Industrial separation processes: fundamentals
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| Main Authors: | , , |
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| Format: | Book |
| Language: | English |
| Published: |
Berlin
De Gruyter
[2020]
|
| Edition: | 2nd edition |
| Series: | De Gruyter graduate
|
| Subjects: | |
| Online Access: | Unbekannt Inhaltsverzeichnis |
| Physical Description: | XV, 439 Seiten Illustrationen, Diagramme |
| ISBN: | 9783110654738 3110654733 |
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MARC
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| 100 | 1 | |a Haan, André B. de |d 1964- |e Verfasser |0 (DE-588)1036241904 |4 aut | |
| 245 | 1 | 0 | |a Industrial separation processes |b fundamentals |c André B. de Haan, H. Burak Eral, Boelo Schuur |
| 250 | |a 2nd edition | ||
| 264 | 1 | |a Berlin |b De Gruyter |c [2020] | |
| 264 | 4 | |c © 2020 | |
| 300 | |a XV, 439 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a De Gruyter graduate | |
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| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Eral, H. Burak |e Verfasser |0 (DE-588)1215048742 |4 aut | |
| 700 | 1 | |a Schuur, Boelo |d 1978- |e Verfasser |0 (DE-588)1215047959 |4 aut | |
| 710 | 2 | |a Walter de Gruyter GmbH & Co. KG |0 (DE-588)10095502-2 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-11-065480-6 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-11-065491-2 |
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Record in the Search Index
| DE-BY-862_location | 2000 |
|---|---|
| DE-BY-FWS_call_number | 2000/VN 7121 H111(2) |
| DE-BY-FWS_katkey | 924147 |
| DE-BY-FWS_media_number | 083000522303 |
| _version_ | 1824555129665224704 |
| adam_text | CONTENTS
PREFACE
*
V
CHAPTER
1
CHARACTERISTICS
OF
SEPARATION
PROCESSES
*
1
1.1
1.2
1.2.1
1.2.2
1.2.3
1.3
1.3.1
1.3.2
1.4
1.4.1
1.4.2
SIGNIFICANCE
OF
SEPARATIONS
*
1
CHARACTERISTICS
OF
SEPARATION
PROCESSES
*
4
CATEGORIZATION
*
4
SEPARATING
AGENTS
*
5
SEPARATION
FACTORS
*
7
INDUSTRIAL
SEPARATION
METHODS
*
8
EXPLOITABLE
PROPERTIES
*
8
IMPORTANT
MOLECULAR
SEPARATIONS
*
10
INHERENT
SELECTIVITY
*
11
EQUILIBRIUM-BASED
PROCESSES
*
11
RATE-CONTROLLED
PROCESSES
*
13
NOMENCLATURE
*
14
EXERCISES
*
14
CHAPTER
2
EVAPORATION
AND
DISTILLATION
*
17
2.1
2.1.1
2.1.2
2.2
2.2.1
2.2.2
2.2.2.1
2.2.2.2
2.3
2.3.1
2.3.2
2.3.3
2.3.4
2.4
2.4.1
2.4.1.1
2.4.1.2
2.4.1.3
2.4.1.4
2.4.2
SEPARATION
BY
EVAPORATION
*
17
INTRODUCTION
*
17
VAPOR-LIQUID
EQUILIBRIA
*
18
SEPARATION
BY
SINGLE-STAGE
PARTIAL
EVAPORATION
*
23
DIFFERENTIAL
DISTILLATION
*
23
FLASH
DISTILLATION
*
24
SPECIFYING
T
AND
L/V
-----
26
SPECIFYING
T
AND
P
TOT
-----26
MULTISTAGE
DISTILLATION
*
28
DISTILLATION
CASCADES
*
28
COLUMN
DISTILLATION
*
29
FEASIBLE
DISTILLATION
CONDITIONS
*
31
EXTERNAL
COLUMN
BALANCES
*
31
MCCABE-THIELE
ANALYSIS
*
32
INTERNAL
BALANCES
*
32
RECTIFYING
SECTION
*
33
STRIPPING
SECTION
*
34
FEED
STAGE
CONSIDERATIONS
*
35
FEED
LINE
*
36
REQUIRED
NUMBER
OF
EQUILIBRIUM
STAGES
*
37
VIII
CONTENTS
2.4.2.1
2.4.2.2
2.4.23
2.4.2.4
2.4.3
2.5
2.5.1
2.5.2
2.5.3
GRAPHICAL
DETERMINATION
OF
STAGES
AND
LOCATION
OF
FEED
STAGE
-----
37
LIMITING
CONDITIONS
-----
40
FENSKE
AND
UNDERWOOD
EQUATIONS
*
41
USE
OF
MURPHREE
EFFICIENCY
-----
44
ENERGY
REQUIREMENTS
*
45
ADVANCED
DISTILLATION
