORKFLOWS
103
4.4.4.2
DLLME
FOR
SOIL
AND
URINE
103
4.4.4.3
DLLME
FOR
PESTICIDES
IN
FOOD
104
4.4.4.4
DLLME
HYPHENATION
WITH
LC
104
4.4.5
SORPTIVE
SAMPLE
PREPARATION
104
4.4.5.1
SOLID-PHASE
MICRO-EXTRACTION
105
4.4.5.2
SPME
FIBER
109
4.4.5.3
SPME
ARROW
112
4.4.5.4
SOLID-PHASE
MICRO-EXTRACTION
WITH
DERIVATIZATION
116
4.4.5.5
DIRECT
SOLID-PHASE
MICRO-EXTRACTION
MASS
SPECTROMETRY
119
4.4.5.6
STIR BAR
SORPTIVE
EXTRACTION
121
4.4.5.7
THIN-FILM
MICRO-EXTRACTION
123
4.5
CLEAN-UP
PROCEDURES
124
4.5.1
FILTRATION
124
4.5.1.1
FILTER
MATERIALS
125
4.5.1.2
SYRINGE
FILTER
126
4.5.1.3
FILTER
VIALS
127
4.5.2
SOLID-PHASE
EXTRACTION
129
4.5.2.1
THE
GENERAL
SPE
CLEAN-UP
PROCEDURE
133
4.5.2.2
ON-LINE
SPE
134
4.5.2.3
MICRO-SPE
CLEAN-UP
137
4.5.2.4
SYRINGE-BASED
MICRO-SPE
141
4.5.3
GEL
PERMEATION
CHROMATOGRAPHY
143
4.5.3.1
STANDARDIZED
METHODS
145
4.5.3.2
WORKFLOW
AND
INSTRUMENT
CONFIGURATION
145
4.5.3.3
GPC-GC
ONLINE
COUPLING
146
4.5.3.4
MICRO-GPC-GC
ONLINE
COUPLING
147
4.6
CENTRIFUGATION
148
4.7
EVAPORATION
150
4.8
DERIVATIZATION
153
4.8.1
FOR
LC
AND
LC-MS
154
4.8.1.1
AROMATIC
ACID
CHLORIDES
154
4.8.1.2
DANSYLCHLORIDE
155
CONTENTS
4.8.1.3
4.8.1.4
4.8.2
4.8.2.1
4.8.2.2
4.8.2.3
4.8.2.4
4.8.2.5
4.8.3
4.9
4.9.1
4.9.1.1
4.9.2
4.10
4.10.1
4.10.2
4.10.3
4.10.4
4.10.5
NINHYDRIN
REACTION
155
FMOC
DERIVATIZATION
155
FOR
GC
AND
GC-MS
156
SILYLATION
156
ACETYLATION
157
METHYLATION
157
METHOXYAMINATION
158
FLUORINATING
REAGENTS
158
FOR
GC
AND
GC-MS
IN-PORT
DERIVATIZATION
159
TEMPERATURE
CONTROL
163
HEATING
163
INCUBATION
OVERLAPPING
163
COOLING
164
MIXING
166
VORTEXING
166
AGITATION
167
SPINNING
169
MIXING
WITH
SYRINGES
169
CYCLOIDAL
MIXING
169
REFERENCES
171
5
5.1
5.1.1
5.1.1.1
5.1.1.2
5.1.1.3
5.1.2
5.1.3
5.1.3.1
5.1.3.2
5.1.3.3
5.1.3.4
5.1.4
5.2
5.2.1
5.2.2
5.2.3
5.2.4
5.3
5.4
5.4.1
5.4.2
INTEGRATION
INTO
ANALYSIS
TECHNIQUES
191
GC
VOLATILES
ANALYSIS
191
STATIC
HEADSPACE
ANALYSIS
192
OVERCOMING
MATRIX
EFFECTS
194
MEASURES
TO
INCREASE
ANALYTE
SENSITIVITY
195
STATIC
HEADSPACE
INJECTION
TECHNIQUE
195
MULTIPLE
HEADSPACE
QUANTIFICATION
197
DYNAMIC
HEADSPACE
ANALYSIS
201
PURGE
