High-pressure calorimetry: evaluation of methods and measurement of heat capacities:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Düren
Shaker Verlag
2021
|
| Series: | Darmstädter Schriftenreihe der Polymerisationstechnik
18 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | i, 154, XIV Seiten Illustrationen, Diagramme |
| ISBN: | 9783844080742 3844080740 |
Staff View
MARC
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| 100 | 1 | |a Nowottny, Jonas |e Verfasser |0 (DE-588)1236782127 |4 aut | |
| 245 | 1 | 0 | |a High-pressure calorimetry: evaluation of methods and measurement of heat capacities |c Jonas Nowottny |
| 264 | 1 | |a Düren |b Shaker Verlag |c 2021 | |
| 300 | |a i, 154, XIV Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Darmstädter Schriftenreihe der Polymerisationstechnik |v 18 | |
| 502 | |b Dissertation |c Technische Universität Darmstadt |d 2021 | ||
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| 653 | |a Calorimetry | ||
| 653 | |a Pressure | ||
| 653 | |a Heat Capacities | ||
| 653 | |a PC-SAFT | ||
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Record in the Search Index
| _version_ | 1804182911843303424 |
|---|---|
| adam_text | CONTENTS
1
INTRODUCTION
5
2
THEORY
8
2.1
THERMODYNAMICS
.........................................................................................................
8
2.1.1
HEAT
AND
HEAT
CAPACITY
.................................................................................
8
2.2
EQUATION
OF
STATE
(EOS)
.............................................................................................
14
2.2.1
REDLICH-KWONG-SOAVE
(RKS)
...........................................................................
14
2.2.2
PENG-ROBINSON
(PR)
.......................................................................................
14
2.2.3
TAIT-EQUATION
...................................................................................................
15
2.2.4
LEE-KESLER-PLOECKER
(LKP)
.................................................................................
15
2.2.5
EUROPEAN
GAS
RESEARCH
GROUP
MODEL
(GERG-MODEL)
...................................
15
2.2.6
PERTURBED-CHAIN
STATISTICAL-ASSOCIATING-FLUID-THEORY
(PC-SAFT)
...............
16
2.3
THERMAL
ANALYSIS:
THE
CALORIMETER
...........................................................................
18
2.3.1
EXPERIMENTAL
SET-UP
OF
CALORIMETERS
............................................................
19
2.3.2
MEASURING
PRINCIPLES
FOR
HEAT
DETECTION
IN
CALORIMETERS
............................
19
2.3.3
OPERATING
MODE
OF
A
CALORIMETER:
THERMODYNAMIC
CONDITIONS
DURING
A
MEASUREMENT
...................................................................................................
21
2.4
APPLICATION
OF
CALORIMETERS
IN
THERMAL
ANALYSIS:
DTA
AND
DSC
..............................
22
2.4.1
COMPARING
CALORIMETERS:
THE
TIME
CONSTANT
.............................................
23
2.4.2
CALIBRATION
OF
CALORIMETERS
AND
REFERENCE
SUBSTANCES
.................................
26
2.5
METHODS
FOR
EXPERIMENTAL
DETERMINATION
OF
HEAT
CAPACITIES
.................................
27
2.5.1
RESISTANCE
WIRE
................................................................................................
27
2.5.2
FLOW
CALORIMETRY
.............................................................................................
28
2.5.3
SPEED
OF
SOUND
................................................................................................
28
2.5.4
DIFFERENCE
SCANNING
CALORIMETRY:
THREE-STEP
METHOD
.................................
29
2.5.5
DIFFERENCE
SCANNING
CALORIMETRY:
TWO-STEP
METHOD
...............................
30
2.5.6
DIFFERENCE
SCANNING
CALORIMETRY:
TEMPERATURE-STEP
METHOD
.......................
31
2.5.7
DIFFERENCE
SCANNING
CALORIMETRY:
PRESSURE-SCAN
METHOD
...........................
32
2.5.8
DIFFERENCE
SCANNING
CALORIMETRY:
PRESSURE-STEP
METHOD
............................
34
2.5.9
DIFFERENCE
SCANNING
CALORIMETRY:
TEMPERATURE
MODULATION
........................
35
3
EXPERIMENTAL
SECTION
38
3.1
DSC
..............................................................................................................................
38
3.1.1
ALUMINIUM
CRUCIBLES
.......................................................................................
