Diethylamide and tetraethylaluminate chemistry of the rare earth metals:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Tübingen
[2018]
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | 160 Seiten Illustrationen, Diagramme 21 cm |
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MARC
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| 100 | 1 | |a Krenzer, Andreas |e Verfasser |0 (DE-588)1216846138 |4 aut | |
| 245 | 1 | 0 | |a Diethylamide and tetraethylaluminate chemistry of the rare earth metals |c vorgelegt von Dipl. Chem. Andreas Krenzer |
| 264 | 1 | |a Tübingen |c [2018] | |
| 300 | |a 160 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Eberhard Karls Universität Tübingen |d 2018 | ||
| 650 | 0 | 7 | |a Aluminate |0 (DE-588)4307669-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Seltenerdmetallkomplexe |0 (DE-588)4386077-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Diethylamin |0 (DE-588)4711939-1 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Seltenerdmetallkomplexe |0 (DE-588)4386077-1 |D s |
| 689 | 0 | 1 | |a Diethylamin |0 (DE-588)4711939-1 |D s |
| 689 | 0 | 2 | |a Aluminate |0 (DE-588)4307669-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 710 | 2 | |a Eberhard Karls Universität Tübingen |0 (DE-588)36187-2 |4 dgg | |
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Record in the Search Index
| _version_ | 1804182557779034112 |
|---|---|
| adam_text | ABBREVIATIONS
CHAPTER
1
:
GENERAL
INTRODUCTION
1
1.1
CHEMISTRY
OF
THE
RARE
EARTH
METALS
1
1.2
ZIEGLER-NATTA
CATALYSIS
2
1.3
OUTLINE
ABOUT
THE
RARE
EARTH
METAL
ETHYL
ALUMINATES
5
1.4
RARE
EARTH
METAL
(LN
3+
)
AMIDES
9
CHAPTER
2
:
MOTIVATION
13
CHAPTER
3
:
HOMOLEPTIC
TETRAETHYLALUMINATES
OF
THE
RARE
EARTH
METALS
17
3.1
DETERMINATION
OF
THE
SMALLEST
ISOLABLE
LN(AIET
4
)
3
17
3.2
ATTEMPT
TO
SYNTHESIS
OF
SM(AIE1
4
)
3
AT
LOW
TEMPERATURES
AND
REDUCTION
TO
[SM(AIET
4
)
2
]
N
19
3.3
CONCLUSION
21
CHAPTER
4
:
FROM
THE
NOVEL
BIS(TETRAETHYLALUMINATE)
LANTHANUM
COMPLEX
VIA
A-C-H
ACTIVATION
TO
THE
FIRST
RARE
EARTH
METAL
ETHYLIDENE
COMPLEX
22
4.1
INTRODUCTION
22
4.2
SYNTHESIS
AND
STRUCTURAL
CHARACTERIZATION
24
4.3
NMR
MECHANISTIC
STUDY
OF
THE
C-H
ACTIVATION
28
4.4
CONCLUSION
34
CHAPTER
5
:
SYNTHESIS
AND
CHARACTERIZATION
WITH
SUBSEQUENT
DECOMPOSITION
OF
Y(AIET
4
)
3
AS
WELL
AS
ATTEMPTED
CONVERSION
OF
THE
COMPLEX
35
5.1
INTRODUCTION
35
5.2.
CHARACTERIZATION
OF
Y(AIET
4
)
3
AND
THE
FIRST
DECOMPOSITION
PRODUCT
36
5.3
REACTION
OFF
KTP**
**
6
WITH
THE
CRUDE
MIXTURE
OF
Y(AIET
4
)
3
40
5.4
-NET
2
ROUTE
:
INVESTIGATION
OFF
THE
TEMPERATURE
DEPENDENT
PRODUCT
FORMATION
44
5.5
-NPH
2
ROUTE
:
ATTEMPT
TO
ISOLATE
THE
MAIN
BYPRODUCT
50
5.6
CONCLUSION
54
CHAPTER
6
:
POLYMERIZATION
PERFORMANCE
OF
THE
HOMOLEPTIC
TRIS(TETRAETHYLALUMINATE)
NEODYMIUM
55
6.1
INTRODUCTION
55
6.1.1
INTRODUCTION
TO
THE
DIENE
POLYMERIZATION
55
6.1.2
GENERAL
CONSIDERATION
RELATING
TO
THE
POLYMERIZATION
AND
POLYMERIZATION
RESULTS
56
6.2
COMPARISON
OF
ND(AIET
4
)3
VS.
