Nanomechanics & nanorheology of polymer networks: An AFM study:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Berlin
2020
|
| Subjects: | |
| Online Access: | Abstract Inhaltsverzeichnis Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | 111 Seiten Illustrationen, Diagramme 30 cm |
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| 245 | 1 | 0 | |a Nanomechanics & nanorheology of polymer networks: An AFM study |c vorgelegt von Johannes Hellwig |
| 246 | 1 | 3 | |a Nanomechanics and nanorheology of polymer networks: An AFM study |
| 264 | 1 | |a Berlin |c 2020 | |
| 300 | |a 111 Seiten |b Illustrationen, Diagramme |c 30 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 502 | |b Dissertation |c Technische Universität Berlin |d 2020 | ||
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CONTENTS
1
INTRODUCTION
11
2
SCIENTIFIC
BACKGROUND
13
2.1
POLYELECTROLYTES
AND
POLYELECTROLYTE
MULTILAYERS
.
13
2.1.1
POLYELECTROLYTES
.
13
2.1.2
POLYELECTROLYTE
MULTILAYERS
.
13
2.1.3
ENERGETIC
CONSIDERATIONS
.
14
2.1.4
BUILD-UP
MECHANISM
OF
PEMS
.
15
2.1.5
PREPARATION
CONDITIONS
.
16
2.2
MECHANICAL
PROPERTIES
.
16
2.2.1
ELASTICITY:
STRESS
AND
STRAIN
.
17
2.2.2
VISCOELASTICITY
.
18
2.3
(NANO-)MECHANICS
OF
POLYMER
MATERIALS
AND
MEMBRANES
.
19
2.3.1
MECHANICAL
PROPERTIES
OF
POLYELECTROLYTE
MULTILAYERS
.
20
2.3.2
MECHANICAL
PROPERTIES
OF
BIOMATERIALS
.
20
2.4
POLY(L-LYSINE)
/
HYALURONIC
ACID
MULTILAYER
FILM
.
21
2.5
COLLAGEN
SCAFFOLDS
.
21
2.6
HETEROGENEOUS
POLYMER
GELS
.
22
3
METHODS
25
3.1
ATOMIC
FORCE
MICROSCOPY
(AFM)
.
25
3.1.1
PRINCIPLES
OF
ATOMIC
FORCE
MICROSCOPY
.
25
3.1.2
SCANNING
PROBE
AFM
.
26
3.1.3
STATIC
FORCE
MEASUREMENTS
.
27
3.1.4
HERTZ-,
JKR-,
DMT-
AND
DIMITRIADIS
MODEL
.
28
3.1.5
DYNAMIC
FORCE
MEASUREMENTS
.
30
3.1.6
RELAXATION
MEASUREMENTS
.
34
3.2
QUARTZ
CRYSTAL
MICROBALANCE
WITH
DISSIPATION
MONITORING
.
37
4
EXPERIMENTAL
SECTION
39
4.1
MATERIALS
.
39
4.2
PREPARATION
.
40
4.2.1
HA/PLL
MULTILAYERS:
LAYER-BY-LAYER
METHOD
.
40
4.2.2
HA/PLL
CROSSLINKING
.
40
4.2.3
NIPAM
MICROGEL
PARTICLES
.
41
4.2.4
NATIVE
COLLAGEN
FIBERS
.
41
4.2.5
HETEROGENEOUS
AND
HOMOGENEOUS
PNIPAM
GELS
.
42
2
CONTENTS
4.3
AFM
EXPERIMENTS
.
43
4.3.1
COLLOIDAL
PROBE
ATTACHMENT
.
43
4.3.2
STATIC
FORCE
MEASUREMENTS
ON
HA/PLL
MULTILAYERS
.
44
4.3.3
DYNAMIC
FORCE
MEASUREMENTS
ON
HA/PLL
MULTILAYERS
.
45
4.3.4
RELAXATION
MEASUREMENTS
.
46
4.3.5
FORCE
MEASUREMENTS
ON
HETEROGENEOUS
PNIPAM
GELS
.
46
4.4
QUARTZ
CRYSTAL
MICROBALANCE
WITH
DDISSIPATION
MONITORING
.