AND
TRAP
202
DYNAMIC
HEADSPACE
ANALYSIS
WITH
IN-TUBE
EXTRACTION
204
DYNAMIC
HEADSPACE
ANALYSIS
USING
SORBENT
TUBES
207
NEEDLE
TRAP
MICROEXTRACTION
208
TUBE
ADSORPTION
210
GC
LIQUID
INJECTION
222
SANDWICH
INJECTION
222
HOT
NEEDLE
INJECTION
222
LIQUID
BAND
INJECTION
224
AUTOMATED
LINER
EXCHANGE
226
LC-GC
ONLINE
INJECTION
230
LC
INJECTION
233
DYNAMIC
LOAD
AND
WASH
234
USING
LC
INJECTION
PORTS
WITH
A
PIPETTE
TOOL
235
REFERENCES
237
CONTENTS
XI
6
SOLUTIONS
FOR
AUTOMATED
ANALYSES
247
FIRST
ABOUT
SAFETY
248
6.1
DILUTION
248
6.1.1
GEOMETRIC
DILUTION
OF
REFERENCE
STANDARDS
248
6.1.2
DILUTION
FOR
CALIBRATION
CURVES
251
6.1.3
PREPARATION
OF
WORKING
STANDARDS
256
6.2
DERIVATIZATION
259
6.2.1
SILYLATION
260
6.2.2
SPME
ON-FIBER
DERIVATIZATION
262
6.2.3
METABOLITE
PROFILING
BY
METHOXIMATION
AND
SILYLATION
266
6.3
TASTE
AND
ODOR
COMPOUNDS
TRACE
ANALYSIS
271
6.4
SULFUR
COMPOUNDS
IN
TROPICAL
FRUITS
276
6.5
ETHANOL
RESIDUES
IN
HALAL
FOOD
284
6.6
VOLATILE
ORGANIC
COMPOUNDS
IN
DRINKING
WATER
289
6.7
GEOSMIN
AND
2-MIB
295
6.8
SOLVENT
ELUTION
FROM
CHARCOAL
301
6.9
SEMIVOLATILE
ORGANIC
COMPOUNDS
IN
WATER
304
6.10
POLYAROMATIC
HYDROCARBONS
IN
DRINKING
WATER
315
6.11
FATTY
ACID
METHYLESTER
321
6.11.1
APPLICATION
321
6.12
MCPD
AND
GLYCIDOL
IN
VEGETABLE
OILS
328
6.13
MINERAL
OIL
HYDROCARBONS
MOSH/MOAH
339
6.14
PESTICIDES
ANALYSIS
-
QUECHERS
EXTRACT
CLEAN-UP
347
6.15
GLYPHOSATE,
AMPA,
AND
GLUFOSINATE
BY
ONLINE
SPE-LC-MS
362
6.16
PESTICIDES,
PPCPS,
AND
PAHS
BY
ONLINE-SPE
WATER
ANALYSIS
368
6.17
RESIDUAL
SOLVENTS
375
6.18
CHEMICAL
WARFARE
AGENTS
IN
WATER
AND
SOIL
382
6.19
SHALE
ALDEHYDES
IN
BEER
390
6.20
PHTHALATES
IN
POLYMERS
394
REFERENCES
400
K
APPENDIX
413
A.L
ROBOTIC
SYSTEM
CONTROL
413
A.1.1
MAESTRO
SOFTWARE
413
A.
1.2
CHRONOS
SOFTWARE
414
A.L.
3
GRAPHICAL
WORKFLOW
PROGRAMMING
415
A.
1.4
SAMPLE
CONTROL
SOFTWARE
416
A.1.5
LOCAL
SYSTEM
CONTROL
417
A.1.6
SCRIPT
CONTROL
LANGUAGE
418
A.2
SYSTEM
MAINTENANCE
418
A.2.1
SYRINGES
418
A.2.1.1
MANUAL
SYRINGE
HANDLING
418
A.2.1.
2
SYRINGE
CLEANING
418
A.2.1.3
PLUNGER
CLEANING
419
A.2.1.4
NEEDLE
CLEANING
419
XII
CONTENTS
A.2.1.