ND(AIME
4
)
3
RELATING
TO
THE
ISOPRENE
POLYMERIZATION
57
6.3
CATALYTIC
PERFORMANCE
OF
ND(AIET
4
)
3
IN
DEPENDENCE
OF
THE
CHLORINATING
AGENT
IN
THE
RESPECTIVE
SOLVENT
59
6.4
FORMATION
OF
THE
ACTIVE
SPECIES
63
6.5
SOLVENT
INFLUENCE
AT
ND(AIET
4
)
3
/ME
2
AICI
AND
ND(AIET
4
)3/ETAICI
2
IN
DETAIL
66
6.6
CONCLUSION
68
CHAPTER
7
:
THE
RARE
EARTH
METAL
DIETHYLAMIDE
COMPLEXES
69
7.1
INTRODUCTION
69
7.2
SYNTHESIS
AND
CHARACTERIZATION
OF
[(NET
2
)
2
LN(P-NET
2
)(DO)]
2
70
7.3
SYNTHESIS
OF
DIETHYLAMIDE
COMPLEXES
OF
SCANDIUM
AND
INVESTIGATION
OF
THE
DONOR RARE
EARTH
METAL
BINDING
75
7.4
SYNTHESIS
AND
CHARACTERIZATION
OF
[(NNBU
2
)
2
Y(P-NNBU
2
)(THF)]
2
80
7.5
IMPLEMENTATION
OF
THE
SYNTHESIS
ROUTE
TO
THE
PARAMAGNETIC
LANTHANIDES
AND
APPLICATION
OF
THE
COMPLEX
[(NET
2
)
2
LN(P-NET
2
)(DO)]
82
7.5.1
SYNTHESIS
OF
[(NET
2
)
2
SM(P-NET
2
)(PY)]
2
82
7.5.2
APPLICATION
OF
[(NET
2
)
2
Y(P-NET
2
)(PY)]
2
:
TRANSAMINATION
83
7.5.3
POLYMERIZATION
WITH
[(NET
2
)
2
ND(P-NET
2
)(THF)]
2
AS
PRECURSOR
87
7.6
CONCLUSION
90
CHAPTER
8
:
STRUCTURAL
DIFFERENCES
BETWEEN
DIETHYLAMIDE
AND
DIISOPROPYLAMIDE
NEODYMIUM
COMPLEXES
AND
BIS(DIETHYLAMIDE)
YTTRIUM
HALFSANDWICH
COMPLEXES
FOR
FURTHER
INSIGHTS
IN
THE
DIETHYLAMIDE
COORDINATION
CHEMISTRY
92
8.1
INTRODUCTION
92
8.2
COMPARISON
OF
DIETHYLAMIDE
AND
DIISOPROPYLAMIDE
NEODYMIUM
COMPLEXES
93
8.3
INSIGHTS
TO
THE
COORDINATION
CHEMISTRY
OF
THE
DIETHYLAMIDE
COMPLEXES
BY
USAGE
OF
ANCILLARY
LIGANDS
96
8.4
CONCLUSION
103
ZUSAMMENFASSUNG
DER
ERGEBNISSE
104
SUPPLEMENTS
114
SUPPLEMENTS
CHAPTER
3
:
THE
HOMOLEPIC
TETRAETHYLALUMINATES
OF
THE
RARE
EARTH
METALS
115
SUPPLEMENTS
CHAPTER
4
:
FROM
THE
NOVEL
BIS(TETRAETHYLALUMINATE)
LANTHANUM
COMPLEX
VIA
A-H
ACTIVATION
TO
THE
FIRST
RARE-EARTH
METAL
ETHYLIDENE
COMPLEX
118
SUPPLEMENTS
CHAPTER
5
:
SYNTHESIS
AND
CHARACTERIZATION
WITH
SUBSEQUENT
DECOMPOSITION
OF
Y(AIET
4
)
3
AS
WELL
AS
ATTEMPTED
CONVERSION
OF
THE
COMPLEX
129
SUPPLEMENTS
CHAPTER
6
:
POLYMERIZATION
PERFORMANCE
OF
THE
