Micro-Raman spectroscopy: theory and application
Saved in:
| Other Authors: | , |
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| Format: | Book |
| Language: | English |
| Published: |
Berlin ; Boston
De Gruyter
[2020]
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| Subjects: | |
| Online Access: | http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110514797&searchTitles=true Inhaltsverzeichnis |
| Physical Description: | XII, 219 Seiten Illustrationen, Diagramme (überwiegend farbig) |
| ISBN: | 9783110514797 |
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Record in the Search Index
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| adam_text | CONTENTS
LIST OF CONTRIBUTING AUTHORS * XI
DANA CIALLA-MAY, MICHAEL SCHMITT AND JIIRGEN POPP
1 THEORETICAL PRINCIPLES OF RAMAN SPECTROSCOPY * 1
1.1 INELASTIC LIGHT SCATTERING - A BRIEF INTRODUCTION INTO LINEAR RAMAN
SPECTROSCOPY * 2
1.1.1 BASIC PRINCIPLES OF RAMAN SPECTROSCOPY * 2
1.1.2 RESONANCE RAMAN SCATTERING (RRS) * 5
1.1.3 SURFACE ENHANCED RAMAN SPECTROSCOPY (SERS) * 7
1.2 NONLINEAR RAMAN-BASED PROCESSES * 9
1.2.1 HYPER-RAMAN SPECTROSCOPY * 9
1.2.2 COHERENT ANTI-STOKES RAMAN SPECTROSCOPY (CARS) AND CARS
MICROSCOPY *10
1.2.3 STIMULATED RAMAN SCATTERING (SRS) *12
REFERENCES *13
PHILIPPE DE BETTIGNIES
2 OPTICS/INSTRUMENTATION *15
2.1 INTRODUCTION *15
2.2 OVERALL SCHEME *15
2.3 LASER *17
2.3.1 WAVELENGTH CHOICE (AND WHY) *17
2.3.2 LASER TYPES * 20
2.3.3 SPECTRAL QUALITY * 22
2.3.4 SPATIAL QUALITY: BEAM SIZE, DIVERGENCE, ELLIPTICITY * 22
2.3.5 POWER AND POWER CONTROL * 24
2.3.6 LASER SAFETY * 25
2.4 MICROSCOPE-26
2.4.1 TYPES OF MICROSCOPES * 26
2.4.2 ILLUMINATION TECHNIQUES AND VIDEO CAMERA * 27
2.4.3 OBJECTIVES-27
2.4.4 CONFOCAL MICROSCOPE * 29
2.4.5 SPATIAL RESOLUTION OF RAMAN CONFOCAL MICROSCOPES * 29
2.5 FILTERING-32
2.5.1 RAYLEIGH FILTER (EDGE OR NOTCH) * 32
2.5.2 TRIPLE MONOCHROMATOR: A TUNABLE FILTERING SPECTROMETER * 34
2.5.3 VBG FILTERS FOR ULTRA LOW FREQUENCY (ULF) MEASURES * 34
2.6 SPECTROMETER * 36
2.6.1 SPECTROMETER PRINCIPLE * 36
2.6.2 GRATINGS-37
BIBLIOGRAFISCHE INFORMATIONEN
HTTP://D-NB.INFO/1140856898
VI ** CONTENTS
2.6.3 GRATING DRIVE, LINEARITY, CALIBRATION * 39
2.6.4 SLIT * 39
2.6.5 OPTICS AND SPECTROMETER COUPLING * 40
2.6.6 SPECTRAL RESOLUTION/DISPERSION * 41
2.7 DETECTOR * 44
2.7.1 WHAT IS A CCD DETECTOR? * 44
2.7.2 QUANTUM EFFICIENCY * 45
2.7.3 NOISE * 45
2.7.4 ETALONING EFFECT * 46
2.7.5 TYPES OF CCD - COMPARISON TABLE * 47
2.7.6 EMCCD-47
2.7.7 INFRARED DETECTORS * 48
2.7.8 MONOCHANNELS DETECTORS * 49
2.8 SOFTWARE, AUTOMATION, ELECTRONICS * 49
2.9 QUALITY ASSESSMENT * 49
2.9.1 S/N RATIO * 49
2.9.2 SPATIAL RESOLUTION * 51
2.10 ADVANCED * 52
2.10.1 RAMAN IMAGING * 52
2.10.2 AUTOFOCUS/3D IMAGING * 55
2.11 OTHER POPULAR OPTIONS * 57
2.11.1 POLARIZATION * 57
2.11.2 UV RAMAN * 58
2.11.3 COUPLING TO SPM, TERS-58
2.11.4 OTHERS * 59
IZABELLA JOLAN JAHN, LYDIA LEHNIGER, KARINA WEBER, DANA CIALLA-MAY AND
JLIRGEN POPP
3 SAMPLE PREPARATION FOR RAMAN MICROSPECTROSCOPY*61
3.1 INTRODUCTION * 61