39
3.1.2
HIGH-PRESSURE
STEEL
CRUCIBLES
AND
THEIR
CLOSING
UNDER
PRESSURE
................
39
3.2
TRANSITIOMETER
............................................................................................................
40
3.2.1
INDICATION
AND
REGULATION
..............................................................................
43
3.2.2
MEASUREMENT
CELIS
..........................................................................................
45
3.2.3
OPTIONAL
SAMPLE
CONTAINERS:
THE
AMPOULES
................................................
47
3.3
SIZE
EXCLUSION
CHROMATOGRAPHY
SEC
........................................................................
49
4
METHOD
EVALUATION:
DETERMINING
A
PRESSURE
DEPENDENCE
ON
HEAT
CAPACITIES
BY
CALORIMETRY
51
4.1
TIME
CONSTANTS
OF
APPLIED
CALORIMETERS
...................................................................
51
4.2
METHOD
PROCESSING
FOR
DETERMINING
HEAT
CAPACITIES
BY
CALORIMETRY
.....................
53
4.2.1
COMPARISON
OF
DIFFERENT
METHODS
FOR
DETERMINATION
OF
HEAT
CAPACITIES
IN
THE
DSC
.............................................................................................................
57
4.2.2
APPROACH:
INFLUENCE
OF
PRESSURE
ON
HEAT
CAPACITIES
IN
HIGH-PRESSURE
CRUCIBLES
60
4.2.3
COMPARISON
OF
DIFFERENT
METHODS
FOR
DETERMINATION
OF
HEAT
CAPACITIES
IN
THE
TRANSITIOMETER
...........................................................................................
62
4.2.4
EVALUATION
OF
THE
THREE-STEP
METHOD
IN
THE
TRANSITIOMETER
........................
62
4.2.5
APPLICATION
OF
THE
TEMPERATURE-STEP
METHOD
IN
THE
TRANSITIOMETER
....
69
4.2.6
APPLICATION
OF
THE
PRESSURE-SCAN
METHOD
IN
THE
TRANSITIOMETER
...................
74
4.2.7
APPLICATION
OF
THE
PRESSURE-STEP
METHOD
IN
THE
TRANSITIOMETER
...................
78
4.2.8
CONCLUSIONS
TO
THE
METHOD
EVALUATION
IN
DSC
AND
TRANSITIOMETER
............
79
5
RESULTS:
MEASUREMENT
OF
THERMO-PHYSICAL
PROPERTIES
IN
THE
TRANSITIOMETER
81
5.1
PRESSURE
SCAN:
DENSITIES
..............................................................................................
81
5.1.1
EXCURSUS:
CALORIMETRIC
SIGNAL
AND
VOLUME-STEP
DUERING
PRESSURE-SCAN
EX
PERIMENTS
..............................................................................................
82
5.1.2
PRESSURE
SCAN
EXPERIMENTS:
DENSITIES
WITH
VOLUME
CORRECTION
..................
86
5.2
PRESSURE
SCAN:
EXPANSION
COEFFICIENTS
......................................................................
92
5.3
PRESSURE
SCAN:
HEAT
CAPACITIES
....................................................................................
102
5.3.1
IMPORTANT
PARAMETERS
IN
THE
EVALUATION
PROCEDURE
OF
HEAT
CAPACITIES
FROM
EXPANSION
COEFFICIENTS
........................................................................................
102
5.3.2
RESULTS
OF
HEAT
CAPACITIES
WITH
THE
PRESSURE-SCAN
METHOD
...........................
105
5.3.3
EXCURSUS:
COMPARING
THE
PRESSURE
DEPENDENCE
ON
HEAT
CAPACITIES
OF
POLYPROPYLENE
MEASURED
IN
TWO
DIFFERENT
DEVICES
AND
LABORATORIES
....
115
5.3.4
VALIDATION
OF
THE
PRESSURE-SCAN
WITH
THE
PRESSURE-STEP
METHOD
.....................
118
5.4
DEGRADATION
OF
POLYPROPYLENE
(AND
OTHER
POLYMERS)
WITH
TEMPERATURE
AND
TIME
.
127
5.4.1
PROGRESSION
OF
MOLECULAR
WEIGHT
WITH
TEMPERATURE
AND
TIME
.....................
127
5.4.2
DETERMINATION
OF
IMPACT
OF
MOLECULAR
WEIGHT
DEGRADATION
OF
POLYMER
SAMPLES
ON
THE
HEAT
CAPACITY
...........................................................................