HOMOLEPTIC
TRIS(TETRAETHYLALUMINATE)
NEODYMIUM
133
SUPPLEMENTS
CHAPTER
7
:
THE
RARE
EARTH
METAL
DIETHYLAMIDE
COMPLEXES
139
SUPPLEMENTS
CHAPTER
8
:
STRUCTURAL
DIFFERENCES
OF
THE
RARE
EARTH
METAL
DIETHYLAMIDE
VS
DIISOPROPYLEAMIDE
NEODYMIUM
COMPLEX
AND
BIS(DIETHYLAMIDE)YTTRIUM
HALFSANDWICH
COMPLEX
FOR
FURTHER
INSIGHTS
IN
THE
DIETHYLAMIDE
COORDINATION
CHEMISTRY
149
REFERENCES
153
FURTHER
CONTRIBUTION
160
|
| adam_txt |
ABBREVIATIONS
CHAPTER
1
:
GENERAL
INTRODUCTION
1
1.1
CHEMISTRY
OF
THE
RARE
EARTH
METALS
1
1.2
ZIEGLER-NATTA
CATALYSIS
2
1.3
OUTLINE
ABOUT
THE
RARE
EARTH
METAL
ETHYL
ALUMINATES
5
1.4
RARE
EARTH
METAL
(LN
3+
)
AMIDES
9
CHAPTER
2
:
MOTIVATION
13
CHAPTER
3
:
HOMOLEPTIC
TETRAETHYLALUMINATES
OF
THE
RARE
EARTH
METALS
17
3.1
DETERMINATION
OF
THE
SMALLEST
ISOLABLE
LN(AIET
4
)
3
17
3.2
ATTEMPT
TO
SYNTHESIS
OF
SM(AIE1
4
)
3
AT
LOW
TEMPERATURES
AND
REDUCTION
TO
[SM(AIET
4
)
2
]
N
19
3.3
CONCLUSION
21
CHAPTER
4
:
FROM
THE
NOVEL
BIS(TETRAETHYLALUMINATE)
LANTHANUM
COMPLEX
VIA
A-C-H
ACTIVATION
TO
THE
FIRST
RARE
EARTH
METAL
ETHYLIDENE
COMPLEX
22
4.1
INTRODUCTION
22
4.2
SYNTHESIS
AND
STRUCTURAL
CHARACTERIZATION
24
4.3
NMR
MECHANISTIC
STUDY
OF
THE
C-H
ACTIVATION
28
4.4
CONCLUSION
34
CHAPTER
5
:
SYNTHESIS
AND
CHARACTERIZATION
WITH
SUBSEQUENT
DECOMPOSITION
OF
Y(AIET
4
)
3
AS
WELL
AS
ATTEMPTED
CONVERSION
OF
THE
COMPLEX
35
5.1
INTRODUCTION
35
5.2.
CHARACTERIZATION
OF
Y(AIET
4
)
3
AND
THE
FIRST
DECOMPOSITION
PRODUCT
36
5.3
REACTION
OFF
KTP**
**
6
WITH
THE
CRUDE
MIXTURE
OF
Y(AIET
4
)
3
40
5.4
-NET
2
ROUTE
:
INVESTIGATION
OFF
THE
TEMPERATURE
DEPENDENT
PRODUCT
FORMATION
44
5.5
-NPH
2
ROUTE
:
ATTEMPT
TO
ISOLATE
THE
MAIN
BYPRODUCT
50
5.6
CONCLUSION
54
CHAPTER
6
:
POLYMERIZATION
PERFORMANCE
OF
THE
HOMOLEPTIC
TRIS(TETRAETHYLALUMINATE)
NEODYMIUM
55
6.1
INTRODUCTION
55
6.1.1
INTRODUCTION
TO
THE
DIENE
POLYMERIZATION
55
6.1.2
GENERAL
CONSIDERATION
RELATING
TO
THE
POLYMERIZATION
AND
POLYMERIZATION
RESULTS
56
6.2
COMPARISON
OF
ND(AIET
4
)3
VS.
