Spectroscopic methods in organic chemistry:
Saved in:
| Main Authors: | , , , , , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Stuttgart ; New York
Georg Thieme Verlag
[2021]
|
| Edition: | 3rd fully revised and extended edition |
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | viii, 498 Seiten Illustrationen, Diagramme (überwiegend farbig) 24 cm x 17 cm |
| ISBN: | 9783132434080 3132434086 |
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MARC
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| 020 | |a 3132434086 |9 3-13-243408-6 | ||
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| 100 | 1 | |a Hesse, Manfred |d 1935-2011 |e Verfasser |0 (DE-588)101805281X |4 aut | |
| 245 | 1 | 0 | |a Spectroscopic methods in organic chemistry |c Hesse-Meier-Zeeh, Prof. Dr. Stefan Bienz, Prof. Dr. Laurent Bigler, Dr. Thomas Fox, Prof. Dr. Herbert Meier |
| 246 | 1 | 3 | |a Hesse-Meier-Zeeh spectroscopic methods in organic chemistry |
| 246 | 1 | 3 | |a Hesse Meier Zeeh spectroscopic methods in organic chemistry |
| 250 | |a 3rd fully revised and extended edition | ||
| 264 | 1 | |a Stuttgart ; New York |b Georg Thieme Verlag |c [2021] | |
| 264 | 4 | |c © 2021 | |
| 300 | |a viii, 498 Seiten |b Illustrationen, Diagramme (überwiegend farbig) |c 24 cm x 17 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 650 | 0 | 7 | |a Organische Chemie |0 (DE-588)4043793-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Spektroskopie |0 (DE-588)4056138-0 |2 gnd |9 rswk-swf |
| 653 | |a hyphenated techniques | ||
| 653 | |a infrared spectroscopy | ||
| 653 | |a organic compounds | ||
| 653 | |a spectroscopy | ||
| 653 | |a UV/Vis spectroscopy | ||
| 653 | |a NMR spectroscopy | ||
| 653 | |a organic chemistry | ||
| 653 | |a Raman spectroscopy | ||
| 653 | |a mass spectrometry | ||
| 653 | |a nuclear magnetic resonance spectroscopy | ||
| 653 | |a 161 | ||
| 653 | |a Chemie | ||
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| 689 | 0 | 1 | |a Spektroskopie |0 (DE-588)4056138-0 |D s |
| 689 | 0 | |5 DE-604 | |
| 700 | 1 | |a Meier, Herbert |d 1939- |e Verfasser |0 (DE-588)13810817X |4 aut | |
| 700 | 1 | |a Zeeh, Bernd |d 1938- |e Verfasser |0 (DE-588)1107058449 |4 aut | |
| 700 | 1 | |a Bienz, Stefan |d 1958- |e Verfasser |0 (DE-588)1089234775 |4 aut | |
| 700 | 1 | |a Bigler, Laurent |d 1968- |e Verfasser |0 (DE-588)115378014 |4 aut | |
| 700 | 1 | |a Fox, Thomas |d 1962- |e Verfasser |0 (DE-588)1104398958 |4 aut | |
| 710 | 2 | |a Georg Thieme Verlag KG |0 (DE-588)1064287301 |4 pbl | |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, PDF |z 978-3-13-243410-3 |
| 776 | 0 | 8 | |i Erscheint auch als |n Online-Ausgabe, EPUB |z 978-3-13-243411-0 |
| 780 | 0 | 0 | |i Vorangegangen ist |z 9783131060426 |
| 856 | 4 | 2 | |m X:MVB |q text/html |u http://deposit.dnb.de/cgi-bin/dokserv?id=6bd7a274b9ef4f7cada52e5513dd71f7&prov=M&dok_var=1&dok_ext=htm |3 Inhaltstext |
| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031730559&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 943 | 1 | |a oai:aleph.bib-bvb.de:BVB01-031730559 | |
Record in the Search Index
| _version_ | 1815597405832216576 |
|---|---|
| adam_text |
CONTENTS
1
UV/VIS
SPECTROSCOPY
1
1.1
THEORETICAL
INTRODUCTION
-2
1.1.1
ELECTROMAGNETIC
WAVES
AND
ELECTRON
TRANSITIONS
IN
MOLECULES
-
2
1.1.2
LIGHT
ABSORPTION
AND
THE
SPECTRUM
-7
1.2
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
SPECTRA
-10
1.3
CHROMOPHORES
-11
1.3.1
INDIVIDUAL
CHROMOPHORIC
GROUPS
AND
THEIR
INTERACTIONS
YY11
1.3.2
OLEFINS
AND
POLYENES
-14
1.3.3
BENZENE
AND
BENZENOID
AROMATICS
-18
1.3.4
HETEROAROMATICS
(HETARENES)
YY23
1.3.5
CARBONYL
COMPOUNDS
-25
1.3.6
CONJUGATED
OLIGOMERS
AND
POLYMERS
-
28
1.3.7
AGGREGATED
MOLECULES,
CHARGE-TRANSFER
COMPLEXES
-31
1.4
APPLICATIONS
OF
UV/VIS
SPECTROSCOPY
YY32
1.5
DERIVATIVE
SPECTROSCOPY
-35
1.6
CHIROPTICAL
METHODS
-
36
SUPPLEMENTARY
LITERATURE
-40
UV/VIS
SPECTROSCOPY
-40
CHIROPTICAL
METHODS
-41
2
INFRARED
AND
RAMAN
SPECTRA
43
2.1
INTRODUCTION
-44
2.2
BASIC
PRINCIPLES
-44
2.3
INFRARED
SPECTROMETER
YY46
2.3.1
CLASSICAL
(SCANNING)
INFRARED
SPECTROMETERS
-47
2.3.2
FOURIER
TRANSFORM
SPECTROMETER
-47
2.4
SAMPLE
PREPARATION
-49
2.4.1
SAMPLE
PREPARATION
FOR
MEASUREMENTS
IN
TRANSMISSION
YY49
2.4.2
REFLECTION
MEASUREMENTS
YY50
2.4.3
RAMAN
MEASUREMENTS
-50
2.5
INFRARED
SPECTRUM
-50
2.5.1
NUMBER
AND
TYPES
OF
VIBRATIONS
YY51
2.5.2
SPECTRUM
INTERPRETATION
YY52
2.6
CHARACTERISTIC
ABSORPTIONS:
AN
OVERVIEW
-56
2.7
INFRARED
ABSORPTIONS
OF
SINGLE
BONDS
WITH
HYDROGEN
-56
2.7.1
(CH)
ABSORPTION
-56
2.7.2
(O-H)
AND
(N
H)
ABSORPTIONS
-58
2.8
INFRARED
ABSORPTIONS
OF
TRIPLE
BONDS
AND
CUMULATED
DOUBLE
BONDS
-60
2.9
INFRARED
ABSORPTIONS
OF
DOUBLE
BONDS
C=O,
C=N,
C=C,
N=N,
AND
N=O
-
61
2.10
INFRARED
ABSORPTION
OF
AROMATIC
COMPOUNDS
-
65
2.11
INFRARED
ABSORPTION
IN
THE
FINGERPRINT
RANGE
-
66
2.12
EXAMPLES
OF
INFRARED
SPECTRA
-67
2.13
INFORMATION
TECHNOLOGY
ASSISTED
SPECTROSCOPY
-73
2.14
QUANTITATIVE
INFRARED
SPECTROSCOPY
YY75
2.15
RAMAN
SPECTROSCOPY
-77
2.15.1
EXCITATION
MECHANISMS
-77
2.15.2
SELECTION
RULES
-78
2.15.3
RAMAN
SPECTROMETER
-79
2.15.4
APPLICATIONS
-80
2.15.5
COMPARISON
OF
INFRARED
AND
RAMAN
-
82
LITERATURE
-
83
RAMAN
SPECTROSCOPY
-
83
PARTICULAR
TECHNIQUES
-
84
DATABASES
AND
APPLICATION
-84
3
NUCLEAR
MAGNETIC
RESONANCE
SPECTROSCOPY
85
3.1
PHYSICAL
PRINCIPLES
YY86
3.1.1
THE
RESONANCE
PHENOMENON
-
86
3.1.2
CHEMICAL
SHIFT
-
88
3.1.3
SPIN-SPIN
COUPLING
-
89
3.1.4
LINEWIDTHS
-97
3.1.5
INTENSITY
-98
3.2
NMR
SPECTRA
AND
MOLECULAR
STRUCTURE
-100
3.2.1
MOLECULES
WITH
"
RIGID
"
ATOMIC
POSITIONS
-100
3.2.2
INTRAMOLECULAR
MOTION
-100
3.2.3
CHEMICAL
EXCHANGE
PROCESSES
-110
3.3
'
H
NMR
SPECTROSCOPY
-117
3.3.1
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
'H
NMR
SPECTRA
-117
3.3.2
'H
CHEMICAL
SHIFTS
-122
3.3.3