132
5.5
APPROACH:
FITTING
OF
PC-SAFT
PARAMETERS
TO
MEASURED
HEAT
CAPACITIES
...............
137
5.6
APPLICATION
OF
EXPERIMENTALLY
DETERMINED
HEAT
CAPACITY
CORRELATIONS
IN
A
FICTIVE
TUBE
REACTOR
MODEL
.......................................................................................................
144
6
SUMMARY
149
7
OUTLOOK
AND
FUERTHER
RESEARCH
152
|
| adam_txt |
CONTENTS
1
INTRODUCTION
5
2
THEORY
8
2.1
THERMODYNAMICS
.
8
2.1.1
HEAT
AND
HEAT
CAPACITY
.
8
2.2
EQUATION
OF
STATE
(EOS)
.
14
2.2.1
REDLICH-KWONG-SOAVE
(RKS)
.
14
2.2.2
PENG-ROBINSON
(PR)
.
14
2.2.3
TAIT-EQUATION
.
15
2.2.4
LEE-KESLER-PLOECKER
(LKP)
.
15
2.2.5
EUROPEAN
GAS
RESEARCH
GROUP
MODEL
(GERG-MODEL)
.
15
2.2.6
PERTURBED-CHAIN
STATISTICAL-ASSOCIATING-FLUID-THEORY
(PC-SAFT)
.
16
2.3
THERMAL
ANALYSIS:
THE
CALORIMETER
.
18
2.3.1
EXPERIMENTAL
SET-UP
OF
CALORIMETERS
.
19
2.3.2
MEASURING
PRINCIPLES
FOR
HEAT
DETECTION
IN
CALORIMETERS
.
19
2.3.3
OPERATING
MODE
OF
A
CALORIMETER:
THERMODYNAMIC
CONDITIONS
DURING
A
MEASUREMENT
.
21
2.4
APPLICATION
OF
CALORIMETERS
IN
THERMAL
ANALYSIS:
DTA
AND
DSC
.
22
2.4.1
COMPARING
CALORIMETERS:
THE
TIME
CONSTANT
.
23
2.4.2
CALIBRATION
OF
CALORIMETERS
AND
REFERENCE
SUBSTANCES
.
26
2.5
METHODS
FOR
EXPERIMENTAL
DETERMINATION
OF
HEAT
CAPACITIES
.
27
2.5.1
RESISTANCE
WIRE
.
27
2.5.2
FLOW
CALORIMETRY
.
28
2.5.3
SPEED
OF
SOUND
.
28
2.5.4
DIFFERENCE
SCANNING
CALORIMETRY:
THREE-STEP
METHOD
.
29
2.5.5
DIFFERENCE
SCANNING
CALORIMETRY:
TWO-STEP
METHOD
.
30
2.5.6
DIFFERENCE
SCANNING
CALORIMETRY:
TEMPERATURE-STEP
METHOD
.
31
2.5.7
DIFFERENCE
SCANNING
CALORIMETRY:
PRESSURE-SCAN
METHOD
.
32
2.5.8
DIFFERENCE
SCANNING
CALORIMETRY:
PRESSURE-STEP
METHOD
.
34
2.5.9
DIFFERENCE
SCANNING
CALORIMETRY:
TEMPERATURE
MODULATION
.
35
3
EXPERIMENTAL
SECTION
38
3.1
DSC
.
38
3.1.1
ALUMINIUM
CRUCIBLES
.
39
3.1.2
HIGH-PRESSURE
STEEL
CRUCIBLES
AND
THEIR
CLOSING
UNDER
PRESSURE
.
39
3.2
TRANSITIOMETER
.
40
3.2.1
INDICATION
AND
REGULATION
.
43
3.2.2
MEASUREMENT
CELIS
.
45
3.2.3
OPTIONAL
SAMPLE
CONTAINERS:
THE
AMPOULES
.
47
3.3
SIZE
EXCLUSION
CHROMATOGRAPHY
SEC
.
49
4
METHOD
EVALUATION:
DETERMINING
A
PRESSURE
DEPENDENCE
ON
HEAT
CAPACITIES
BY
CALORIMETRY
51
4.1
TIME
CONSTANTS
OF
APPLIED
CALORIMETERS
.