TECHNIQUES
*
45
BATCH
DISTILLATION
-----
45
CONTINUOUS
SEPARATION
OF
MULTIPLE
PRODUCT
MIXTURES
*
47
SEPARATION
OF
AZEOTROPES
*
48
NOMENCLATURE
*
50
EXERCISES
-----
51
CHAPTER
3
ABSORPTION
AND
STRIPPING
*
57
3.1
3.2
3.3
3.4
3.4.1
3.4.2
3.5
3.5.1
3.5.2
3.5.3
3.6
3.6.1
3.6.2
3.6.3
3.6.4
INTRODUCTION
*
57
THE
AIM
OF
ABSORPTION
*
59
GENERAL
DESIGN
APPROACH
*
60
ABSORPTION
AND
STRIPPING
EQUILIBRIA
*
61
GASEOUS
SOLUTE
SOLUBILITIES
*
61
MINIMUM
ABSORBENT
FLOW
*
63
ABSORBER
AND
STRIPPER
DESIGN
*
64
OPERATING
LINES
FOR
ABSORPTION
*
64
STRIPPING
ANALYSIS
*
68
ANALYTICAL
KREMSER
SOLUTION
*
69
INDUSTRIAL
ABSORBERS
*
72
PACKED
COLUMNS
*
73
PLATE
COLUMNS
*
74
SPRAY
AND
BUBBLE
COLUMNS
*
74
COMPARISON
OF
ABSORPTION
COLUMNS
*
75
NOMENCLATURE
*
77
EXERCISES
-----
77
CHAPTER
4
GENERAL
DESIGN
OF
GAS/LIQUID
CONTACTORS
*
81
4.1
4.2
4.3
4.3.1
4.3.2
4.3.2.1
43.2.2
4.3.23
INTRODUCTION
*
81
MODELING
MASS
TRANSFER
*
81
PLATE
COLUMNS
*
86
DIMENSIONING
A
TRAY
COLUMN
*
89
HEIGHT
OF
A
TRAY
COLUMN
*
90
TRAY
SPACING
*
90
TRAY
EFFICIENCY
*
90
TRANSFER
UNITS
*
92
CONTENTS
*
IX
4.3.2.4
OVERALL
EFFICIENCY
-----
93
4.3.3
DIAMETER
OF
A
TRAY
COLUMN
*
95
4.3.3.1
FLOODING
-----
96
4.3.3.2
DOWNCOMER
FLOODING
-----
97
4.33.3
ENTRAINMENT
FLOODING
*
99
4.33.4
TRAY
DIAMETER
AND
PRESSURE
DROP
*
100
4.33.5
REMARK
ON
FLOODING
CHARTS
*
100
4.4
PACKED
COLUMNS
-----
101
4.4.1
RANDOM
PACKING
*
102
4.4.2
STRUCTURED
PACKING
-----
103
4.4.3
DIMENSIONING
A
PACKED
COLUMN
*
104
4.4.4
HEIGHT
OF
A
PACKED
COLUMN
*
105
4.4.4.1
TRANSFER
UNITS
------
105
4.4.5
MINIMUM
COLUMN
DIAMETER
-----
108
4.4.6
PRESSURE
DROP
-----
110
4.5
CRITERIA
FOR
COLUMN
SELECTION
*
111
NOMENCLATURE
*
112
EXERCISES
*
113
CHAPTER
5
LIQUID-LIQUID
EXTRACTION
*
117
5.1
INTRODUCTION
*
117
5.1.1
GENERAL
INTRODUCTION
*
117
5.1.2
LIQUID-LIQUID
EQUILIBRIA
*
120
5.1.3
SOLVENT
SELECTION
*
121
5.2
EXTRACTION
SCHEMES
*
123
5.2.1
SINGLE
EQUILIBRIUM
STAGE
*
124
5.2.2 COCURRENT
CASCADE
*
125
5.2.3
CROSSCURRENT
*
126
5.2.4
COUNTERCURRENT
*
126
5.3
DESIGN
OF
COUNTERCURRENT
EXTRACTIONS
*
127
5.3.1
GRAPHICAL
MCCABE-THIELE
METHOD
FOR
IMMISCIBLE
SYSTEMS
*
127
5.3.2
ANALYTICAL
KREMSER
METHOD
FOR
IMMISCIBLE
SYSTEMS
*
130
5.3.3
GRAPHICAL
METHOD
FOR
PARTIALLY
MISCIBLE
SYSTEMS
*
131
5.3.4
EFFICIENCY
OF
AN
IDEAL
NONEQUILIBRIUM
MIXER
*
136
5.4
INDUSTRIAL
LIQUID-LIQUID
EXTRACTORS
*
137
5.4.1
MIXER-SETTLERS
*
137
5.4.2
MECHANICALLY
AGITATED
COLUMNS
*
138
5.4.3
UNAGITATED
AND
PULSED
COLUMNS
*
139
5.4.4
CENTRIFUGAL
EXTRACTORS
*
141
X
CONTENTS
5.4.5
SELECTION
OF
AN
EXTRACTOR
*
143
NOMENCLATURE
*
147
EXERCISES
*
147
CHAPTER
6
ADSORPTION
AND
ION
EXCHANGE
*
155
6.1
INTRODUCTION
*
155
6.2
ADSORPTION
FUNDAMENTALS
*
158
6.2.1
INDUSTRIAL
ADSORBENTS
*
158
6.2.2
EQUILIBRIA
-----
164
6.2.3
KINETICS
-----
168
6.3
FIXED-BED
ADSORPTION
*
171
6.3.1
BED
PROFILES
AND
BREAKTHROUGH
CURVES
*
171
6.3.2
EQUILIBRIUM
THEORY
MODEL
*
173
6.3.3
MODELING
OF
MASS
TRANSFER
EFFECTS
*
175
6.4
BASIC
ADSORPTION/DESORPTION
CYCLES
*
177
6.4.1
TEMPERATURE
SWING
*
179
6.4.2
PRESSURE
SWING
*
180
6.4.3
INERT
AND
DISPLACEMENT
PURGE
CYCLES
*
181
6.5
PRINCIPLES
OF
ION
EXCHANGE
*
182
6.5.1
ION
EXCHANGE
RESINS
*
183
6.5.2
EQUILIBRIA
AND
SELECTIVITY
*
184
6.6
ION
EXCHANGE
PROCESSES
*
185
NOMENCLATURE
*
187
EXERCISES
*
188
CHAPTER
7
DRYING
OF
SOLIDS
*
195
7.1
INTRODUCTION
-----
195
7.2
HUMIDITY