ND(AIME
4
)
3
RELATING
TO
THE
ISOPRENE
POLYMERIZATION
57
6.3
CATALYTIC
PERFORMANCE
OF
ND(AIET
4
)
3
IN
DEPENDENCE
OF
THE
CHLORINATING
AGENT
IN
THE
RESPECTIVE
SOLVENT
59
6.4
FORMATION
OF
THE
ACTIVE
SPECIES
63
6.5
SOLVENT
INFLUENCE
AT
ND(AIET
4
)
3
/ME
2
AICI
AND
ND(AIET
4
)3/ETAICI
2
IN
DETAIL
66
6.6
CONCLUSION
68
CHAPTER
7
:
THE
RARE
EARTH
METAL
DIETHYLAMIDE
COMPLEXES
69
7.1
INTRODUCTION
69
7.2
SYNTHESIS
AND
CHARACTERIZATION
OF
[(NET
2
)
2
LN(P-NET
2
)(DO)]
2
70
7.3
SYNTHESIS
OF
DIETHYLAMIDE
COMPLEXES
OF
SCANDIUM
AND
INVESTIGATION
OF
THE
DONOR RARE
EARTH
METAL
BINDING
75
7.4
SYNTHESIS
AND
CHARACTERIZATION
OF
[(NNBU
2
)
2
Y(P-NNBU
2
)(THF)]
2
80
7.5
IMPLEMENTATION
OF
THE
SYNTHESIS
ROUTE
TO
THE
PARAMAGNETIC
LANTHANIDES
AND
APPLICATION
OF
THE
COMPLEX
[(NET
2
)
2
LN(P-NET
2
)(DO)]
82
7.5.1
SYNTHESIS
OF
[(NET
2
)
2
SM(P-NET
2
)(PY)]
2
82
7.5.2
APPLICATION
OF
[(NET
2
)
2
Y(P-NET
2
)(PY)]
2
:
TRANSAMINATION
83
7.5.3
POLYMERIZATION
WITH
[(NET
2
)
2
ND(P-NET
2
)(THF)]
2
AS
PRECURSOR
87
7.6
CONCLUSION
90
CHAPTER
8
:
STRUCTURAL
DIFFERENCES
BETWEEN
DIETHYLAMIDE
AND
DIISOPROPYLAMIDE
NEODYMIUM
COMPLEXES
AND
BIS(DIETHYLAMIDE)
YTTRIUM
HALFSANDWICH
COMPLEXES
FOR
FURTHER
INSIGHTS
IN
THE
DIETHYLAMIDE
COORDINATION
CHEMISTRY
92
8.1
INTRODUCTION
92
8.2
COMPARISON
OF
DIETHYLAMIDE
AND
DIISOPROPYLAMIDE
NEODYMIUM
COMPLEXES
93
8.3
INSIGHTS
TO
THE
COORDINATION
CHEMISTRY
OF
THE
DIETHYLAMIDE
COMPLEXES
BY
USAGE
OF
ANCILLARY
LIGANDS
96
8.4
CONCLUSION
103
ZUSAMMENFASSUNG
DER
ERGEBNISSE
104
SUPPLEMENTS
114
SUPPLEMENTS
CHAPTER
3
:
THE
HOMOLEPIC
TETRAETHYLALUMINATES
OF
THE
RARE
EARTH
METALS
115
SUPPLEMENTS
CHAPTER
4
:
FROM
THE
NOVEL
BIS(TETRAETHYLALUMINATE)
LANTHANUM
COMPLEX
VIA
A-H
ACTIVATION
TO
THE
FIRST
RARE-EARTH
METAL
ETHYLIDENE
COMPLEX
118
SUPPLEMENTS
CHAPTER
5
:
SYNTHESIS
AND
CHARACTERIZATION
WITH
SUBSEQUENT
DECOMPOSITION
OF
Y(AIET
4
)
3
AS
WELL
AS
ATTEMPTED
CONVERSION
OF
THE
COMPLEX
129
SUPPLEMENTS
CHAPTER
6
:
POLYMERIZATION
PERFORMANCE
OF
THE
HOMOLEPTIC
TRIS(TETRAETHYLALUMINATE)
NEODYMIUM
133
SUPPLEMENTS
CHAPTER
7
:
THE
RARE
EARTH
METAL
DIETHYLAMIDE
COMPLEXES
139
SUPPLEMENTS
CHAPTER
8
:
STRUCTURAL
DIFFERENCES
OF
THE
RARE
EARTH
METAL
DIETHYLAMIDE
VS
DIISOPROPYLEAMIDE
NEODYMIUM
COMPLEX
AND
BIS(DIETHYLAMIDE)YTTRIUM
HALFSANDWICH
COMPLEX
FOR
FURTHER
INSIGHTS
IN
THE
DIETHYLAMIDE
COORDINATION
CHEMISTRY
149
REFERENCES
153
FURTHER
CONTRIBUTION
160 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Krenzer, Andreas |
| author_GND | (DE-588)1216846138 |
| author_facet | Krenzer, Andreas |
| author_role | aut |
| author_sort | Krenzer, Andreas |
| author_variant | a k ak |
| building | Verbundindex |
| bvnumber | BV047341174 |
| ctrlnum | (OCoLC)1237352737 (DE-599)KXP1728089611 |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV047341174 |
| illustrated | Illustrated |
| index_date | 2024-07-03T17:34:27Z |
| indexdate | 2024-07-10T09:09:27Z |
| institution | BVB |
| institution_GND | (DE-588)36187-2 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032743573 |
