Lithic residue analysis: a review and guide to techniques
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| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Oxford
BAR Publishing
2021
|
| Series: | BAR
International Series ; 3023 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 107 Seiten Illustrationen, Diagramme |
| ISBN: | 9781407358024 |
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Record in the Search Index
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Contents List of Figures.1X List of Tables.χΐ List of Abbreviations.χϋ 1. Introduction.1 1.1. Why review lithic residue analysis?. 1 1.2. Who is this monograph for?.1 1.3. What types of archaeological residues can be found on stone tools? .1 1.4. Brief history. 2 2. Current Issues in Lithic Residue Analysis.5 2.1. Formation
mechanisms. 5 2.2. Preservation mechanisms. 5 2.3. Identification . 7 2.4. Contamination. 8 3. Visual Microscopy Techniques. 11 3.1. Microscopy: in situ.11 3.1.1. Reflected visible light microscopy (VLM).11 3.1.2. Laser scanning confocal microscopy (LSCM).12 3.1.3. Scanning electron microscopy (SEM). 13 3.1.4. Combined microscopic
approaches.15 3.2. Microscopy: extraction.16 3.2.1. Transmitted visible light microscopy.16 3.2.2. Stains.17 3.2.2.1. Iodine potassium iodide. 17 3.2.2.2. Phloroglucinol.17 3.2.2.3. Safranın.18 3.2.2.4. Congo red.18 3.2.2.5. Picrosirius red (PSR).18 3.2.2.6. Trypan
blue. 19 3.2.2.7. Rhodamine В.19 3.2.2.8. Eosin.19 3.2.2.9. Sudanin.19 3.2.2.10. Sudan IV. 20 3.2.2.11. Orange G. 20 3.2.2.12. Toluidine blue. 20 3.2.2.13. Methylene blue. 20 3.2.2.14. Wright’s stain. 20 3.2.3. Presumptive
tests. 21 3.2.3.1. Haemoglobin (Hb) crystallisation. 21 3.2.3.2. Dot blot test. 22 3.2.3.3. Urinalysis test strips. 22 3.2.3.4. Luminol. 23 4. Chemical Characterisation Techniques. 25 4.1. Chemical characterisation: elemental analysis techniques .25 4.1.1. Scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDS). 25 4.1.2. Rutherford backscattering spectrometry (RBS). 29 4.1.3. Particle-induced X-ray emission spectroscopy (PIXE).30 4.1.4. X-ray fluorescence spectroscopy
(XRF). 31 4.1.5. Energy dispersive X-ray fluorescence spectroscopy (EDXRF). 31 vii
Lithic Residue Analysis 4.1.6. Microscopic X-ray diffraction spectroscopy coupled with microscopic X-ray fluorescence spectroscopy (p-XRD-p-XRF). 32 4.1.7. Inductively coupled plasma atomic emission spectroscopy (ICP-AES).32 4.1.8. Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS).33 4.2. Chemical characterisation: molecular analysis techniques.33 4.2.1. Light-based spectroscopy techniques. 34 4.2.1.1. Fourier transform infrared spectroscopy (FTIR).34 4.2.1.2. Fourier transform infrared microspectroscopy (FTIRM).35 4.2.1.3. Raman spectroscopy.39 4.2.2. Chromatographic separation-based techniques.45 4.2.3. Mass spectrometry-based techniques. 46 4.2.3.1. Gas chromatography-mass spectrometry (GC-
MS).46 4.2.3.2. Other mass spectrometry-based techniques. 50 4.2.4. DNA techniques. 52 4.3. Chemical characterisation: crystal structure . 53 4.3.1. X-ray diffraction spectroscopy (XRD). 53 4.4. Chemical characterisation: immunological techniques for proteins.54 4.4.1. Crossover Immunoelectrophoresis (CIEP). 55 4.4.2. Enzyme linked immunosorbent assay (ELISA). 55 4.4.3. Radioimmunoassay (RIA). 56 4.4.4. Concerns and limitations of immunological methods. 56 4.4.5. Future work on ancient proteins. 58 4.5.