OF
CARRIER
GAS
*
196
7.2.1
DEFINITIONS
*
196
7.2.2
AIR-WATER
SYSTEM:
A
SPECIAL
CASE
*
198
7.2.3
PSYCHROMETRIC
CHARTS
*
199
7.3
MOISTURE
IN
SOLIDS
*
201
7.3.1
BOUND
AND
UNBOUND
WATER
*
201
7.4
DRYING
MECHANISMS
-----
206
7.4.1
CONSTANT
DRYING
RATE
*
207
7.4.2
FALLING
DRYING
RATE
-----
208
7.4.3
ESTIMATION
OF
DRYING
TIME
-----
208
7.5
CLASSIFICATION
OF
DRYING
OPERATIONS
*
210
7.5.1
DIRECT-HEAT
DRYERS
*
211
7.5.1.1
BATCH
COMPARTMENT
DRYERS
*
212
CONTENTS
*
XI
7.5.1.2
BELT
DRYERS
*
212
7.5.1.3
ROTARY
DRYERS
-----
213
7.5.1.4
FLASH
DRYERS
-----
214
7.5.1.5
FLUIDIZED
BED
DRYERS
*
214
7.5.1.6
SPRAY
DRYERS
*
216
7.5.2
CONTACT
DRYERS
*
217
7.5.2.1
ROTARY
AND
AGITATOR
DRYERS
------
217
7.5.2.2
VACUUM
DRYERS
*
217
7.5.2.3
FLUID
BED
DRYERS
------
218
7.5.3
OTHER
DRYING
METHODS
*
219
NOMENCLATURE
-----
220
EXERCISES
*
221
APPENDIX
-----
223
CHAPTER
8
CRYSTALLIZATION
*
227
8.1
INTRODUCTION
-----
227
8.2
CRYSTAL
QUALITY
PARAMETERS
*
232
8.2.1
CRYSTAL
SIZE
DISTRIBUTION
*
233
8.2.2
MORPHOLOGY
-----
234
8.2.3
CRYSTAL
FORM
-----
235
8.2.4
PURITY
-----
236
8.2.5
INTERDEPENDENCY
AMONG
CRYSTAL
QUALITY
PARAMETERS
*
237
8.3
PHASE
DIAGRAMS
*
237
8.3.1
PREDICTING
SOLUBILITY
CURVES
*
241
8.3.2
MEASURING
SOLUBILITY
CURVES
*
241
8.4
KINETICS
OF
CRYSTALLIZATION
*
242
8.4.1
METASTABLE
ZONE
LIMIT
*
242
8.4.2
MEASURING
METASTABLE
ZONE
WIDTH
*
244
8.4.3
SUPERSATURATION
*
244
8.4.4
THEORY
OF
CRYSTALLIZATION
*
245
8.4.5
NUCLEATION
*
247
8.4.6
CRYSTAL
GROWTH
-----
252
8.4.7
POPULATION
BALANCE
EQUATIONS
FOR
THE
MSMPR
CRYSTALLIZER
*
255
8.5
METHODS
OF
SUPERSATURATION
GENERATION
*
259
8.5.1
COOLING
-----
259
8.5.2
EVAPORATION
*
260
8.5.3
VACUUM
CRYSTALLIZATION
*
260
8.5.4
PRECIPITATION
*
261
8.5.5
ANTI-SOLVENT
CRYSTALLIZATION
-----
262
8.5.6
MELT
CRYSTALLIZATION
-----
263
XII
CONTENTS
8.5.7
CHOOSING
A
METHOD
OF
SUPERSATURATION
GENERATION
*
263
8.6
BASIC
DESIGN
FOR
INDUSTRIAL
CRYSTALLIZERS
*
264
8.6.1
PROCESS
AND
DESIGN
SPECIFICATIONS
*
266
8.6.2
THERMODYNAMIC
AND
LAB-SCALE
KINETIC
INFORMATION
*
266
8.6.3
DESIGN
DECISIONS
*
267
8.6.3.1
SELECTING
METHOD
OF
SUPERSATURATION
GENERATION
*
267
8.63.2
OPERATION
MODES:
BATCH
VERSUS
CONTINUOUS
OPERATION
*
268
8.6.3.3
NUMBER
OF
STAGES:
SINGLE-
AND
MULTISTAGE
OPERATION
SELECTION
*
270
8.63.4
SELECTING
THE
CRYSTALLIZER
TYPE
*
270
8.63.5
STIRRED
TANK
AND
COOLING
DISK
CRYSTALLIZER
*
271
8.63.6
FORCED
CIRCULATION
CRYSTALLIZERS
*
272
8.63.7
DRAFT
TUBE
BAFFLE
CRYSTALLIZER
*
273
8.63.8
FLUIDIZED
BED
CRYSTALLIZERS
*
273
8.63.9
MELT
CRYSTALLIZERS
*
274
8.6.3.10
VACUUM
CRYSTALLIZERS
*
276
8.7
CRYSTALLIZER
CALCULATIONS
*
277
8.7.1
MASS
BALANCE
*
277
8.7.2
BASIC
YIELD
CALCULATIONS
*
278
8.7.3
ENTHALPY
BALANCE
*
279
8.7.4
CRYSTALLIZER
DIMENSIONS
*
280
8.8
FINAL
DESIGN
PROCEDURE
*
281
8.8.1
ECONOMIC
EVALUATION
*
281
8.8.2
DETAILED
DESIGN
WITH
PRODUCTION
SCALE
KINETIC
DATA
*
282
NOMENCLATURE
*
283
EXERCISES
*
284
CHAPTER
9
SEDIMENTATION
AND
SETTLING
*
289
9.1
INTRODUCTION
*
289
9.2
GRAVITY
SEDIMENTATION
*
290
9.2.1
SEDIMENTATION
MECHANISMS
*
291
9.2.2
DILUTE
SEDIMENTATION
*
293
9.2.3
HINDERED
SETTLING
*
296
9.2.4
CONTINUOUS
SEDIMENTATION
TANK
(GRAVITY-SETTLING
TANK)
*
296
9.2.5
GRAVITY
SEDIMENTATION
EQUIPMENT
*
299
9.2.6
BROWNIAN
MOTION
AND
ITS
INFLUENCE
ON
SEDIMENTATION
*
300
9.2.7
COLLOIDAL
STABILITY
*
302
9.3
CENTRIFUGAL
SEDIMENTATION
*