5
A.2.1.
6
A.2.2
A.2.2.1
A.2.2.2
A.2.3
A.3
A.4
A.5
A.5.1
A.5.2
A.5.2.1
A.5.2.
2
A.5.
3
A.6
A.6.1
A.6.2
A.6.3
CONFIRMING
THE
DISPENSED
VOLUME
OF
A
SYRINGE
420
STERILIZATION
420
PIPETTES
421
CALIBRATION
421
PIPETTE
PARTS
MAINTENANCE
421
SYSTEM
HARDWARE
MAINTENANCE
SCHEDULE
422
SYRINGE
NEEDLE
GAUGE
423
PRESSURE
UNITS
CONVERSION
425
SOLVENTS
425
SOLVENT
MISCIBILITY
425
SOLVENT
STABILITY
428
HALOGENATED
SOLVENTS
428
ETHERS
429
SOLVENT
VISCOSITY
429
MATERIAL
RESISTANCE
429
GLASS
432
POLYMERS
432
STAINLESS
STEEL
433
REFERENCES
437
GLOSSARY
441
REFERENCES
451
INDEX
453
|
| adam_txt |
VII
CONTENTS
FOREWORD
XIII
PREFACE
XV
1
INTRODUCTION
1
1.1
A
PERSPECTIVE
ON
HUMAN
PERFORMANCE
2
REFERENCES
5
2
THE
ANALYTICAL
PROCESS
7
2.1
LABORATORY
LOGISTICS
7
2.1.1
ANALYTICAL
BENEFITS
OF
INSTRUMENTAL
WORKFLOWS
9
2.1.1.1
DATA
QUALITY
11
2.1.1.2
TURNKEY
OPERATION
11
2.1.1.3
GREEN
ANALYTICAL
CHEMISTRY
11
2.1.1.4
PRODUCTIVITY
12
2.1.2
STANDARD
OPERATION
PROCEDURE
13
2.1.3
ECONOMICAL
ASPECTS
15
REFERENCES
16
3
WORKFLOW
CONCEPTS
19
3.1
SAMPLE
PREPARATION
WORKFLOW
DESIGN
19
3.1.1
TRANSFER
OF
STANDARD
METHODS
TO
AUTOMATED
WORKFLOWS
20
3.1.2
METHOD
TRANSLATION
21
3.1.2.1
SKETCHING
THE
AUTOMATED
WORKFLOW
22
3.1.2.2
ROBOTIC
SYSTEM
CONFIGURATION
22
3.1.3
ONLINE
OR
OFFLINE
CONFIGURATION
25
3.2
INSTRUMENTAL
CONCEPTS
25
3.2.1
WORKSTATIONS
25
3.2.2
REVOLVING
TRAY
AUTOSAMPLERS
26
3.2.3
SELECTIVE
COMPLIANCE
ARTICULATED
ROBOTS
28
3.2.4
CARTESIAN
ROBOTS
28
3.2.5
MULTIPLE
AXIS
ROBOTS
32
3.2.6
COLLABORATIVE
ROBOTS
33
VIII
CONTENTS
3.3
3.3.1
3.3.2
3.3.3
3.3.4
3.3.5
3.3.6
3.3.6.1
3.3.6.2
3.4
3.4.1
3.4.2
3.4.3
3.5
3.5.1
3.5.2
3.5.3
3.6
SAMPLE
PROCESSING
35
SEQUENTIAL
SAMPLE
PREPARATION
35
PREP-AHEAD
MODE
35
INCUBATION
OVERLAPPING
36
BATCH
PROCESSING
36
PARALLEL
PROCESSING
WORKFLOWS
38
SAMPLE
IDENTIFICATION
38
BARCODES
38
RADIO-FREQUENCY
IDENTIFICATION
CHIPS
40
TOOL
CHANGE
41
MANUAL
TOOL
CHANGE
41
AUTOMATED
TOOL
CHANGE
42
TOOL
IDENTIFICATION
44
OBJECT
TRANSPORT
46
MAGNETIC
TRANSPORT
46
GRIPPER
TRANSPORT
48
NEEDLE
TRANSPORT
50
VIAL
DECAPPING
50
REFERENCES
52
4
4.1
4.1.1
4.1.2
4.1.2.1
4.1.2.2
4.1.2.3
4.1.2.4
4.1.2.5
4.1.2.6
4.1.3
4.1.4
4.1.4.1
4.1.4.2
4.1.4.3
4.1.4.4
4.1.4.5
4.1.4.6
4.1.4.7
4.1.4.8
4.1.4.9
4.1.4.10
4.1.5
4.1.6
4.2
ANALYTICAL
ASPECTS
55
LIQUID
HANDLING
55
ABOUT
DROPS
AND
DROPLETS
55
SYRINGES
56
PRECISION
AND
ACCURACY
57
SYRINGE
NEEDLES
58
SYRINGE
NEEDLE
POINT
STYLES
59
SYRINGE
PLUNGER
TYPES
60