3.2 SAMPLE CLEAN-UP AND ENRICHMENT STRATEGIES * 63
3.2.1 FILTRATION AND CENTRIFUGATION * 63
3.2.2 IMMUNOCAPTURE-LIKE ASSAYS * 64
3.2.3 LIQUID-LIQUID EXTRACTION (LLE) * 67
3.2.4 SOLID-PHASE EXTRACTION (SPE) * 67
3.2.5 TISSUE PROCESSING * 68
3.3 INNOVATIVE PLATFORM APPROACHES * 70
3.3.1 MICROFLUIDICS * 70
3.3.2 OPTICAL TWEEZERS AS TOOL IN RAMAN MICROSPECTROSCOPY *
3.4 FUTURE PERSPECTIVES AND CONCLUSION * 75
REFERENCES * 76
CONTENTS * VII
OLEG RYABCHYKOV, SHUXIA GUO AND THOMAS BOCKLITZ
4 ANALYZING RAMAN SPECTROSCOPIC DATA * 81
4.1 GENERAL ANALYSIS PIPELINE * 81
4.2 DATA PRETREATMENT * 82
4.2.1 SPIKE CORRECTION * 82
4.2.2 SPECTROMETER CALIBRATION * 85
4.3 DATA PREPROCESSING * 88
4.3.1 SMOOTHING * 88
4.3.2 BACKGROUND CORRECTION * 89
4.3.3 NORMALIZATION * 90
4.3.4 DIMENSION REDUCTION * 91
4.4 MODELS * 94
4.4.1 CLUSTERING AND UNMIXING FOR IMAGING * 95
4.4.2 CLASSIFICATION FOR DIAGNOSTICS AND REGRESSION MODELS FOR
ANALYTICS * 95
4.4.3 EVALUATION PROCEDURES * 96
4.5 NEW TRENDS * 98
4.5.1 MODEL TRANSFER * 98
4.5.2 DATA FUSION *101
4.6 SUMMARY: DOS AND DON TS IN ANALYZING RAMAN SPECTRA *102
REFERENCES *103
NATHALIE JUNG AND MAIKE WINDBERGS
5 RAMAN SPECTROSCOPY IN PHARMACEUTICAL RESEARCH AND INDUSTRY *107
5.1 RAMAN SPECTROSCOPY IN EARLY DRUG DEVELOPMENT AND
PREFORMULATION *108
5.1.1 IDENTIFICATION OF ACTIVE PHARMACEUTICAL INGREDIENTS (APIS) *108
5.1.2 SELECTION AND OPTIMISATION OF APIS *109
5.1.3 INTERACTION OF APIS WITH EXCIPIENTS * 111
5.2 CHARACTERIZATION AND EVALUATION OF ADVANCED DRUG DELIVERY
SYSTEMS *112
5.2.1 TECHNICAL REQUIREMENTS FOR IMAGING PHARMACEUTICAL SAMPLES *112
5.2.2 COMPOSITION AND PHYSICOCHEMICAL STABILITY OF DRUG DELIVERY
SYSTEMS *113
5.2.3 SPATIAL COMPONENT DISTRIBUTION WITHIN DRUG DELIVERY SYSTEMS *114
5.2.4 DRUG RELEASE FROM DELIVERY SYSTEMS *115
5.2.5 INTERACTION WITH BIOLOGICAL SYSTEMS *116
5.3 PROCESS ANALYTICAL TECHNOLOGY (PAT) AND QUALITY CONTROL DURING
PHARMACEUTICAL MANUFACTURING *119
5.3.1 PAT FOR THE MANUFACTURING OF SOLID DRUG DELIVERY SYSTEMS *119
5.3.2 PAT FOR BIOLOGICALLY-DERIVED PHARMACEUTICALS *122
VIII * CONTENTS
5.4 FUTURE PERSPECTIVES OF RAMAN SPECTROSCOPY IN PHARMACEUTICAL
RESEARCH AND INDUSTRY *124
REFERENCES *125
MARKUS LANKERS
6 APPLICATIONS IN: ENVIRONMENTAL ANALYTICS (FINE PARTICLES)-133
6.1 INTRODUCTION-133
6.2 APPLICATIONS-134
6.2.1 AEROSOL-134
6.2.2 MICROPLASTIC-135
6.3 AUTOMATION-137
6.3.1 SUBSTRATE AND SAMPLING-137
6.3.2 AUTOMATION WORKFLOW-138
6.3.3 PARAMETERIZATION / VALIDATION-140
6.3.4 ADVANTAGES OVER OTHER TECHNIQUES / FUTURE TRENDS-140
REFERENCES *143
CHRISTOPH KRAFFT AND JTIRGEN POPP
7 MICRO-RAMAN SPECTROSCOPY IN MEDICINE *147
7.1 INTRODUCTION-147
7.1.1 MOTIVATION FOR MICRO-RAMAN SPECTROSCOPY IN MEDICINE *147
7.1.2 RAMAN SPECTRA OF BIOMOLECULES-148
7.2 MICRO-RAMAN SPECTROSCOPY OF BACTERIA-150
7.2.1 EXPERIMENTAL CONSIDERATIONS-150
7.2.2 MICROBIAL APPLICATIONS OF MICRO-RAMAN SPECTROSCOPY *151
7.3 MICRO-RAMAN SPECTROSCOPY OF CELLS-155
7.3.1 EXPERIMENTAL CONSIDERATIONS-155
7.3.2 CYTOLOGICAL APPLICATIONS OF MICRO-RAMAN SPECTROSCOPY *156