47
5
NANOSCALE
SEPARATION
OF
STORAGE
AND
LOSS
MODULUS
OF
A
PLL/HA
MULTILAYER
FILM
USING
DYNAMIC
FORCE
MEASUREMENTS 49
5.1
ABSTRACT
.
49
5.2
INTRODUCTION
.
50
5.3
HYDRODYNAMIC
DRAG
CORRECTION
.
51
5.4
RESULTS
.
52
5.5
DISCUSSION
.
55
5.6
SUMMARY
AND
CONCLUSION
.
58
6
EFFECTS
OF
ENVIRONMENTAL
PARAMETERS
ON
THE
MECHANICAL
PROPERTIES
OF
PLL/HA
MULTILAYER
FILMS 59
6.1
ABSTRACT
.
59
6.2
INTRODUCTION
.
60
6.3
RESULTS
AND
DISCUSSION
.
60
6.4
SUMMARY
AND
CONCLUSION
.
64
7
PLL/HA
MULTILAYERS
COATED
WITH
PNIPAM
MICROGELS
AND
THEIR
POTENTIAL
USE
AS
DRUG
DELIVERY
SYSTEM
65
7.1
ABSTRACT
.
65
7.2
INTRODUCTION
.
65
7.3
RESULTS
.
66
7.4
DISCUSSION
.
73
7.5
SUMMARY
AND
CONCLUSION
.
76
8
COMPARISON
BETWEEN
MACROSCOPIC
AND
MICROSCOPIC
ELASTICITY
OF
HETEROGE
NEOUS
POLYMER
GELS
77
8.1
ABSTRACT
.
77
8.2
INTRODUCTION
.
77
8.3
RESULTS
AND
DISCUSSION
.
78
8.4
SUMMARY
AND
CONCLUSION
.
87
CONTENTS
3
9
MEASURING
OF
CELL
EFFECTIVE
STIFFNESS
OF
MACROPOROUS
COLLAGEN
SCAFFOLDS
89
9.1
ABSTRACT
.
89
9.2
INTRODUCTION
.
89
9.3
SAMPLE
PREPARATION
.
90
9.4
RESULTS
.
91
9.5
DISCUSSION
.
96
9.6
SUMMARY
AND
CONCLUSION
.
97
10
SUMMARY
AND
OUTLOOK
99 |
| adam_txt |
CONTENTS
1
INTRODUCTION
11
2
SCIENTIFIC
BACKGROUND
13
2.1
POLYELECTROLYTES
AND
POLYELECTROLYTE
MULTILAYERS
.
13
2.1.1
POLYELECTROLYTES
.
13
2.1.2
POLYELECTROLYTE
MULTILAYERS
.
13
2.1.3
ENERGETIC
CONSIDERATIONS
.
14
2.1.4
BUILD-UP
MECHANISM
OF
PEMS
.
15
2.1.5
PREPARATION
CONDITIONS
.
16
2.2
MECHANICAL
PROPERTIES
.
16
2.2.1
ELASTICITY:
STRESS
AND
STRAIN
.
17
2.2.2
VISCOELASTICITY
.
18
2.3
(NANO-)MECHANICS
OF
POLYMER
MATERIALS
AND
MEMBRANES
.
19
2.3.1
MECHANICAL
PROPERTIES
OF
POLYELECTROLYTE
MULTILAYERS
.
20
2.3.2
MECHANICAL
PROPERTIES
OF
BIOMATERIALS
.
20
2.4
POLY(L-LYSINE)
/
HYALURONIC
ACID
MULTILAYER
FILM
.
21
2.5
COLLAGEN
SCAFFOLDS
.
21
2.6
HETEROGENEOUS
POLYMER
GELS
.
22
3
METHODS
25
3.1
ATOMIC
FORCE
MICROSCOPY
(AFM)
.
25
3.1.1
PRINCIPLES
OF
ATOMIC
FORCE
MICROSCOPY
.
25
3.1.2
SCANNING
PROBE
AFM
.
26
3.1.3
STATIC
FORCE
MEASUREMENTS
.
27
3.1.4
HERTZ-,
JKR-,
DMT-
AND
DIMITRIADIS
MODEL
.
28
3.1.5
DYNAMIC
FORCE
MEASUREMENTS
.
30
3.1.6
RELAXATION
MEASUREMENTS
.
34
3.2
QUARTZ
CRYSTAL
MICROBALANCE
WITH
DISSIPATION
MONITORING
.