| oclc_num | 1237352737 |
| open_access_boolean | |
| owner | DE-29T |
| owner_facet | DE-29T |
| physical | 160 Seiten Illustrationen, Diagramme 21 cm |
| publishDate | 2018 |
| publishDateSearch | 2018 |
| publishDateSort | 2018 |
| record_format | marc |
| spelling | Krenzer, Andreas Verfasser (DE-588)1216846138 aut Diethylamide and tetraethylaluminate chemistry of the rare earth metals vorgelegt von Dipl. Chem. Andreas Krenzer Tübingen [2018] 160 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Eberhard Karls Universität Tübingen 2018 Aluminate (DE-588)4307669-5 gnd rswk-swf Seltenerdmetallkomplexe (DE-588)4386077-1 gnd rswk-swf Diethylamin (DE-588)4711939-1 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Seltenerdmetallkomplexe (DE-588)4386077-1 s Diethylamin (DE-588)4711939-1 s Aluminate (DE-588)4307669-5 s DE-604 Eberhard Karls Universität Tübingen (DE-588)36187-2 dgg B:DE-101 application/pdf https://d-nb.info/1218084324/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032743573&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p dnb 20201016 DE-101 https://d-nb.info/provenance/plan#dnb |
| spellingShingle | Krenzer, Andreas Diethylamide and tetraethylaluminate chemistry of the rare earth metals Aluminate (DE-588)4307669-5 gnd Seltenerdmetallkomplexe (DE-588)4386077-1 gnd Diethylamin (DE-588)4711939-1 gnd |
| subject_GND | (DE-588)4307669-5 (DE-588)4386077-1 (DE-588)4711939-1 (DE-588)4113937-9 |
| title | Diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| title_auth | Diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| title_exact_search | Diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| title_exact_search_txtP | Diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| title_full | Diethylamide and tetraethylaluminate chemistry of the rare earth metals vorgelegt von Dipl. Chem. Andreas Krenzer |
| title_fullStr | Diethylamide and tetraethylaluminate chemistry of the rare earth metals vorgelegt von Dipl. Chem. Andreas Krenzer |
| title_full_unstemmed | Diethylamide and tetraethylaluminate chemistry of the rare earth metals vorgelegt von Dipl. Chem. Andreas Krenzer |
| title_short | Diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| title_sort | diethylamide and tetraethylaluminate chemistry of the rare earth metals |
| topic | Aluminate (DE-588)4307669-5 gnd Seltenerdmetallkomplexe (DE-588)4386077-1 gnd Diethylamin (DE-588)4711939-1 gnd |
| topic_facet | Aluminate Seltenerdmetallkomplexe Diethylamin Hochschulschrift |
| url | https://d-nb.info/1218084324/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032743573&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT krenzerandreas diethylamideandtetraethylaluminatechemistryoftherareearthmetals AT eberhardkarlsuniversitattubingen diethylamideandtetraethylaluminatechemistryoftherareearthmetals |
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