SYRINGE
TERMINATION
61
OPERATIONAL
PARAMETERS
62
VIAL
BOTTOM
SENSING
66
PIPETTING
67
AIR
DISPLACEMENT
PIPETTES
68
POSITIVE
DISPLACEMENT
PIPETS
69
PIPETTING
MODES
69
ASPIRATION
71
DISPENSING
73
LIQUID-LEVEL
DETECTION
74
LIQUID
CLASSES
75
PIPET
TIPS
75
FUNCTIONAL
PIPET
TIPS
78
PIPET
TIP
MATERIALS
81
DILUTOR/DISPENSER
OPERATION
82
FLOW
CELL
SAMPLING
84
SOLID
MATERIALS
HANDLING
85
CONTENTS
IX
4.2.1
WORKFLOWS
WITH
SOLID
MATERIALS
86
4.2.2
AUTOMATED
SOLIDS
DOSING
BY
POWDER
DISPENSING
86
4.3
WEIGHING
88
4.4
EXTRACTION
90
4.4.1
LIQUID
EXTRACTION
91
4.4.2
PRESSURIZED
FLUID
EXTRACTION
92
4.4.2.1
SOLVENTS
AND
EXTRACTION
93
4.4.2.2
MINIATURIZATION
AND
AUTOMATION
94
4.4.2.3
IN-CELL
CLEAN-UP
96
4.4.2.4
INTERNATIONAL
STANDARD
METHODS
97
4.4.3
LIQUID/LIQUID
EXTRACTION
97
4.4.4
DISPERSIVE
LIQUID/LIQUID
MICRO-EXTRACTION
100
4.4.4.1
AUTOMATED
DLLME
WORKFLOWS
103
4.4.4.2
DLLME
FOR
SOIL
AND
URINE
103
4.4.4.3
DLLME
FOR
PESTICIDES
IN
FOOD
104
4.4.4.4
DLLME
HYPHENATION
WITH
LC
104
4.4.5
SORPTIVE
SAMPLE
PREPARATION
104
4.4.5.1
SOLID-PHASE
MICRO-EXTRACTION
105
4.4.5.2
SPME
FIBER
109
4.4.5.3
SPME
ARROW
112
4.4.5.4
SOLID-PHASE
MICRO-EXTRACTION
WITH
DERIVATIZATION
116
4.4.5.5
DIRECT
SOLID-PHASE
MICRO-EXTRACTION
MASS
SPECTROMETRY
119
4.4.5.6
STIR BAR
SORPTIVE
EXTRACTION
121
4.4.5.7
THIN-FILM
MICRO-EXTRACTION
123
4.5
CLEAN-UP
PROCEDURES
124
4.5.1
FILTRATION
124
4.5.1.1
FILTER
MATERIALS
125
4.5.1.2
SYRINGE
FILTER
126
4.5.1.3
FILTER
VIALS
127
4.5.2
SOLID-PHASE
EXTRACTION
129
4.5.2.1
THE
GENERAL
SPE
CLEAN-UP
PROCEDURE
133
4.5.2.2
ON-LINE
SPE
134
4.5.2.3
MICRO-SPE
CLEAN-UP
137
4.5.2.4
SYRINGE-BASED
MICRO-SPE
141
4.5.3
GEL
PERMEATION
CHROMATOGRAPHY
143
4.5.3.1
STANDARDIZED
METHODS
145
4.5.3.2
WORKFLOW
AND
INSTRUMENT
CONFIGURATION
145
4.5.3.3
GPC-GC
ONLINE
COUPLING
146
4.5.3.4
MICRO-GPC-GC
ONLINE
COUPLING
147
4.6
CENTRIFUGATION
148
4.7
EVAPORATION
150
4.8
DERIVATIZATION
153
4.8.1
FOR
LC
AND
LC-MS
154
4.8.1.1
AROMATIC
ACID
CHLORIDES
154
4.8.1.2
DANSYLCHLORIDE
155
CONTENTS
4.8.1.3
4.8.1.4
4.8.2
4.8.2.1
4.8.2.2
4.8.2.3
4.8.2.4
4.8.2.5
4.8.3
4.9
4.9.1
4.9.1.1
4.9.2
4.10
4.10.1
4.10.2
4.10.3
4.10.4
4.10.5
NINHYDRIN
REACTION
155
FMOC
DERIVATIZATION
155
FOR
GC
AND
GC-MS
156
SILYLATION
156
ACETYLATION
157
METHYLATION
157
METHOXYAMINATION
158
FLUORINATING
REAGENTS
158
FOR
GC
AND
GC-MS
IN-PORT
DERIVATIZATION
159
TEMPERATURE
CONTROL
163
HEATING
163
INCUBATION
OVERLAPPING
163
COOLING
164
MIXING
166
VORTEXING