Chemical characterisation: summary. 59 5. Methodological Critique and Possible Solutions.61 5.1. Improving the impact of lithic residue studies. 61 5.2. Sampling .61 5.3. Use of artefacts from insecure contexts .61 5.4. Collection of sediment samples for comparison. 62 5.5. Storage.62 5.6. In situ versus extractive approach.62 5.7. Cleaning.63 5.8. Residue distribution mapping
.64 5.9. Problems with microscopic identification of residues by analogy. 65 5.10. Presentation of visual results.65 5.11. Best practice guide for lithic residue analysis.66 5.11.1. Essential planning.66 5.11.2. Excavation.67 5.11.3. Sample selection.67 5.11.4. Storage. 67 5.11.5. Prior to analysis. 67 5.11.5.1. Test consumables and lab spaces. 67
5.11.5.2. Artefact photography. 68 5.11.5.3. Artefact cleaning (or not). 68 5.11.6. Analysis. 68 5.11.6.1. Visual examination of in situ residues. 68 5.11.6.2. Chemical characterisation. 69 5.11.6.3. Experimental controls. 69 6. Conclusion.71 Appendix.73 References.79 viii |
| adam_txt |
Contents List of Figures.1X List of Tables.χΐ List of Abbreviations.χϋ 1. Introduction.1 1.1. Why review lithic residue analysis?. 1 1.2. Who is this monograph for?.1 1.3. What types of archaeological residues can be found on stone tools? .1 1.4. Brief history. 2 2. Current Issues in Lithic Residue Analysis.5 2.1. Formation
mechanisms. 5 2.2. Preservation mechanisms. 5 2.3. Identification . 7 2.4. Contamination. 8 3. Visual Microscopy Techniques. 11 3.1. Microscopy: in situ.11 3.1.1. Reflected visible light microscopy (VLM).11 3.1.2. Laser scanning confocal microscopy (LSCM).12 3.1.3. Scanning electron microscopy (SEM). 13 3.1.4. Combined microscopic
approaches.15 3.2. Microscopy: extraction.16 3.2.1. Transmitted visible light microscopy.16 3.2.2. Stains.17 3.2.2.1. Iodine potassium iodide. 17 3.2.2.2. Phloroglucinol.17 3.2.2.3. Safranın.18 3.2.2.4. Congo red.18 3.2.2.5. Picrosirius red (PSR).18 3.2.2.6. Trypan
blue. 19 3.2.2.7. Rhodamine В.19 3.2.2.8. Eosin.19 3.2.2.9. Sudanin.19 3.2.2.10. Sudan IV. 20 3.2.2.11. Orange G. 20 3.2.2.12. Toluidine blue. 20 3.2.2.13. Methylene blue. 20 3.2.2.14. Wright’s stain. 20 3.2.3. Presumptive
tests. 21 3.2.3.1. Haemoglobin (Hb) crystallisation. 21 3.2.3.2. Dot blot test. 22 3.2.3.3. Urinalysis test strips. 22 3.2.3.4. Luminol. 23 4. Chemical Characterisation Techniques. 25 4.1. Chemical characterisation: elemental analysis techniques .25 4.1.1. Scanning electron microscopy-energy dispersive X-ray spectroscopy (SEM-EDS). 25 4.1.2. Rutherford backscattering spectrometry (RBS). 29 4.1.3. Particle-induced X-ray emission spectroscopy (PIXE).30 4.1.4. X-ray fluorescence spectroscopy
(XRF). 31 4.1.5. Energy dispersive X-ray fluorescence spectroscopy (EDXRF). 31 vii
Lithic Residue Analysis 4.1.6. Microscopic X-ray diffraction spectroscopy coupled with microscopic X-ray fluorescence spectroscopy (p-XRD-p-XRF). 32 4.1.7. Inductively coupled plasma atomic emission spectroscopy (ICP-AES).32 4.1.8. Laser ablation inductively coupled plasma mass spectrometry (LA-ICP-MS).33 4.2. Chemical characterisation: molecular analysis techniques.33 4.2.1. Light-based spectroscopy techniques. 34 4.2.1.1. Fourier transform infrared spectroscopy (FTIR).34 4.2.1.2. Fourier transform infrared microspectroscopy (FTIRM).35 4.2.1.3. Raman spectroscopy.39 4.2.2. Chromatographic separation-based techniques.45 4.2.3. Mass spectrometry-based techniques. 46 4.2.3.1. Gas chromatography-mass spectrometry (GC-
MS).46 4.2.3.2. Other mass spectrometry-based techniques. 50 4.2.4. DNA techniques. 52 4.3. Chemical characterisation: crystal structure . 53 4.3.1. X-ray diffraction spectroscopy (XRD). 53 4.4. Chemical characterisation: immunological techniques for proteins.54 4.4.1. Crossover Immunoelectrophoresis (CIEP). 55 4.4.2. Enzyme linked immunosorbent assay (ELISA). 55 4.4.3. Radioimmunoassay (RIA). 56 4.4.4. Concerns and limitations of immunological methods. 56 4.4.5. Future work on ancient proteins. 58 4.5.