7.4 MICRO-RAMAN SPECTROSCOPY OF TISSUES-161
7.4.1 EXPERIMENTAL CONSIDERATIONS-161
7.4.2 APPLICATIONS OF MICRO-RAMAN IMAGING-162
7.5 OUTLOOK-166
REFERENCES-167
ANASTASIA ROUSAKI, LUC MOENS AND PETER VANDENABEELE
8 ARCHAEOLOGICAL INVESTIGATIONS (ARCHAEOMETRY)-173
8.1 INTRODUCTION-173
8.2 BENCHTOP RAMAN INSTRUMENTATION AND POSSIBILITIES-174
8.3 DIRECT RAMAN ANALYSIS-179
8.4 RAMAN SPECTROSCOPY IN COMBINATION WITH OTHER TECHNIQUES-181
8.5 CONCLUSIONS-182
REFERENCES-183
CONTENTS
IX
MARISIA A. FIKIET, SHELBY R. KHANDASAMMY, EWELINA MISTEK, YASMINE AHMED,
LENKA HALAMKOVA, JUSTIN BUENO AND IGOR K. LEDNEV
9 FORENSICS: EVIDENCE EXAMINATION VIA RAMAN SPECTROSCOPY *189
9.1 INTRODUCTION-189
9.2 CHEMOMETRICS *190
9.3 BIOLOGICAL SAMPLES-191
9.4 CONTROLLED SUBSTANCES *194
9.4.1 COUNTERFEIT PHARMACEUTICALS *195
9.4.2 TOXICOLOGY-196
9.5 EXPLOSIVES AND GUNSHOT RESIDUE-196
9.5.1 EXPLOSIVES-197
9.5.2 GUNSHOT RESIDUE-199
9.6 QUESTIONED DOCUMENTS-200
9.7 TRACE ANALYSIS-202
9.7.1 PAINT-202
9.7.2 FIBERS-206
9.7.3 HAIR-207
9.8 CONCLUDING REMARKS-209
REFERENCES * 209
INDEX-217
|
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| spelling | Micro-Raman spectroscopy theory and application edited by Jürgen Popp and Thomas Mayerhöfer Berlin ; Boston De Gruyter [2020] © 2020 XII, 219 Seiten Illustrationen, Diagramme (überwiegend farbig) txt rdacontent n rdamedia nc rdacarrier Mikroskopie (DE-588)4039238-7 gnd rswk-swf Raman-Spektroskopie (DE-588)4176916-8 gnd rswk-swf Raman-Spektroskopie (DE-588)4176916-8 s DE-604 Mikroskopie (DE-588)4039238-7 s Popp, Jürgen 1966- (DE-588)131701819 edt Mayerhöfer, Thomas 1969- (DE-588)121637360 edt Walter de Gruyter GmbH & Co. KG (DE-588)10095502-2 pbl Erscheint auch als Online-Ausgabe 978-3-11-051531-2 X:MVB http://www.degruyter.com/search?f_0=isbnissn&q_0=9783110514797&searchTitles=true DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030950531&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Micro-Raman spectroscopy theory and application Mikroskopie (DE-588)4039238-7 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd |
| subject_GND | (DE-588)4039238-7 (DE-588)4176916-8 |
| title | Micro-Raman spectroscopy theory and application |
| title_auth | Micro-Raman spectroscopy theory and application |
| title_exact_search | Micro-Raman spectroscopy theory and application |
| title_full | Micro-Raman spectroscopy theory and application edited by Jürgen Popp and Thomas Mayerhöfer |
| title_fullStr | Micro-Raman spectroscopy theory and application edited by Jürgen Popp and Thomas Mayerhöfer |
| title_full_unstemmed | Micro-Raman spectroscopy theory and application edited by Jürgen Popp and Thomas Mayerhöfer |
| title_short | Micro-Raman spectroscopy |
| title_sort | micro raman spectroscopy theory and application |
| title_sub | theory and application |
| topic | Mikroskopie (DE-588)4039238-7 gnd Raman-Spektroskopie (DE-588)4176916-8 gnd |
| topic_facet | Mikroskopie Raman-Spektroskopie |
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