303
9.3.1
PARTICLE
VELOCITY
IN
A
CENTRIFUGAL
FIELD
*
304
9.3.2
SEDIMENTING
CENTRIFUGES
*
304
9.3.3
BOWL
CENTRIFUGE
SEPARATION
CAPABILITY
*
307
CONTENTS
*
XIII
9.3.4
9.3.5
9.3.6
9.4
9.4.1
9.4.2
THE
SIGMA
CONCEPT
*
308
CAPACITY
OF
DISK
CENTRIFUGES
*
310
HYDROCYCLONES
-----
311
ELECTROSTATIC
PRECIPITATION
*
315
PRINCIPLES
*
315
EQUIPMENT
AND
COLLECTING
EFFICIENCY
*
317
NOMENCLATURE
*
319
EXERCISES
*
320
CHAPTER
10
FILTRATION
*
325
10.1
10.2
10.2.1
10.2.2
10.2.3
10.2.4
10.3
10.3.1
10.3.2
10.3.3
10.4
10.5
10.5.1
10.5.2
10.6
10.6.1
10.6.2
10.6.3
10.6.4
THE
FILTRATION
PROCESS
*
325
FILTRATION
FUNDAMENTALS
*
328
FLOW
THROUGH
PACKED
BEDS
*
328
CAKE
FILTRATION
*
329
CONSTANT
PRESSURE
AND
CONSTANT
RATE
FILTRATION
*
331
COMPRESSIBLE
CAKES
*
332
FILTRATION
EQUIPMENT
*
333
CONTINUOUS
LARGE-SCALE
VACUUM
FILTERS
*
334
BATCH
VACUUM
FILTERS
*
337
PRESSURE
FILTERS
*
338
FILTER
MEDIA
*
340
CENTRIFUGAL
FILTRATION
*
342
CENTRIFUGAL
FILTERS
*
342
FILTRATION
RATES
IN
CENTRIFUGES
*
344
INTERCEPTIVE
FILTRATION
*
347
DEEP
BED
FILTRATION
*
347
IMPINGEMENT
FILTRATION
OF
GASES
*
348
INTERCEPTION
MECHANISMS
*
350
LAMELLAR
PLATE
SEPARATORS
*
352
NOMENCLATURE
*
353
EXCERCISES
*
353
CHAPTER
11
MEMBRANE
FILTRATION
*
359
11.1
11.2
11.3
11.4
11.4.1
11.4.2
INTRODUCTION
*
359
MEMBRANE
SELECTION
*
360
MEMBRANE
FILTRATION
PROCESSES
*
362
FLUX
EQUATIONS
AND
SELECTIVITY
*
365
FLUX
DEFINITIONS
*
366
PERMEABILITY
FOR
DIFFUSION
IN
POROUS
MEMBRANES
*
367
XIV
*
CONTENTS
11.4.3
11.4.4
11.5
11.6
11.6.1
11.7
PERMEABILITY
FOR
SOLUTION-DIFFUSION
IN
DENSE
MEMBRANES
*
369
SELECTIVITY
AND
RETENTION
-----
370
CONCENTRATION
POLARIZATION
*
372
MEMBRANE
MODULES
-----
375
DESIGN
PROCEDURE
*
379
CONCLUDING
REMARKS
*
380
NOMENCLATURE
-----
381
EXERCISES
-----
382
APPENDIX
-----
384
CHAPTER
12
SEPARATION
METHOD
SELECTION
*
385
12.1
INTRODUCTION
*
385
12.1.1
INDUSTRIAL
SEPARATION
PROCESSES
*
385
12.1.2
FACTORS
INFLUENCING
THE
CHOICE
OF
A
SEPARATION
PROCESS
*
387
12.1.2.1
ECONOMICS
-----
387
12.1.2.2
FEASIBILITY
-----
388
12.1.2.3
PRODUCT
STABILITY
-----
389
12.1.2.4
DESIGN
RELIABILITY
*
389
12.2
SELECTION
OF
FEASIBLE
SEPARATION
PROCESSES
*
390
12.2.1
CLASSES
OF
PROCESSES
*
390
12.2.2
INITIAL
SCREENING
*
391
12.2.3
SEPARATION
FACTOR
*
392
12.3
SEPARATION
OF
HOMOGENEOUS
LIQUID
MIXTURES
*
394
12.3.1
STRENGTHS
OF
DISTILLATION
*
394
12.3.2
LIMITATIONS
OF
DISTILLATION
*
397
12.3.3
LOW
RELATIVE
VOLATILITIES
*
399
12.3.4
OVERLAPPING
BOILING
POINTS
*
401
12.3.5
LOW
CONCENTRATIONS
*
402
12.3.6
DISSOLVED
SOLIDS
*
403
12.4
SEPARATOR,
SYSTEMS
FOR
GAS
MIXTURES
*
404
12.4.1
GENERAL
SELECTION
CONSIDERATIONS
*
404
12.4.2
COMPARISON
OF
GAS
SEPARATION
TECHNIQUES
*
406
12.4.2.1
ABSORPTION
*
406
12.4.2.2
ADSORPTION
*
407
12.4.2.3
MEMBRANE
SEPARATION
*
407
12.5
SEPARATION
METHODS
FOR
SOLID-LIQUID
MIXTURES
*
408
EXCERCISES
*
410
APPENDIX
ANSWERS
TO
EXERCISES
*
413
REFERENCES
AND
FURTHER
READING
*
425
INDEX
*
429
CONTENTS
*
XV
|
| adam_txt |
CONTENTS
PREFACE
*
V
CHAPTER
1
CHARACTERISTICS
OF
SEPARATION
PROCESSES
*
1
1.1
1.2
1.2.1
1.2.2
1.2.3
1.3
1.3.1
1.3.2
1.4
1.4.1
1.4.2
SIGNIFICANCE
OF
SEPARATIONS
*
1
CHARACTERISTICS
OF
SEPARATION
PROCESSES
*
4
CATEGORIZATION
*
4
SEPARATING
AGENTS
*
5
SEPARATION
FACTORS
*
7
INDUSTRIAL
SEPARATION
METHODS
*
8
EXPLOITABLE
PROPERTIES
*
8
IMPORTANT
MOLECULAR
SEPARATIONS
*
10
INHERENT