Chemical characterisation: summary. 59 5. Methodological Critique and Possible Solutions.61 5.1. Improving the impact of lithic residue studies. 61 5.2. Sampling .61 5.3. Use of artefacts from insecure contexts .61 5.4. Collection of sediment samples for comparison. 62 5.5. Storage.62 5.6. In situ versus extractive approach.62 5.7. Cleaning.63 5.8. Residue distribution mapping
.64 5.9. Problems with microscopic identification of residues by analogy. 65 5.10. Presentation of visual results.65 5.11. Best practice guide for lithic residue analysis.66 5.11.1. Essential planning.66 5.11.2. Excavation.67 5.11.3. Sample selection.67 5.11.4. Storage. 67 5.11.5. Prior to analysis. 67 5.11.5.1. Test consumables and lab spaces. 67
5.11.5.2. Artefact photography. 68 5.11.5.3. Artefact cleaning (or not). 68 5.11.6. Analysis. 68 5.11.6.1. Visual examination of in situ residues. 68 5.11.6.2. Chemical characterisation. 69 5.11.6.3. Experimental controls. 69 6. Conclusion.71 Appendix.73 References.79 viii |
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| illustrated | Illustrated |
| index_date | 2024-07-03T17:26:19Z |
| indexdate | 2024-07-20T06:12:06Z |
| institution | BVB |
| isbn | 9781407358024 |
| language | English |
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| physical | XII, 107 Seiten Illustrationen, Diagramme |
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| spelling | Croft, Shannon 1985- Verfasser (DE-588)1238534848 aut Lithic residue analysis a review and guide to techniques Shannon Croft Oxford BAR Publishing 2021 XII, 107 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier BAR : International Series 3023 Rückstandsanalyse (DE-588)4050855-9 gnd rswk-swf Steingerät (DE-588)4057175-0 gnd rswk-swf Archäologie, Methodenfragen (DE-2581)TH000012818 gbd Steingerät (DE-588)4057175-0 s Rückstandsanalyse (DE-588)4050855-9 s DE-604 Erscheint auch als Online-Ausgabe 978-1-4073-5803-1 BAR International Series ; 3023 (DE-604)BV023549802 3023 Digitalisierung BSB München - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032714990&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Croft, Shannon 1985- Lithic residue analysis a review and guide to techniques BAR Rückstandsanalyse (DE-588)4050855-9 gnd Steingerät (DE-588)4057175-0 gnd |
| subject_GND | (DE-588)4050855-9 (DE-588)4057175-0 |
| title | Lithic residue analysis a review and guide to techniques |
| title_auth | Lithic residue analysis a review and guide to techniques |
| title_exact_search | Lithic residue analysis a review and guide to techniques |
| title_exact_search_txtP | Lithic residue analysis a review and guide to techniques |
| title_full | Lithic residue analysis a review and guide to techniques Shannon Croft |
| title_fullStr | Lithic residue analysis a review and guide to techniques Shannon Croft |
| title_full_unstemmed | Lithic residue analysis a review and guide to techniques Shannon Croft |
| title_short | Lithic residue analysis |
| title_sort | lithic residue analysis a review and guide to techniques |
| title_sub | a review and guide to techniques |
| topic | Rückstandsanalyse (DE-588)4050855-9 gnd Steingerät (DE-588)4057175-0 gnd |
| topic_facet | Rückstandsanalyse Steingerät |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032714990&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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