166
AGITATION
167
SPINNING
169
MIXING
WITH
SYRINGES
169
CYCLOIDAL
MIXING
169
REFERENCES
171
5
5.1
5.1.1
5.1.1.1
5.1.1.2
5.1.1.3
5.1.2
5.1.3
5.1.3.1
5.1.3.2
5.1.3.3
5.1.3.4
5.1.4
5.2
5.2.1
5.2.2
5.2.3
5.2.4
5.3
5.4
5.4.1
5.4.2
INTEGRATION
INTO
ANALYSIS
TECHNIQUES
191
GC
VOLATILES
ANALYSIS
191
STATIC
HEADSPACE
ANALYSIS
192
OVERCOMING
MATRIX
EFFECTS
194
MEASURES
TO
INCREASE
ANALYTE
SENSITIVITY
195
STATIC
HEADSPACE
INJECTION
TECHNIQUE
195
MULTIPLE
HEADSPACE
QUANTIFICATION
197
DYNAMIC
HEADSPACE
ANALYSIS
201
PURGE
AND
TRAP
202
DYNAMIC
HEADSPACE
ANALYSIS
WITH
IN-TUBE
EXTRACTION
204
DYNAMIC
HEADSPACE
ANALYSIS
USING
SORBENT
TUBES
207
NEEDLE
TRAP
MICROEXTRACTION
208
TUBE
ADSORPTION
210
GC
LIQUID
INJECTION
222
SANDWICH
INJECTION
222
HOT
NEEDLE
INJECTION
222
LIQUID
BAND
INJECTION
224
AUTOMATED
LINER
EXCHANGE
226
LC-GC
ONLINE
INJECTION
230
LC
INJECTION
233
DYNAMIC
LOAD
AND
WASH
234
USING
LC
INJECTION
PORTS
WITH
A
PIPETTE
TOOL
235
REFERENCES
237
CONTENTS
XI
6
SOLUTIONS
FOR
AUTOMATED
ANALYSES
247
FIRST
ABOUT
SAFETY
248
6.1
DILUTION
248
6.1.1
GEOMETRIC
DILUTION
OF
REFERENCE
STANDARDS
248
6.1.2
DILUTION
FOR
CALIBRATION
CURVES
251
6.1.3
PREPARATION
OF
WORKING
STANDARDS
256
6.2
DERIVATIZATION
259
6.2.1
SILYLATION
260
6.2.2
SPME
ON-FIBER
DERIVATIZATION
262
6.2.3
METABOLITE
PROFILING
BY
METHOXIMATION
AND
SILYLATION
266
6.3
TASTE
AND
ODOR
COMPOUNDS
TRACE
ANALYSIS
271
6.4
SULFUR
COMPOUNDS
IN
TROPICAL
FRUITS
276
6.5
ETHANOL
RESIDUES
IN
HALAL
FOOD
284
6.6
VOLATILE
ORGANIC
COMPOUNDS
IN
DRINKING
WATER
289
6.7
GEOSMIN
AND
2-MIB
295
6.8
SOLVENT
ELUTION
FROM
CHARCOAL
301
6.9
SEMIVOLATILE
ORGANIC
COMPOUNDS
IN
WATER
304
6.10
POLYAROMATIC
HYDROCARBONS
IN
DRINKING
WATER
315
6.11
FATTY
ACID
METHYLESTER
321
6.11.1
APPLICATION
321
6.12
MCPD
AND
GLYCIDOL
IN
VEGETABLE
OILS
328
6.13
MINERAL
OIL
HYDROCARBONS
MOSH/MOAH
339
6.14
PESTICIDES
ANALYSIS
-
QUECHERS
EXTRACT
CLEAN-UP
347
6.15
GLYPHOSATE,
AMPA,
AND
GLUFOSINATE
BY
ONLINE
SPE-LC-MS
362
6.16
PESTICIDES,
PPCPS,
AND
PAHS
BY
ONLINE-SPE
WATER
ANALYSIS
368
6.17
RESIDUAL
SOLVENTS
375
6.18
CHEMICAL
WARFARE
AGENTS
IN
WATER
AND
SOIL
382
6.19
SHALE
ALDEHYDES
IN
BEER
390
6.20
PHTHALATES
IN
POLYMERS
394
REFERENCES
400
K
APPENDIX
413
A.L
ROBOTIC
SYSTEM
CONTROL
413
A.1.1
MAESTRO
SOFTWARE
413
A.
1.2
CHRONOS
SOFTWARE
414
A.L.
3
GRAPHICAL
WORKFLOW
PROGRAMMING
415
A.
1.4
SAMPLE
CONTROL
SOFTWARE
416
A.1.5
LOCAL
SYSTEM
CONTROL
417
A.1.6
SCRIPT
CONTROL
LANGUAGE