51
4.2
METHOD
PROCESSING
FOR
DETERMINING
HEAT
CAPACITIES
BY
CALORIMETRY
.
53
4.2.1
COMPARISON
OF
DIFFERENT
METHODS
FOR
DETERMINATION
OF
HEAT
CAPACITIES
IN
THE
DSC
.
57
4.2.2
APPROACH:
INFLUENCE
OF
PRESSURE
ON
HEAT
CAPACITIES
IN
HIGH-PRESSURE
CRUCIBLES
60
4.2.3
COMPARISON
OF
DIFFERENT
METHODS
FOR
DETERMINATION
OF
HEAT
CAPACITIES
IN
THE
TRANSITIOMETER
.
62
4.2.4
EVALUATION
OF
THE
THREE-STEP
METHOD
IN
THE
TRANSITIOMETER
.
62
4.2.5
APPLICATION
OF
THE
TEMPERATURE-STEP
METHOD
IN
THE
TRANSITIOMETER
.
69
4.2.6
APPLICATION
OF
THE
PRESSURE-SCAN
METHOD
IN
THE
TRANSITIOMETER
.
74
4.2.7
APPLICATION
OF
THE
PRESSURE-STEP
METHOD
IN
THE
TRANSITIOMETER
.
78
4.2.8
CONCLUSIONS
TO
THE
METHOD
EVALUATION
IN
DSC
AND
TRANSITIOMETER
.
79
5
RESULTS:
MEASUREMENT
OF
THERMO-PHYSICAL
PROPERTIES
IN
THE
TRANSITIOMETER
81
5.1
PRESSURE
SCAN:
DENSITIES
.
81
5.1.1
EXCURSUS:
CALORIMETRIC
SIGNAL
AND
VOLUME-STEP
DUERING
PRESSURE-SCAN
EX
PERIMENTS
.
82
5.1.2
PRESSURE
SCAN
EXPERIMENTS:
DENSITIES
WITH
VOLUME
CORRECTION
.
86
5.2
PRESSURE
SCAN:
EXPANSION
COEFFICIENTS
.
92
5.3
PRESSURE
SCAN:
HEAT
CAPACITIES
.
102
5.3.1
IMPORTANT
PARAMETERS
IN
THE
EVALUATION
PROCEDURE
OF
HEAT
CAPACITIES
FROM
EXPANSION
COEFFICIENTS
.
102
5.3.2
RESULTS
OF
HEAT
CAPACITIES
WITH
THE
PRESSURE-SCAN
METHOD
.
105
5.3.3
EXCURSUS:
COMPARING
THE
PRESSURE
DEPENDENCE
ON
HEAT
CAPACITIES
OF
POLYPROPYLENE
MEASURED
IN
TWO
DIFFERENT
DEVICES
AND
LABORATORIES
.
115
5.3.4
VALIDATION
OF
THE
PRESSURE-SCAN
WITH
THE
PRESSURE-STEP
METHOD
.
118
5.4
DEGRADATION
OF
POLYPROPYLENE
(AND
OTHER
POLYMERS)
WITH
TEMPERATURE
AND
TIME
.
127
5.4.1
PROGRESSION
OF
MOLECULAR
WEIGHT
WITH
TEMPERATURE
AND
TIME
.
127
5.4.2
DETERMINATION
OF
IMPACT
OF
MOLECULAR
WEIGHT
DEGRADATION
OF
POLYMER
SAMPLES
ON
THE
HEAT
CAPACITY
.
132
5.5
APPROACH:
FITTING
OF
PC-SAFT
PARAMETERS
TO
MEASURED
HEAT
CAPACITIES
.
137
5.6
APPLICATION
OF
EXPERIMENTALLY
DETERMINED
HEAT
CAPACITY
CORRELATIONS
IN
A
FICTIVE
TUBE
REACTOR
MODEL
.