SELECTIVITY
*
11
EQUILIBRIUM-BASED
PROCESSES
*
11
RATE-CONTROLLED
PROCESSES
*
13
NOMENCLATURE
*
14
EXERCISES
*
14
CHAPTER
2
EVAPORATION
AND
DISTILLATION
*
17
2.1
2.1.1
2.1.2
2.2
2.2.1
2.2.2
2.2.2.1
2.2.2.2
2.3
2.3.1
2.3.2
2.3.3
2.3.4
2.4
2.4.1
2.4.1.1
2.4.1.2
2.4.1.3
2.4.1.4
2.4.2
SEPARATION
BY
EVAPORATION
*
17
INTRODUCTION
*
17
VAPOR-LIQUID
EQUILIBRIA
*
18
SEPARATION
BY
SINGLE-STAGE
PARTIAL
EVAPORATION
*
23
DIFFERENTIAL
DISTILLATION
*
23
FLASH
DISTILLATION
*
24
SPECIFYING
T
AND
L/V
-----
26
SPECIFYING
T
AND
P
TOT
-----26
MULTISTAGE
DISTILLATION
*
28
DISTILLATION
CASCADES
*
28
COLUMN
DISTILLATION
*
29
FEASIBLE
DISTILLATION
CONDITIONS
*
31
EXTERNAL
COLUMN
BALANCES
*
31
MCCABE-THIELE
ANALYSIS
*
32
INTERNAL
BALANCES
*
32
RECTIFYING
SECTION
*
33
STRIPPING
SECTION
*
34
FEED
STAGE
CONSIDERATIONS
*
35
FEED
LINE
*
36
REQUIRED
NUMBER
OF
EQUILIBRIUM
STAGES
*
37
VIII
CONTENTS
2.4.2.1
2.4.2.2
2.4.23
2.4.2.4
2.4.3
2.5
2.5.1
2.5.2
2.5.3
GRAPHICAL
DETERMINATION
OF
STAGES
AND
LOCATION
OF
FEED
STAGE
-----
37
LIMITING
CONDITIONS
-----
40
FENSKE
AND
UNDERWOOD
EQUATIONS
*
41
USE
OF
MURPHREE
EFFICIENCY
-----
44
ENERGY
REQUIREMENTS
*
45
ADVANCED
DISTILLATION
TECHNIQUES
*
45
BATCH
DISTILLATION
-----
45
CONTINUOUS
SEPARATION
OF
MULTIPLE
PRODUCT
MIXTURES
*
47
SEPARATION
OF
AZEOTROPES
*
48
NOMENCLATURE
*
50
EXERCISES
-----
51
CHAPTER
3
ABSORPTION
AND
STRIPPING
*
57
3.1
3.2
3.3
3.4
3.4.1
3.4.2
3.5
3.5.1
3.5.2
3.5.3
3.6
3.6.1
3.6.2
3.6.3
3.6.4
INTRODUCTION
*
57
THE
AIM
OF
ABSORPTION
*
59
GENERAL
DESIGN
APPROACH
*
60
ABSORPTION
AND
STRIPPING
EQUILIBRIA
*
61
GASEOUS
SOLUTE
SOLUBILITIES
*
61
MINIMUM
ABSORBENT
FLOW
*
63
ABSORBER
AND
STRIPPER
DESIGN
*
64
OPERATING
LINES
FOR
ABSORPTION
*
64
STRIPPING
ANALYSIS
*
68
ANALYTICAL
KREMSER
SOLUTION
*
69
INDUSTRIAL
ABSORBERS
*
72
PACKED
COLUMNS
*
73
PLATE
COLUMNS
*
74
SPRAY
AND
BUBBLE
COLUMNS
*
74
COMPARISON
OF
ABSORPTION
COLUMNS
*
75
NOMENCLATURE
*
77
EXERCISES
-----
77
CHAPTER
4
GENERAL
DESIGN
OF
GAS/LIQUID
CONTACTORS
*
81
4.1
4.2
4.3
4.3.1
4.3.2
4.3.2.1
43.2.2
4.3.23
INTRODUCTION
*
81
MODELING
MASS
TRANSFER
*
81
PLATE
COLUMNS
*
86
DIMENSIONING
A
TRAY
COLUMN
*
89
HEIGHT
OF
A
TRAY
COLUMN
*
90
TRAY
SPACING
*
90
TRAY
EFFICIENCY
*
90
TRANSFER
UNITS
*
92
CONTENTS
*
IX
4.3.2.4
OVERALL
EFFICIENCY
-----
93
4.3.3
DIAMETER
OF
A
TRAY
COLUMN
*
95
4.3.3.1
FLOODING
-----
96
4.3.3.2
DOWNCOMER
FLOODING
-----
97
4.33.3
ENTRAINMENT
FLOODING
*
99
4.33.4
TRAY
DIAMETER
AND
PRESSURE
DROP
*
100
4.33.5
REMARK
ON
FLOODING
CHARTS
*
100
4.4
PACKED
COLUMNS
-----
101
4.4.1
RANDOM
PACKING
*
102
4.4.2
STRUCTURED
PACKING
-----
103
4.4.3
DIMENSIONING
A
PACKED
COLUMN
*
104
4.4.4
HEIGHT
OF
A
PACKED
COLUMN
*
105
4.4.4.1
TRANSFER
UNITS
------
105
4.4.5
MINIMUM
COLUMN
DIAMETER
-----
108
4.4.6
PRESSURE
DROP
-----
110
4.5
CRITERIA
FOR
COLUMN
SELECTION
*
111
NOMENCLATURE
*
112
EXERCISES
*
113
CHAPTER
5
LIQUID-LIQUID
EXTRACTION
*
117
5.1
INTRODUCTION
*
117
5.1.1
GENERAL
INTRODUCTION
*
117
5.1.2
LIQUID-LIQUID
EQUILIBRIA
*
120
5.1.3
SOLVENT
SELECTION
*
121
5.2
EXTRACTION
SCHEMES
*
123
5.2.1
SINGLE
EQUILIBRIUM
STAGE
*
124
5.2.2 COCURRENT
CASCADE
*
125
5.2.3
CROSSCURRENT
*
126
5.2.4
COUNTERCURRENT
*
126
5.3
DESIGN
OF
COUNTERCURRENT
EXTRACTIONS
*
127
5.3.1
GRAPHICAL
MCCABE-THIELE
METHOD
FOR
IMMISCIBLE
SYSTEMS
*
127
5.3.2
ANALYTICAL
KREMSER
METHOD
FOR
IMMISCIBLE
SYSTEMS