418
A.2
SYSTEM
MAINTENANCE
418
A.2.1
SYRINGES
418
A.2.1.1
MANUAL
SYRINGE
HANDLING
418
A.2.1.
2
SYRINGE
CLEANING
418
A.2.1.3
PLUNGER
CLEANING
419
A.2.1.4
NEEDLE
CLEANING
419
XII
CONTENTS
A.2.1.
5
A.2.1.
6
A.2.2
A.2.2.1
A.2.2.2
A.2.3
A.3
A.4
A.5
A.5.1
A.5.2
A.5.2.1
A.5.2.
2
A.5.
3
A.6
A.6.1
A.6.2
A.6.3
CONFIRMING
THE
DISPENSED
VOLUME
OF
A
SYRINGE
420
STERILIZATION
420
PIPETTES
421
CALIBRATION
421
PIPETTE
PARTS
MAINTENANCE
421
SYSTEM
HARDWARE
MAINTENANCE
SCHEDULE
422
SYRINGE
NEEDLE
GAUGE
423
PRESSURE
UNITS
CONVERSION
425
SOLVENTS
425
SOLVENT
MISCIBILITY
425
SOLVENT
STABILITY
428
HALOGENATED
SOLVENTS
428
ETHERS
429
SOLVENT
VISCOSITY
429
MATERIAL
RESISTANCE
429
GLASS
432
POLYMERS
432
STAINLESS
STEEL
433
REFERENCES
437
GLOSSARY
441
REFERENCES
451
INDEX
453 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Hübschmann, Hans-Joachim |
| author_GND | (DE-588)1029246297 |
| author_facet | Hübschmann, Hans-Joachim |
| author_role | aut |
| author_sort | Hübschmann, Hans-Joachim |
| author_variant | h j h hjh |
| building | Verbundindex |
| bvnumber | BV047651072 |
| classification_rvk | VG 9800 |
| ctrlnum | (OCoLC)1296951665 (DE-599)DNB1222860198 |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV047651072 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:49:58Z |
| indexdate | 2024-07-10T09:18:19Z |
| institution | BVB |
| institution_GND | (DE-588)16179388-5 |
| isbn | 9783527345076 3527345078 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-033035128 |
| oclc_num | 1296951665 |
| open_access_boolean | |
| owner | DE-11 |
| owner_facet | DE-11 |
| physical | xvii, 459 Seiten Illustrationen, Diagramme (überwiegend farbig) |
| publishDate | 2022 |
| publishDateSearch | 2022 |
| publishDateSort | 2022 |
| publisher | WILEY-VCH |
| record_format | marc |
| spelling | Hübschmann, Hans-Joachim Verfasser (DE-588)1029246297 aut Automated sample preparation methods for GC-MS and LC-MS Hans-Joachim Hübschmann Weinheim WILEY-VCH [2022] © 2022 xvii, 459 Seiten Illustrationen, Diagramme (überwiegend farbig) txt rdacontent n rdamedia nc rdacarrier GC-MS (DE-588)4414891-4 gnd rswk-swf Probenvorbereitung (DE-588)4588977-6 gnd rswk-swf LC-MS (DE-588)4539813-6 gnd rswk-swf Automation (DE-588)4003957-2 gnd rswk-swf Chemical Analysis / Sample Preparation Chemie Chemische Analyse / Probenvorbereitung Chemistry Environmental Analysis Food Chemistry Food Science & Technology