Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry: = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Erlangen ; Nürnberg
[2019]
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Physical Description: | VIII, 279 Seiten Illustrationen, Diagramme 21 cm |
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| 100 | 1 | |a Dörr, Sabrina |d 1989- |e Verfasser |0 (DE-588)1182466273 |4 aut | |
| 245 | 1 | 0 | |a Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry |b = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |c vorgelegt von Sabrina Dörr |
| 246 | 1 | 3 | |a Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| 246 | 1 | 1 | |a Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| 264 | 1 | |a Erlangen ; Nürnberg |c [2019] | |
| 300 | |a VIII, 279 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2019 | ||
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| _version_ | 1804180013784760320 |
|---|---|
| adam_text | TABLE
OF
CONTENTS
TABLE
OF
CONTENTS
................................................................................................................
I
LIST
OF
SYMBOLS
AND
ABBREVIATIONS
................................................................................
ILL
1
INTRODUCTION
.............................................................................................................
-1
-
1.1
SUPRAMOLECULAR
CHEMISTRY
.................................................................................
-1
-
1.1.1
DEVELOPMENT
OF
SUPRAMOLECULAR
CHEMISTRY
.................................................
-
5
-
1.1.2
RELEVANCE
AND
APPLICATION
OF
SUPRAMOLECULAR
CHEMISTRY
.............................
-
6
-
1.1.3
SUPRAMOLECULAR
INTERACTIONS
........................................................................
-
8
-
1.2
ANION
RECEPTORS
..................................................................................................
-14
-
1.2.1
PROPERTIES
AND
DESIGN
OF
ANION
RECEPTORS
...................................................
-14
-
1.2.2
(THIO)UREA
BASED
RECEPTORS
.........................................................................
-18
-
1.2.3
APPLICATIONS
OF
ANION
RECEPTORS
...................................................................
-
21
-
1.3
TRIANGULENIUM
DERIVATIVES
...............................................................................
-
22
-
1.3.1
STRUCTURES
AND
STABILITIES
OF
TRIANGULENIUM
DERIVATIVES
..............................
-
24
-
1.3.2
AZATRIANGULENIUM
SALTS
................................................................................
-
26-
1.3.3
HELICENES
&
CHIRALITY
........
..........................................................................
-
29
-
1.3.4
APPLICATIONS
.................................................................................................
-33-
1.4
BORON
CONTAINING
TRIANGULENIUM
DERIVATIVES
..................................................
-
35
-
2
MOTIVATION
..............................................................................................................
-
37
-
3
RESULTS
AND
DISCUSSION
.........................................................................................
-
40-
3.1
SYNTHESES
OF
ANION
RECEPTORS
..........................................................................
-
40
-
3.1.1
SYNTHESES
OF
AZAANGULENIUM-BASED
RECEPTORS
..........................................
-
40
-
3.1.2
SYNTHESES
OF
AZAANGULENIUM-TWEEZERS
AS
RECEPTORS
.................................
-
57
-
3.1.3
SYNTHESES
OF
PRECURSORS
FOR
BORON-BASED
RECEPTORS
.................................
-
61
-
3.2
PROPERTIES
AND
SPECTROSCOPIC
ANALYSIS
...............................................................
-
76
-
3.2.1 UV/VIS
AND
ECD
SPECTROSCOPY
.....................................................................
-
76
-
3.2.2
X-RAY
CRYSTALLOGRAPHIC
ANALYSIS
...................................................................
-
80
-
3.2.3
ELECTROCHEMICAL
ANALYSIS
.............................................................................
-
89
-
3.3
ANALYSIS
OF
ANION-BINDING
PROPERTIES
...............................................................
-
95
-
3.3.1 SELF-AGGREGATION
BEHAVIOR
OF
RECEPTORS
VIA
UV/VIS
TITRATION
EXPERIMENTS
.
-
97
-
3.3.2 COMPLEX
STOICHIOMETRY
OF
RECEPTORS
VIA
UV/VIS
TITRATION
EXPERIMENTS
....
-
99
-
3.3.3
ANION
BINDING
PROPERTIES
OF
AZAANGULENIUM
RECEPTORS
VIA
UV/VIS
TITRATION
EXPERIMENTS
................................................................................
-103
-
I
3.3.4
SELF-AGGREGATION
BEHAVIOR
OF
RECEPTORS
VIA
^-NMR
TITRATION
EXPERIMENTS
................................................................................................
-120-
3.3.5 COMPLEX
STOICHIOMETRY
OF
RECEPTORS
VIA
^-NMR
TITRATION
EXPERIMENTS.
-122
-
3.3.6
ANION-BINDING
PROPERTIES
OF
AZAANGULENIUM
RECEPTORS
VIA
^-NMR
TITRATION
EXPERIMENTS
................................................................................
-126
-
3.3.7
MISCELLANEOUS
............................................................................................
-143-
4
SUMMARY
..............................................................................................................
-145-
5
ZUSAMMENFASSUNG
..............................................................................................
-155
-
6
EXPERIMENTAL
SECTION
.........................................................................................
-166
-
6.1
GENERAL
INFORMATION
AND
METHODS
................................................................
-166
-
6.2
EXPERIMENTAL
PROCEDURES
AND
SPECTROSCOPIC
DATA
........................................
-169
-
6.2.1
SYNTHESES
OF
METHOXY-SUBSTITUTED
PRECURSORS
.........................................