*
130
5.3.3
GRAPHICAL
METHOD
FOR
PARTIALLY
MISCIBLE
SYSTEMS
*
131
5.3.4
EFFICIENCY
OF
AN
IDEAL
NONEQUILIBRIUM
MIXER
*
136
5.4
INDUSTRIAL
LIQUID-LIQUID
EXTRACTORS
*
137
5.4.1
MIXER-SETTLERS
*
137
5.4.2
MECHANICALLY
AGITATED
COLUMNS
*
138
5.4.3
UNAGITATED
AND
PULSED
COLUMNS
*
139
5.4.4
CENTRIFUGAL
EXTRACTORS
*
141
X
CONTENTS
5.4.5
SELECTION
OF
AN
EXTRACTOR
*
143
NOMENCLATURE
*
147
EXERCISES
*
147
CHAPTER
6
ADSORPTION
AND
ION
EXCHANGE
*
155
6.1
INTRODUCTION
*
155
6.2
ADSORPTION
FUNDAMENTALS
*
158
6.2.1
INDUSTRIAL
ADSORBENTS
*
158
6.2.2
EQUILIBRIA
-----
164
6.2.3
KINETICS
-----
168
6.3
FIXED-BED
ADSORPTION
*
171
6.3.1
BED
PROFILES
AND
BREAKTHROUGH
CURVES
*
171
6.3.2
EQUILIBRIUM
THEORY
MODEL
*
173
6.3.3
MODELING
OF
MASS
TRANSFER
EFFECTS
*
175
6.4
BASIC
ADSORPTION/DESORPTION
CYCLES
*
177
6.4.1
TEMPERATURE
SWING
*
179
6.4.2
PRESSURE
SWING
*
180
6.4.3
INERT
AND
DISPLACEMENT
PURGE
CYCLES
*
181
6.5
PRINCIPLES
OF
ION
EXCHANGE
*
182
6.5.1
ION
EXCHANGE
RESINS
*
183
6.5.2
EQUILIBRIA
AND
SELECTIVITY
*
184
6.6
ION
EXCHANGE
PROCESSES
*
185
NOMENCLATURE
*
187
EXERCISES
*
188
CHAPTER
7
DRYING
OF
SOLIDS
*
195
7.1
INTRODUCTION
-----
195
7.2
HUMIDITY
OF
CARRIER
GAS
*
196
7.2.1
DEFINITIONS
*
196
7.2.2
AIR-WATER
SYSTEM:
A
SPECIAL
CASE
*
198
7.2.3
PSYCHROMETRIC
CHARTS
*
199
7.3
MOISTURE
IN
SOLIDS
*
201
7.3.1
BOUND
AND
UNBOUND
WATER
*
201
7.4
DRYING
MECHANISMS
-----
206
7.4.1
CONSTANT
DRYING
RATE
*
207
7.4.2
FALLING
DRYING
RATE
-----
208
7.4.3
ESTIMATION
OF
DRYING
TIME
-----
208
7.5
CLASSIFICATION
OF
DRYING
OPERATIONS
*
210
7.5.1
DIRECT-HEAT
DRYERS
*
211
7.5.1.1
BATCH
COMPARTMENT
DRYERS
*
212
CONTENTS
*
XI
7.5.1.2
BELT
DRYERS
*
212
7.5.1.3
ROTARY
DRYERS
-----
213
7.5.1.4
FLASH
DRYERS
-----
214
7.5.1.5
FLUIDIZED
BED
DRYERS
*
214
7.5.1.6
SPRAY
DRYERS
*
216
7.5.2
CONTACT
DRYERS
*
217
7.5.2.1
ROTARY
AND
AGITATOR
DRYERS
------
217
7.5.2.2
VACUUM
DRYERS
*
217
7.5.2.3
FLUID
BED
DRYERS
------
218
7.5.3
OTHER
DRYING
METHODS
*
219
NOMENCLATURE
-----
220
EXERCISES
*
221
APPENDIX
-----
223
CHAPTER
8
CRYSTALLIZATION
*
227
8.1
INTRODUCTION
-----
227
8.2
CRYSTAL
QUALITY
PARAMETERS
*
232
8.2.1
CRYSTAL
SIZE
DISTRIBUTION
*
233
8.2.2
MORPHOLOGY
-----
234
8.2.3
CRYSTAL
FORM
-----
235
8.2.4
PURITY
-----
236
8.2.5
INTERDEPENDENCY
AMONG
CRYSTAL
QUALITY
PARAMETERS
*
237
8.3
PHASE
DIAGRAMS
*
237
8.3.1
PREDICTING
SOLUBILITY
CURVES
*
241
8.3.2
MEASURING
SOLUBILITY
CURVES
*
241
8.4
KINETICS
OF
CRYSTALLIZATION
*
242
8.4.1
METASTABLE
ZONE
LIMIT
*
242
8.4.2
MEASURING
METASTABLE
ZONE
WIDTH
*
244
8.4.3
SUPERSATURATION
*
244
8.4.4
THEORY
OF
CRYSTALLIZATION
*
245
8.4.5
NUCLEATION
*
247
8.4.6
CRYSTAL
GROWTH
-----
252
8.4.7
POPULATION
BALANCE
EQUATIONS
FOR
THE
MSMPR
CRYSTALLIZER
*
255
8.5
METHODS
OF
SUPERSATURATION
GENERATION
*
259
8.5.1
COOLING
-----
259
8.5.2
EVAPORATION
*
260
8.5.3
VACUUM
CRYSTALLIZATION
*
260
8.5.4
PRECIPITATION
*
261
8.5.5
ANTI-SOLVENT
CRYSTALLIZATION
-----
262
8.5.6
MELT
CRYSTALLIZATION
-----
263
XII
CONTENTS
8.5.7
CHOOSING
A
METHOD
OF
SUPERSATURATION
GENERATION
*
263
8.6
BASIC
DESIGN
FOR
INDUSTRIAL
CRYSTALLIZERS
*
264
8.6.1
PROCESS
AND
DESIGN
SPECIFICATIONS
*
266
8.6.2
THERMODYNAMIC
AND
LAB-SCALE
KINETIC
INFORMATION
*
266
8.6.3
DESIGN
DECISIONS
*
267
8.6.3.1
SELECTING
METHOD
OF
SUPERSATURATION
GENERATION
*
267
8.63.2
OPERATION
MODES:
BATCH
VERSUS
CONTINUOUS
OPERATION