'H,
'
H
COUPLING
-128
3.3.4
COUPLING
TO
OTHER
NUCLEI
-135
3.3.5
CORRELATION
OF
'
H
SHIFTS
WITH
STRUCTURAL
FEATURES
-137
3.3.6
INCREMENT
SYSTEMS
FOR
ESTIMATING
'H
CHEMICAL
SHIFTS
-144
3.3.7
'H
NMR
DATA
OF
REPRESENTATIVES
OF
COMMON
CLASSES
OF
COMPOUNDS
-144
3.3.8
SPECIALIZED
TECHNIQUES
-145
3.3.9
TWO-DIMENSIONAL
'
H
NMR
SPECTROSCOPY
-162
3.3.10
SIMULATION
OF
'H
NMR
SPECTRA
-171
3.3.11
NMR
SPECTRA
OF
ORIENTED
PHASES
AND
SOLIDS
-172
3.3.12
COMBINATION
OF
SEPARATION
METHODS
WITH
NMR
MEASUREMENTS
-173
3.4
13
C
NMR
SPECTROSCOPY
-173
3.4.1
SAMPLE
PREPARATION
AND
MEASUREMENT
OF
SPECTRA
-173
3.4.2
13
C
CHEMICAL
SHIFTS
-177
3.4.3
CORRELATION
OF
L3C
CHEMICAL
SHIFTS
WITH
STRUCTURAL
FEATURES
-189
3.4.4
INCREMENT
SYSTEMS
FOR
THE
ESTIMATION
OF
,3
C
CHEMICAL
SHIFTS
-189
3.4.5
13
C,'H
COUPLINGS
-191
3.4.6
COUPLING
OF
13
C
TO
OTHER
NUCLEI
(D,
F,
N,
AND
P)
-192
3.4.7
13
C,
13
C
COUPLINGS
-193
3.4.8
SPECIAL
TECHNIQUES
-201
3.4.9
MULTIDIMENSIONAL
,3
C
NMR
SPECTRA
-212
3.4.10
SOLID-STATE
SPECTRA
-222
3.5
COMBINATION
OF
'
H
AND
13
C
NMR
SPECTROSCOPY
-225
3.5.1
COMPLETE
ASSIGNMENT
OF
1
H
AND
L3
C
NMR
SIGNALS
-225
3.5.2
USE
OF
DATABASES
-
229
3.5.3
'
H
AND
,3
C
NMR
DATA
OF
REPRESENTATIVES
OF
THE
MOST
IMPORTANT
CLASSES
OF
COMPOUNDS
-232
3.6
NMR
OF
OTHER
NUCLEI
-266
3.6.1
19
F
NMR
SPECTROSCOPY
-266
3.6.2
31
P
NMR
SPECTROSCOPY
-266
3.6.3
,5
N
NMR
SPECTROSCOPY
-272
3.6.4
COMPLETE
ASSIGNMENT
OF
THE
NMR
SIGNALS
OF
A
COMPOUND
CONTAINING
'H,
13
C,
15
N,
.
-281
3.6.5
OTHER
NUCLEI
-282
LITERATURE
-283
GENERAL
WORKS
-283
SPECIAL
METHODS
AND
EFFECTS
-284
SPECIAL
COMPOUND
CLASSES,
APPLICATIONS
-284
CATALOGUES
-285
SERIALS,
PERIODICALS
-285
4
MASS
SPECTROMETRY
287
4.1
INTRODUCTION
-288
4.2
GENERAL
ASPECTS
OF
MASS
SPECTROMETRY
-289
4.2.1
THE
PRINCIPLE
OF
MASS
SPECTROMETRY
-289
4.2.2
THE
MASS
SPECTRUM
-290
4.3
INSTRUMENTAL
ASPECTS
-303
4.3.1
SAMPLE
INTRODUCTION
(INJECTION)
AND
ION
TYPES
-303
4.3.2
IONIZATION
METHODS
-306
4.3.3
MASS
ANALYZERS
-318
4.3.4
DETECTORS
-325
4.3.5
TANDEM
MASS
SPECTROMETRY
-326
4.3.6
COUPLING
OF
MASS
SPECTROMETRY
WITH
CHROMATOGRAPHIC
METHODS
-329
4.3.7
ION-MOBILITY
MASS
SPECTROMETRY
-335
4.3.8
SELECTION
OF
THE
APPROPRIATE
METHOD
-336
LITERATURE
4.4
INTERPRETATION
OF
SPECTRA
AND
STRUCTURAL
ELUCIDATION
-339
4.4.1
PREPARATION
FOR
THE
INTERPRETATION
-339
4.4.2
STRUCTURAL
INFORMATION
FROM
HR-MS
-341
4.4.3
FRAGMENTATION
REACTIONS
IN
EI-MS
-343
4.4.4
COLLISION-INDUCED
DISSOCIATION
-365
4.4.5
NEIGHBORING
GROUP
PARTICIPATION
AND
STEREOISOMERISM
-372
4.4.6
SPECTRAL
LIBRARIES
-376
4.4.7
SPECIAL
TECHNIQUES
-379
4.4.8
ELUCIDATION
OF
FRAGMENTATION
MECHANISMS
-383
4.5
SAMPLE
PREPARATION
-385
4.5.1
PURIFICATION,
PREPARATION,
AND
ENRICHMENT
-386
4.5.2
SAMPLE
SUBMISSION
AND
DECLARATION
OF
SAMPLE
PROPERTIES
-387
4.5.3
SPECIFIC
PREPARATIONS
FOR
THE
MEASUREMENT
-388
4.6
ARTIFACTS
-389
4.6.1
MEMORY
EFFECT
-389
4.6.2
FORMATION
OF
ARTIFACTS
IN
THE
ION
SOURCE
-390
4.6.3