-169
-
6.2.2
SYNTHESES
OF
ONEFOLD-NITROGEN-BRIDGED
TRIANGULENIUM
SALTS
....................
-170
-
6.2.3
SYNTHESES
OF
TWOFOLD-NITOGEN-BRIDGED
TRIANGULENIUM
SALTS
....................
-193
-
6.2.4
SYNTHESES
OF
THREEFOLD-NITROGEN-BRIDGED
TRIANGULENIUM
SALTS
................
-
203
-
6.2.5
SYNTHESES
OF
TWEEZER-MOLECULES
..............................................................
-
206
-
6.2.6
PRECURSOR
SYNTHESES
FOR
BORON
CONTAINING
TRIANGULENIUM
DERIVATIVES
....
-
213
-
6.2.7
SYNTHESES
OF
TBA-CARBOXYLATES
.................................................................
-
222
-
6.3
EXPERIMENTAL
ANALYSIS
OF
SUPRAMOLECULAR
BINDING
AFFINITIES
VIA
UV/VIS-SPECTROSCOPY
.......................................................................................
-
225
-
6.3.1
DETERMINATION
OF
SELF-AGGREGATION
VIA
UV/VIS-SPECTROSCOPY
...................
-
225
-
6.3.2
DETERMINATION
OF
COMPLEX-STOICHIOMETRY
VIA
UV/VIS-SPECTROSCOPY
........
-
226
-
6.3.3
DETERMINATION
OF
ASSOCIATION-CONSTANTS
VIA
UV/VIS-SPECTROSCOPY
..........
-
227
-
6.4
EXPERIMENTAL
ANALYSIS
OF
SUPRAMOLECULAR
BINDING
AFFINITIES
VIA
^-NMR-SPECTROSCOPY
...................................................................................
-
230
-
6.4.1
DETERMINATION
OF
SELF-AGGREGATION
VIA
^-NMR-SPECTROSCOPY
.................
-
230
-
6.4.2
DETERMINATION
OF
COMPLEX-STOICHIOMETRY
VIA
^-NMR-SPECTROSCOPY
......
-
231
-
6.4.3
DETERMINATION
OF
ASSOCIATION-CONSTANTS
VIA
^-NMR-SPECTROSCOPY
........
-
233
-
7
APPENDIX
...............................................................................................................
-235-
SPECTRAL
DATA
-
NMR
DATA
OF
SELECTED
COMPOUNDS
...............................................
-
235
-
X-RAY
CRYSTALLOGRAPHIC
DATA
..................................................................................
-
258
-
8
REFERENCES
............................................................................................................
-266-
II
|
| any_adam_object | 1 |
| author | Dörr, Sabrina 1989- |
| author_GND | (DE-588)1182466273 |
| author_facet | Dörr, Sabrina 1989- |
| author_role | aut |
| author_sort | Dörr, Sabrina 1989- |
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| bvnumber | BV045871680 |
| ctrlnum | (OCoLC)1104871443 (DE-599)DNB1182465668 |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| id | DE-604.BV045871680 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T08:29:01Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-031255005 |
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| physical | VIII, 279 Seiten Illustrationen, Diagramme 21 cm |
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| spelling | Dörr, Sabrina 1989- Verfasser (DE-588)1182466273 aut Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie vorgelegt von Sabrina Dörr Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie Erlangen ; Nürnberg [2019] VIII, 279 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2019 Supramolekulare Chemie (DE-588)4306141-2 gnd rswk-swf Supramolekulare Struktur (DE-588)4208977-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Supramolekulare Chemie (DE-588)4306141-2 s DE-604 Supramolekulare Struktur (DE-588)4208977-3 s B:DE-101 application/pdf http://d-nb.info/1182465668/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031255005&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Dörr, Sabrina 1989- Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie Supramolekulare Chemie (DE-588)4306141-2 gnd Supramolekulare Struktur (DE-588)4208977-3 gnd |
| subject_GND | (DE-588)4306141-2 (DE-588)4208977-3 (DE-588)4113937-9 |
| title | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| title_alt | Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| title_auth | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| title_exact_search | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| title_full | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie vorgelegt von Sabrina Dörr |
| title_fullStr | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie vorgelegt von Sabrina Dörr |
| title_full_unstemmed | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie vorgelegt von Sabrina Dörr |
| title_short | Synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry |
| title_sort | synthesis and characterization of triangulenium salts for the investigation of supramolecular chemistry synthese und charakterisierung von triangulenium salzen zur untersuchung der supramolekularen chemie |
| title_sub | = Synthese und Charakterisierung von Triangulenium Salzen zur Untersuchung der supramolekularen Chemie |
| topic | Supramolekulare Chemie (DE-588)4306141-2 gnd Supramolekulare Struktur (DE-588)4208977-3 gnd |
| topic_facet | Supramolekulare Chemie Supramolekulare Struktur Hochschulschrift |
| url | http://d-nb.info/1182465668/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=031255005&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT dorrsabrina synthesisandcharacterizationoftrianguleniumsaltsfortheinvestigationofsupramolecularchemistrysyntheseundcharakterisierungvontrianguleniumsalzenzuruntersuchungdersupramolekularenchemie AT dorrsabrina syntheseundcharakterisierungvontrianguleniumsalzenzuruntersuchungdersupramolekularenchemie |
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