*
268
8.6.3.3
NUMBER
OF
STAGES:
SINGLE-
AND
MULTISTAGE
OPERATION
SELECTION
*
270
8.63.4
SELECTING
THE
CRYSTALLIZER
TYPE
*
270
8.63.5
STIRRED
TANK
AND
COOLING
DISK
CRYSTALLIZER
*
271
8.63.6
FORCED
CIRCULATION
CRYSTALLIZERS
*
272
8.63.7
DRAFT
TUBE
BAFFLE
CRYSTALLIZER
*
273
8.63.8
FLUIDIZED
BED
CRYSTALLIZERS
*
273
8.63.9
MELT
CRYSTALLIZERS
*
274
8.6.3.10
VACUUM
CRYSTALLIZERS
*
276
8.7
CRYSTALLIZER
CALCULATIONS
*
277
8.7.1
MASS
BALANCE
*
277
8.7.2
BASIC
YIELD
CALCULATIONS
*
278
8.7.3
ENTHALPY
BALANCE
*
279
8.7.4
CRYSTALLIZER
DIMENSIONS
*
280
8.8
FINAL
DESIGN
PROCEDURE
*
281
8.8.1
ECONOMIC
EVALUATION
*
281
8.8.2
DETAILED
DESIGN
WITH
PRODUCTION
SCALE
KINETIC
DATA
*
282
NOMENCLATURE
*
283
EXERCISES
*
284
CHAPTER
9
SEDIMENTATION
AND
SETTLING
*
289
9.1
INTRODUCTION
*
289
9.2
GRAVITY
SEDIMENTATION
*
290
9.2.1
SEDIMENTATION
MECHANISMS
*
291
9.2.2
DILUTE
SEDIMENTATION
*
293
9.2.3
HINDERED
SETTLING
*
296
9.2.4
CONTINUOUS
SEDIMENTATION
TANK
(GRAVITY-SETTLING
TANK)
*
296
9.2.5
GRAVITY
SEDIMENTATION
EQUIPMENT
*
299
9.2.6
BROWNIAN
MOTION
AND
ITS
INFLUENCE
ON
SEDIMENTATION
*
300
9.2.7
COLLOIDAL
STABILITY
*
302
9.3
CENTRIFUGAL
SEDIMENTATION
*
303
9.3.1
PARTICLE
VELOCITY
IN
A
CENTRIFUGAL
FIELD
*
304
9.3.2
SEDIMENTING
CENTRIFUGES
*
304
9.3.3
BOWL
CENTRIFUGE
SEPARATION
CAPABILITY
*
307
CONTENTS
*
XIII
9.3.4
9.3.5
9.3.6
9.4
9.4.1
9.4.2
THE
SIGMA
CONCEPT
*
308
CAPACITY
OF
DISK
CENTRIFUGES
*
310
HYDROCYCLONES
-----
311
ELECTROSTATIC
PRECIPITATION
*
315
PRINCIPLES
*
315
EQUIPMENT
AND
COLLECTING
EFFICIENCY
*
317
NOMENCLATURE
*
319
EXERCISES
*
320
CHAPTER
10
FILTRATION
*
325
10.1
10.2
10.2.1
10.2.2
10.2.3
10.2.4
10.3
10.3.1
10.3.2
10.3.3
10.4
10.5
10.5.1
10.5.2
10.6
10.6.1
10.6.2
10.6.3
10.6.4
THE
FILTRATION
PROCESS
*
325
FILTRATION
FUNDAMENTALS
*
328
FLOW
THROUGH
PACKED
BEDS
*
328
CAKE
FILTRATION
*
329
CONSTANT
PRESSURE
AND
CONSTANT
RATE
FILTRATION
*
331
COMPRESSIBLE
CAKES
*
332
FILTRATION
EQUIPMENT
*
333
CONTINUOUS
LARGE-SCALE
VACUUM
FILTERS
*
334
BATCH
VACUUM
FILTERS
*
337
PRESSURE
FILTERS
*
338
FILTER
MEDIA
*
340
CENTRIFUGAL
FILTRATION
*
342
CENTRIFUGAL
FILTERS
*
342
FILTRATION
RATES
IN
CENTRIFUGES
*
344
INTERCEPTIVE
FILTRATION
*
347
DEEP
BED
FILTRATION
*
347
IMPINGEMENT
FILTRATION
OF
GASES
*
348
INTERCEPTION
MECHANISMS
*
350
LAMELLAR
PLATE
SEPARATORS
*
352
NOMENCLATURE
*
353
EXCERCISES
*
353
CHAPTER
11
MEMBRANE
FILTRATION
*
359
11.1
11.2
11.3
11.4
11.4.1
11.4.2
INTRODUCTION
*
359
MEMBRANE
SELECTION
*
360
MEMBRANE
FILTRATION
PROCESSES
*
362
FLUX
EQUATIONS
AND
SELECTIVITY
*
365
FLUX
DEFINITIONS
*
366
PERMEABILITY
FOR
DIFFUSION
IN
POROUS
MEMBRANES
*
367
XIV
*
CONTENTS
11.4.3
11.4.4
11.5
11.6
11.6.1
11.7
PERMEABILITY
FOR
SOLUTION-DIFFUSION
IN
DENSE
MEMBRANES
*
369
SELECTIVITY
AND
RETENTION
-----
370
CONCENTRATION
POLARIZATION
*
372
MEMBRANE
MODULES
-----
375
DESIGN
PROCEDURE
*
379
CONCLUDING
REMARKS
*
380
NOMENCLATURE
-----
381
EXERCISES
-----
382
APPENDIX
-----
384
CHAPTER
12
SEPARATION
METHOD
SELECTION
*
385
12.1
INTRODUCTION
*
385
12.1.1
INDUSTRIAL
SEPARATION
PROCESSES
*
385
12.1.2
FACTORS
INFLUENCING
THE
CHOICE
OF
A
SEPARATION
PROCESS
*
387
12.1.2.1
ECONOMICS
-----
387
12.1.2.2
FEASIBILITY
-----
388
12.1.2.3
PRODUCT
STABILITY
-----
389
12.1.2.4
DESIGN
RELIABILITY
*
389
12.2
SELECTION
OF
FEASIBLE
SEPARATION
PROCESSES
*
390
12.2.1
CLASSES
OF
PROCESSES