IDENTIFICATION
OF
ARTIFACTS
-393
4.6.4
PREVENTION
OF
ARTIFACT
FORMATION
-394
4.7
TABLES
TO
THE
MASS
SPECTROMETRY
-394
4.7.1
FREQUENTLY
DETECTED
IONS
-395
4.7.2
FREQUENTLY
DETECTED
MASS
DIFFERENCES
-406
4.7.3
ISOTOPE
DISTRIBUTIONS
OF
HALOGENATED
COMPOUNDS
-414
4.7.4
SOLVENTS
AND
FREQUENT
IMPURITIES
-415
4.7.5
ISOTOPES
OF
NATURALLY
OCCURRING
ELEMENTS
-421
-428
5
HANDLING
OF
SPECTRA
AND
ANALYTICAL
DATA:
PRACTICAL
EXAMPLES
429
5.1
INTRODUCTION
-
430
5.2
CHARACTERIZATION
OF
COMPOUNDS
-
430
EXAMPLE
1
-
431
EXAMPLE
2
-
435
5.3
STRUCTURE
ELUCIDATION
OF
ALLEGEDLY
KNOWN
COMPOUNDS
AND
OF
PRODUCTS
ARISING
FROM
SYNTHESES
-
440
EXAMPLE
3
-
441
EXAMPLE
4
-
443
EXAMPLE
5
-
445
5.4
STRUCTURE
ELUCIDATION
OF
COMPLETELY
UNKNOWN
COMPOUNDS
-
448
EXAMPLE
6
-
448
EXAMPLE
7
-
452
EXAMPLE
8
-
455
EXAMPLE
9
-460
EXAMPLE
10
-
464
LITERATURE
INDEX
-469
-471 |
| any_adam_object | 1 |
| author | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd 1938- Bienz, Stefan 1958- Bigler, Laurent 1968- Fox, Thomas 1962- |
| author_GND | (DE-588)101805281X (DE-588)13810817X (DE-588)1107058449 (DE-588)1089234775 (DE-588)115378014 (DE-588)1104398958 |
| author_facet | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd 1938- Bienz, Stefan 1958- Bigler, Laurent 1968- Fox, Thomas 1962- |
| author_role | aut aut aut aut aut aut |
| author_sort | Hesse, Manfred 1935-2011 |
| author_variant | m h mh h m hm b z bz s b sb l b lb t f tf |
| building | Verbundindex |
| bvnumber | BV046354131 |
| classification_rvk | VG 8901 VK 5661 |
| ctrlnum | (OCoLC)1260845898 (DE-599)DNB1200881311 |
| discipline | Chemie / Pharmazie |
| edition | 3rd fully revised and extended edition |
| format | Book |
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| genre | (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV046354131 |
| illustrated | Illustrated |
| indexdate | 2024-11-13T09:03:34Z |
| institution | BVB |
| institution_GND | (DE-588)1064287301 |
| isbn | 9783132434080 3132434086 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-031730559 |
| oclc_num | 1260845898 |
| open_access_boolean | |
| owner | DE-11 DE-29T DE-1102 DE-83 DE-355 DE-BY-UBR DE-1028 DE-188 |
| owner_facet | DE-11 DE-29T DE-1102 DE-83 DE-355 DE-BY-UBR DE-1028 DE-188 |
| physical | viii, 498 Seiten Illustrationen, Diagramme (überwiegend farbig) 24 cm x 17 cm |
| publishDate | 2021 |
| publishDateSearch | 2021 |
| publishDateSort | 2021 |
| publisher | Georg Thieme Verlag |
| record_format | marc |