Lebensmittelchemie Lebensmittelforschung u. -technologie Umweltanalytik CH18: Chemische Analyse / Probenvorbereitung CH21: Umweltanalytik FO25: Lebensmittelchemie GC-MS (DE-588)4414891-4 s LC-MS (DE-588)4539813-6 s Probenvorbereitung (DE-588)4588977-6 s Automation (DE-588)4003957-2 s DE-604 Wiley-VCH (DE-588)16179388-5 pbl Erscheint auch als Online-Ausgabe, EPUB 978-3-527-81752-8 Erscheint auch als Online-Ausgabe, PDF 978-3-527-81750-4 Erscheint auch als Online-Ausgabe, OBOOK 978-3-527-81751-1 X:MVB http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34507-6/ Kurzbeschreibung DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033035128&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p vlb 20201205 DE-101 https://d-nb.info/provenance/plan#vlb |
| spellingShingle | Hübschmann, Hans-Joachim Automated sample preparation methods for GC-MS and LC-MS GC-MS (DE-588)4414891-4 gnd Probenvorbereitung (DE-588)4588977-6 gnd LC-MS (DE-588)4539813-6 gnd Automation (DE-588)4003957-2 gnd |
| subject_GND | (DE-588)4414891-4 (DE-588)4588977-6 (DE-588)4539813-6 (DE-588)4003957-2 |
| title | Automated sample preparation methods for GC-MS and LC-MS |
| title_auth | Automated sample preparation methods for GC-MS and LC-MS |
| title_exact_search | Automated sample preparation methods for GC-MS and LC-MS |
| title_exact_search_txtP | Automated sample preparation methods for GC-MS and LC-MS |
| title_full | Automated sample preparation methods for GC-MS and LC-MS Hans-Joachim Hübschmann |
| title_fullStr | Automated sample preparation methods for GC-MS and LC-MS Hans-Joachim Hübschmann |
| title_full_unstemmed | Automated sample preparation methods for GC-MS and LC-MS Hans-Joachim Hübschmann |
| title_short | Automated sample preparation |
| title_sort | automated sample preparation methods for gc ms and lc ms |
| title_sub | methods for GC-MS and LC-MS |
| topic | GC-MS (DE-588)4414891-4 gnd Probenvorbereitung (DE-588)4588977-6 gnd LC-MS (DE-588)4539813-6 gnd Automation (DE-588)4003957-2 gnd |
| topic_facet | GC-MS Probenvorbereitung LC-MS Automation |
| url | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34507-6/ http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=033035128&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hubschmannhansjoachim automatedsamplepreparationmethodsforgcmsandlcms AT wileyvch automatedsamplepreparationmethodsforgcmsandlcms |