*
390
12.2.2
INITIAL
SCREENING
*
391
12.2.3
SEPARATION
FACTOR
*
392
12.3
SEPARATION
OF
HOMOGENEOUS
LIQUID
MIXTURES
*
394
12.3.1
STRENGTHS
OF
DISTILLATION
*
394
12.3.2
LIMITATIONS
OF
DISTILLATION
*
397
12.3.3
LOW
RELATIVE
VOLATILITIES
*
399
12.3.4
OVERLAPPING
BOILING
POINTS
*
401
12.3.5
LOW
CONCENTRATIONS
*
402
12.3.6
DISSOLVED
SOLIDS
*
403
12.4
SEPARATOR,
SYSTEMS
FOR
GAS
MIXTURES
*
404
12.4.1
GENERAL
SELECTION
CONSIDERATIONS
*
404
12.4.2
COMPARISON
OF
GAS
SEPARATION
TECHNIQUES
*
406
12.4.2.1
ABSORPTION
*
406
12.4.2.2
ADSORPTION
*
407
12.4.2.3
MEMBRANE
SEPARATION
*
407
12.5
SEPARATION
METHODS
FOR
SOLID-LIQUID
MIXTURES
*
408
EXCERCISES
*
410
APPENDIX
ANSWERS
TO
EXERCISES
*
413
REFERENCES
AND
FURTHER
READING
*
425
INDEX
*
429
CONTENTS
*
XV |
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| author | Haan, André B. de 1964- Eral, H. Burak Schuur, Boelo 1978- |
| author_GND | (DE-588)1036241904 (DE-588)1215048742 (DE-588)1215047959 |
| author_facet | Haan, André B. de 1964- Eral, H. Burak Schuur, Boelo 1978- |
| author_role | aut aut aut |
| author_sort | Haan, André B. de 1964- |
| author_variant | a b d h abd abdh h b e hb hbe b s bs |
| building | Verbundindex |
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| discipline | Chemie / Pharmazie |
| discipline_str_mv | Chemie / Pharmazie |
| edition | 2nd edition |
| format | Book |
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| id | DE-604.BV046854315 |
| illustrated | Illustrated |
| index_date | 2024-07-03T15:10:52Z |
| indexdate | 2025-02-20T07:02:45Z |
| institution | BVB |
| institution_GND | (DE-588)10095502-2 |
| isbn | 9783110654738 3110654733 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-032263084 |
| oclc_num | 1190728635 |
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| owner_facet | DE-83 DE-703 DE-862 DE-BY-FWS DE-11 |
| physical | XV, 439 Seiten Illustrationen, Diagramme |
| publishDate | 2020 |
| publishDateSearch | 2020 |
| publishDateSort | 2020 |
| publisher | De Gruyter |
| record_format | marc |
| series2 | De Gruyter graduate |
| spellingShingle | Haan, André B. de 1964- Eral, H. Burak Schuur, Boelo 1978- Industrial separation processes fundamentals Trennverfahren (DE-588)4078395-9 gnd |
| subject_GND | (DE-588)4078395-9 |
| title | Industrial separation processes fundamentals |
| title_auth | Industrial separation processes fundamentals |
| title_exact_search | Industrial separation processes fundamentals |
| title_exact_search_txtP | Industrial separation processes fundamentals |
| title_full | Industrial separation processes fundamentals André B. de Haan, H. Burak Eral, Boelo Schuur |
| title_fullStr | Industrial separation processes fundamentals André B. de Haan, H. Burak Eral, Boelo Schuur |
| title_full_unstemmed | Industrial separation processes fundamentals André B. de Haan, H. Burak Eral, Boelo Schuur |
| title_short | Industrial separation processes |
| title_sort | industrial separation processes fundamentals |
| title_sub | fundamentals |
| topic | Trennverfahren (DE-588)4078395-9 gnd |
| topic_facet | Trennverfahren |
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Indexes
THWS Schweinfurt Zentralbibliothek Lesesaal
| Call Number: |
2000 VN 7121 H111(2) |
|---|---|
| Copy 1 | ausleihbar Available Place a Hold |