| spelling | Hesse, Manfred 1935-2011 Verfasser (DE-588)101805281X aut Spectroscopic methods in organic chemistry Hesse-Meier-Zeeh, Prof. Dr. Stefan Bienz, Prof. Dr. Laurent Bigler, Dr. Thomas Fox, Prof. Dr. Herbert Meier Hesse-Meier-Zeeh spectroscopic methods in organic chemistry Hesse Meier Zeeh spectroscopic methods in organic chemistry 3rd fully revised and extended edition Stuttgart ; New York Georg Thieme Verlag [2021] © 2021 viii, 498 Seiten Illustrationen, Diagramme (überwiegend farbig) 24 cm x 17 cm txt rdacontent n rdamedia nc rdacarrier Organische Chemie (DE-588)4043793-0 gnd rswk-swf Spektroskopie (DE-588)4056138-0 gnd rswk-swf hyphenated techniques infrared spectroscopy organic compounds spectroscopy UV/Vis spectroscopy NMR spectroscopy organic chemistry Raman spectroscopy mass spectrometry nuclear magnetic resonance spectroscopy 161 Chemie (DE-588)4123623-3 Lehrbuch gnd-content Organische Chemie (DE-588)4043793-0 s Spektroskopie (DE-588)4056138-0 s DE-604 Meier, Herbert 1939- Verfasser (DE-588)13810817X aut Zeeh, Bernd 1938- Verfasser (DE-588)1107058449 aut Bienz, Stefan 1958- Verfasser (DE-588)1089234775 aut Bigler, Laurent 1968- Verfasser (DE-588)115378014 aut Fox, Thomas 1962- Verfasser (DE-588)1104398958 aut Georg Thieme Verlag KG (DE-588)1064287301 pbl Erscheint auch als Online-Ausgabe, PDF 978-3-13-243410-3 Erscheint auch als Online-Ausgabe, EPUB 978-3-13-243411-0 Vorangegangen ist 9783131060426 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=6bd7a274b9ef4f7cada52e5513dd71f7&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031730559&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hesse, Manfred 1935-2011 Meier, Herbert 1939- Zeeh, Bernd 1938- Bienz, Stefan 1958- Bigler, Laurent 1968- Fox, Thomas 1962- Spectroscopic methods in organic chemistry Organische Chemie (DE-588)4043793-0 gnd Spektroskopie (DE-588)4056138-0 gnd |
| subject_GND | (DE-588)4043793-0 (DE-588)4056138-0 (DE-588)4123623-3 |
| title | Spectroscopic methods in organic chemistry |
| title_alt | Hesse-Meier-Zeeh spectroscopic methods in organic chemistry Hesse Meier Zeeh spectroscopic methods in organic chemistry |
| title_auth | Spectroscopic methods in organic chemistry |
| title_exact_search | Spectroscopic methods in organic chemistry |
| title_full | Spectroscopic methods in organic chemistry Hesse-Meier-Zeeh, Prof. Dr. Stefan Bienz, Prof. Dr. Laurent Bigler, Dr. Thomas Fox, Prof. Dr. Herbert Meier |
| title_fullStr | Spectroscopic methods in organic chemistry Hesse-Meier-Zeeh, Prof. Dr. Stefan Bienz, Prof. Dr. Laurent Bigler, Dr. Thomas Fox, Prof. Dr. Herbert Meier |
| title_full_unstemmed | Spectroscopic methods in organic chemistry Hesse-Meier-Zeeh, Prof. Dr. Stefan Bienz, Prof. Dr. Laurent Bigler, Dr. Thomas Fox, Prof. Dr. Herbert Meier |
| title_short | Spectroscopic methods in organic chemistry |
| title_sort | spectroscopic methods in organic chemistry |
| topic | Organische Chemie (DE-588)4043793-0 gnd Spektroskopie (DE-588)4056138-0 gnd |
| topic_facet | Organische Chemie Spektroskopie Lehrbuch |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=6bd7a274b9ef4f7cada52e5513dd71f7&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031730559&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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