37
4
EXPERIMENTAL
SECTION
39
4.1
MATERIALS
.
39
4.2
PREPARATION
.
40
4.2.1
HA/PLL
MULTILAYERS:
LAYER-BY-LAYER
METHOD
.
40
4.2.2
HA/PLL
CROSSLINKING
.
40
4.2.3
NIPAM
MICROGEL
PARTICLES
.
41
4.2.4
NATIVE
COLLAGEN
FIBERS
.
41
4.2.5
HETEROGENEOUS
AND
HOMOGENEOUS
PNIPAM
GELS
.
42
2
CONTENTS
4.3
AFM
EXPERIMENTS
.
43
4.3.1
COLLOIDAL
PROBE
ATTACHMENT
.
43
4.3.2
STATIC
FORCE
MEASUREMENTS
ON
HA/PLL
MULTILAYERS
.
44
4.3.3
DYNAMIC
FORCE
MEASUREMENTS
ON
HA/PLL
MULTILAYERS
.
45
4.3.4
RELAXATION
MEASUREMENTS
.
46
4.3.5
FORCE
MEASUREMENTS
ON
HETEROGENEOUS
PNIPAM
GELS
.
46
4.4
QUARTZ
CRYSTAL
MICROBALANCE
WITH
DDISSIPATION
MONITORING
.
47
5
NANOSCALE
SEPARATION
OF
STORAGE
AND
LOSS
MODULUS
OF
A
PLL/HA
MULTILAYER
FILM
USING
DYNAMIC
FORCE
MEASUREMENTS 49
5.1
ABSTRACT
.
49
5.2
INTRODUCTION
.
50
5.3
HYDRODYNAMIC
DRAG
CORRECTION
.
51
5.4
RESULTS
.
52
5.5
DISCUSSION
.
55
5.6
SUMMARY
AND
CONCLUSION
.
58
6
EFFECTS
OF
ENVIRONMENTAL
PARAMETERS
ON
THE
MECHANICAL
PROPERTIES
OF
PLL/HA
MULTILAYER
FILMS 59
6.1
ABSTRACT
.
59
6.2
INTRODUCTION
.
60
6.3
RESULTS
AND
DISCUSSION
.
60
6.4
SUMMARY
AND
CONCLUSION
.
64
7
PLL/HA
MULTILAYERS
COATED
WITH
PNIPAM
MICROGELS
AND
THEIR
POTENTIAL
USE
AS
DRUG
DELIVERY
SYSTEM
65
7.1
ABSTRACT
.
65
7.2
INTRODUCTION
.
65
7.3
RESULTS
.
66
7.4
DISCUSSION
.
73
7.5
SUMMARY
AND
CONCLUSION
.
76
8
COMPARISON
BETWEEN
MACROSCOPIC
AND
MICROSCOPIC
ELASTICITY
OF
HETEROGE
NEOUS
POLYMER
GELS
77
8.1
ABSTRACT
.
77
8.2
INTRODUCTION
.
77
8.3
RESULTS
AND
DISCUSSION
.
78
8.4
SUMMARY
AND
CONCLUSION
.
87
CONTENTS
3
9
MEASURING
OF
CELL
EFFECTIVE
STIFFNESS
OF
MACROPOROUS
COLLAGEN
SCAFFOLDS
89
9.1
ABSTRACT
.
89
9.2
INTRODUCTION
.
89
9.3
SAMPLE
PREPARATION
.
90
9.4
RESULTS
.
91
9.5
DISCUSSION
.
96
9.6
SUMMARY
AND
CONCLUSION
.