144
6
SUMMARY
149
7
OUTLOOK
AND
FUERTHER
RESEARCH
152 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Nowottny, Jonas |
| author_GND | (DE-588)1236782127 |
| author_facet | Nowottny, Jonas |
| author_role | aut |
| author_sort | Nowottny, Jonas |
| author_variant | j n jn |
| building | Verbundindex |
| bvnumber | BV047567784 |
| ctrlnum | (OCoLC)1273497470 (DE-599)DNB1233939998 |
| dewey-full | 541.36 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.36 |
| dewey-search | 541.36 |
| dewey-sort | 3541.36 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV047567784 |
| illustrated | Illustrated |
| index_date | 2024-07-03T18:29:21Z |
| indexdate | 2024-07-10T09:15:05Z |
| institution | BVB |
| institution_GND | (DE-588)1064118135 |
| isbn | 9783844080742 3844080740 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032953466 |
| oclc_num | 1273497470 |
| open_access_boolean | |
| owner | DE-634 |
| owner_facet | DE-634 |
| physical | i, 154, XIV Seiten Illustrationen, Diagramme |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| publisher | Shaker Verlag |
| record_format | marc |
| series | Darmstädter Schriftenreihe der Polymerisationstechnik |
| series2 | Darmstädter Schriftenreihe der Polymerisationstechnik |
| spelling | Nowottny, Jonas Verfasser (DE-588)1236782127 aut High-pressure calorimetry: evaluation of methods and measurement of heat capacities Jonas Nowottny Düren Shaker Verlag 2021 i, 154, XIV Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Darmstädter Schriftenreihe der Polymerisationstechnik 18 Dissertation Technische Universität Darmstadt 2021 Wärmekapazität (DE-588)4188854-6 gnd rswk-swf Differential scanning calorimetry (DE-588)4320176-3 gnd rswk-swf Hochdruckkalorimetrie (DE-588)4160103-8 gnd rswk-swf Messung (DE-588)4038852-9 gnd rswk-swf Calorimetry Pressure Heat Capacities PC-SAFT (DE-588)4113937-9 Hochschulschrift gnd-content Wärmekapazität (DE-588)4188854-6 s Messung (DE-588)4038852-9 s Differential scanning calorimetry (DE-588)4320176-3 s Hochdruckkalorimetrie (DE-588)4160103-8 s DE-604 Shaker Verlag (DE-588)1064118135 pbl Darmstädter Schriftenreihe der Polymerisationstechnik 18 (DE-604)BV040030872 18 B:DE-101 application/pdf https://d-nb.info/1233939998/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032953466&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p aepkn-pa 0,72695 20210809 DE-101 https://d-nb.info/provenance/plan#aepkn-pa 2\p dnb 20210817 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Nowottny, Jonas High-pressure calorimetry: evaluation of methods and measurement of heat capacities Darmstädter Schriftenreihe der Polymerisationstechnik Wärmekapazität (DE-588)4188854-6 gnd Differential scanning calorimetry (DE-588)4320176-3 gnd Hochdruckkalorimetrie (DE-588)4160103-8 gnd Messung (DE-588)4038852-9 gnd |
| subject_GND | (DE-588)4188854-6 (DE-588)4320176-3 (DE-588)4160103-8 (DE-588)4038852-9 (DE-588)4113937-9 |
| title | High-pressure calorimetry: evaluation of methods and measurement of heat capacities |
| title_auth | High-pressure calorimetry: evaluation of methods and measurement of heat capacities |
| title_exact_search | High-pressure calorimetry: evaluation of methods and measurement of heat capacities |
| title_exact_search_txtP | High-pressure calorimetry: evaluation of methods and measurement of heat capacities |
| title_full | High-pressure calorimetry: evaluation of methods and measurement of heat capacities Jonas Nowottny |
| title_fullStr | High-pressure calorimetry: evaluation of methods and measurement of heat capacities Jonas Nowottny |
| title_full_unstemmed | High-pressure calorimetry: evaluation of methods and measurement of heat capacities Jonas Nowottny |
| title_short | High-pressure calorimetry: evaluation of methods and measurement of heat capacities |
| title_sort | high pressure calorimetry evaluation of methods and measurement of heat capacities |
| topic | Wärmekapazität (DE-588)4188854-6 gnd Differential scanning calorimetry (DE-588)4320176-3 gnd Hochdruckkalorimetrie (DE-588)4160103-8 gnd Messung (DE-588)4038852-9 gnd |
| topic_facet | Wärmekapazität Differential scanning calorimetry Hochdruckkalorimetrie Messung Hochschulschrift |
| url | https://d-nb.info/1233939998/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032953466&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV040030872 |
| work_keys_str_mv | AT nowottnyjonas highpressurecalorimetryevaluationofmethodsandmeasurementofheatcapacities AT shakerverlag highpressurecalorimetryevaluationofmethodsandmeasurementofheatcapacities |
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