97
10
SUMMARY
AND
OUTLOOK
99 |
| any_adam_object | 1 |
| any_adam_object_boolean | 1 |
| author | Hellwig, Johannes |
| author_GND | (DE-588)1228287147 |
| author_facet | Hellwig, Johannes |
| author_role | aut |
| author_sort | Hellwig, Johannes |
| author_variant | j h jh |
| building | Verbundindex |
| bvnumber | BV047212735 |
| classification_rvk | VE 7007 |
| ctrlnum | (OCoLC)1245340474 (DE-599)DNB1226712592 |
| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| format | Thesis Book |
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| id | DE-604.BV047212735 |
| illustrated | Illustrated |
| index_date | 2024-07-03T16:54:54Z |
| indexdate | 2025-02-11T19:01:01Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032617514 |
| oclc_num | 1245340474 |
| open_access_boolean | |
| owner | DE-83 |
| owner_facet | DE-83 |
| physical | 111 Seiten Illustrationen, Diagramme 30 cm |
| publishDate | 2020 |
| publishDateSearch | 2020 |
| publishDateSort | 2020 |
| record_format | marc |
| spelling | Hellwig, Johannes Verfasser (DE-588)1228287147 aut Nanomechanics & nanorheology of polymer networks: An AFM study vorgelegt von Johannes Hellwig Nanomechanics and nanorheology of polymer networks: An AFM study Berlin 2020 111 Seiten Illustrationen, Diagramme 30 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Technische Universität Berlin 2020 Rasterkraftmikroskop (DE-588)4333578-0 gnd rswk-swf Mechanische Eigenschaft (DE-588)4217961-0 gnd rswk-swf Nanomechanik (DE-588)1084609584 gnd rswk-swf Hydrogel (DE-588)4160909-8 gnd rswk-swf Polymeres Netzwerk (DE-588)4307122-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Mechanische Eigenschaft (DE-588)4217961-0 s Rasterkraftmikroskop (DE-588)4333578-0 s Nanomechanik (DE-588)1084609584 s Polymeres Netzwerk (DE-588)4307122-3 s Hydrogel (DE-588)4160909-8 s DE-604 https://services.ub.tu-berlin.de/abstracts/diss/hellwig_johannes_abstract.pdf Abstract https://services.ub.tu-berlin.de/abstracts/diss/hellwig_johannes_inhalt.pdf Inhaltsverzeichnis B:DE-101 application/pdf https://d-nb.info/1226712592/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032617514&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hellwig, Johannes Nanomechanics & nanorheology of polymer networks: An AFM study Rasterkraftmikroskop (DE-588)4333578-0 gnd Mechanische Eigenschaft (DE-588)4217961-0 gnd Nanomechanik (DE-588)1084609584 gnd Hydrogel (DE-588)4160909-8 gnd Polymeres Netzwerk (DE-588)4307122-3 gnd |
| subject_GND | (DE-588)4333578-0 (DE-588)4217961-0 (DE-588)1084609584 (DE-588)4160909-8 (DE-588)4307122-3 (DE-588)4113937-9 |
| title | Nanomechanics & nanorheology of polymer networks: An AFM study |
| title_alt | Nanomechanics and nanorheology of polymer networks: An AFM study |
| title_auth | Nanomechanics & nanorheology of polymer networks: An AFM study |
| title_exact_search | Nanomechanics & nanorheology of polymer networks: An AFM study |
| title_exact_search_txtP | Nanomechanics & nanorheology of polymer networks: An AFM study |
| title_full | Nanomechanics & nanorheology of polymer networks: An AFM study vorgelegt von Johannes Hellwig |
| title_fullStr | Nanomechanics & nanorheology of polymer networks: An AFM study vorgelegt von Johannes Hellwig |
| title_full_unstemmed | Nanomechanics & nanorheology of polymer networks: An AFM study vorgelegt von Johannes Hellwig |
| title_short | Nanomechanics & nanorheology of polymer networks: An AFM study |
| title_sort | nanomechanics nanorheology of polymer networks an afm study |
| topic | Rasterkraftmikroskop (DE-588)4333578-0 gnd Mechanische Eigenschaft (DE-588)4217961-0 gnd Nanomechanik (DE-588)1084609584 gnd Hydrogel (DE-588)4160909-8 gnd Polymeres Netzwerk (DE-588)4307122-3 gnd |
| topic_facet | Rasterkraftmikroskop Mechanische Eigenschaft Nanomechanik Hydrogel Polymeres Netzwerk Hochschulschrift |
| url | https://services.ub.tu-berlin.de/abstracts/diss/hellwig_johannes_abstract.pdf https://services.ub.tu-berlin.de/abstracts/diss/hellwig_johannes_inhalt.pdf https://d-nb.info/1226712592/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=032617514&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT hellwigjohannes nanomechanicsnanorheologyofpolymernetworksanafmstudy AT hellwigjohannes nanomechanicsandnanorheologyofpolymernetworksanafmstudy |
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