Handbook of industrial crystallization:
Saved in:
| Other Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Cambridge, United Kingdom ; New York, NY ; Port Melbourne, Australia ; New Delhi, India ; Singapore
Cambridge University Press
[2019]
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| Edition: | Third edition |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Klappentext |
| Physical Description: | xiii, 527 Seiten Illustrationen |
| ISBN: | 9780521196185 0521196183 |
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Record in the Search Index
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| adam_text | Contents Ստէ oļ Contributors viii Prcļncc to the Սրտէ Edition ix Prcince to the Second Edition xi ľrefnce to the l hird Edition xiii I 4.2 4.3 4.4 Solutions and Solution Properties 1 jennifer Moffitt Sellali and Allan S. Myerson 1.1 1.2 1.3 1.4 1.5 1.6 1.7 1 Introduction and Motivation 1 Units 1 Solubility of Inorganics I Solubility of Organics 9 Supersaturation and Metastability Solution Properties 22 Thermal Properties 25 References 31 4.5 17 5 2.1 Introduction 32 2.2 Basic Concepts of the Solid State 2.3 Crystal Nucléation 41 2.4 Crystal Growth 41 2.5 Crystal Habit 51 2.6 Crystal Polymorphism 59 2.7 Multicomponent Crystals 64 2.8 Crystal Size 68 2.9 Concluding Remarks 70 References 71 ! 1 5.3 5.4 32 5.5 5.6 5.7 5.8 Crystal Nucléation 76 Deni/ Lrdemir, Alfred Y. Lee, and Allan S. Myerson 3.1 3.2 3.3 3.4 3.5 3.6 3.7 3.8 Introduction 76 Homogeneous Nucléation 77 Heterogeneous Nucléation 95 Secondary Nucléation 96 Nucléation Kinetics 98 Control of Nucléation 102 Nucléation in Polymorphic Systems Methods to Induce Nucléation 108 References 110 Molecular Modeling Applications in Crystallization 136 Keith Chadwick, Jie Chen, Erik L. Santiso, and Bernhardt L. Trout 5.1 5.2 Crystals and Crystal Growth 32 Allred V. Lee, Deni/, Lrdemir, and Allan S. Mverson 104 The Influence of Impurities and Additives on Crystallization 115 Lucrèce H. Nicoud and Allan S. Myerson 6 Introduction 115 Introduction 136 Crystal Structure Visualization and Analysis Software 136 Morphology Prediction 138 Crystal Structure Determination from X-Ray Powder Diffraction Data 145 Modeling Nucléation and Phase
Transitions 147 Polymorph Searching and Prediction 154 Solubility Prediction 164 Chapter Summary and Outlook 168 References 169 Crystallization Process Analysis by Population Balance Modeling 172 Åke C. Rasmuson 6.1 6.2 6.3 6.4 6.5 6.6 6.7 6.8 6.9 6.10 4.1 Retention of Foreign Species in Crystals 115 Impact of Foreign Species on Growth Rate 122 Impact of Foreign Species on Crystal Properties 128 Conclusion 132 References 133 Introduction 172 Particle Size and Size Distribution 173 Crystallization Kinetics 177 Population Balance Modeling 178 The Idealized MSMPR Concept 181 Continuous Crystallization and Deviations from the MSMPR Model 184 Batch Crystallization 186 Population Balance Modeling of Non-WellMixed Processes 188 Determination of Crystallization Kinetics for Process Modeling 189 Conclusions 193 References 194 v
Contents Selection and Design of Industrial Crystallizers Herman ). M. Kramer and Richard Lakerveld 7.1 7.2 7.3 7.4 7.5 7.6 Introduction 197 Performance Criteria 198 Crystallization Methods 198 Equipment Design 201 Instrumentation and Actuation 211 Case Study: Optimization of a Base-Case Design 212 References 215 Precipitation Processes 8.3 8.4 8.5 8.6 8.7 8.8 8.9 8.10 Introduction 216 Physical and Thermodynamic Properties 217 Nucléation Kinetics 225 Crystal Growth Kinetics in Precipitation Other Processes and Models in Precipitation 231 Experimental Techniques 245 Modeling and Control of Crystal Size and Crystal Size Distribution 248 Scale-Up Rules for Precipitation 253 Precipitation in Practice 256 Summary 262 References 263 Melt Crystallization 266 Joachim Ulrich and Torsten Slelzer 9.1 9.2 9.3 9.4 9.5 9.6 9.7 9.8 9.9 Definitions 266 Benefits of Melt Crystallization 266 Phase Diagrams 268 Crystallization Kinetics 270 Processes of Melt Crystallization 273 Post-Crystallization Treatments 275 Concepts of Commercial Plants 280 Eutectic Freeze Crystallization 285 Summary and View to the Future 287 References 287 10 Crystallizer Mixing 290 Understanding and Modeling Crystallizer Mixing and Suspension Flow Daniel A. Green 10.1 10.2 10.3 10.4 10.5 10.6 VI I I Monitoring and Advanced Control of Crystallization Processes 313 Zoltan К. Nagy, Mitsuko l- ujiwara, and Richard D. Braatz 11.1 11.2 11.3 11.4 11.5 216 Piotr H. Karpiński and Jerzy Baldyga 8.1 8.2 197 Introduction 290 Crystallizer Flows 290 Crystallizers 294 Scale-Up 300 Modeling 302 Summary 310 References 311 Introduction
313 Crystallization Process Monitoring 316 Model-Based Optimization and Control of Crystallization Processes 323 Model-Free (Direct Design) Approaches 337 Summary 342 References 342 17 Batch Crystallization 346 Piotr H. Karpiński and ļcr/.у Batdyga 12.1 12.2 12.3 12.4 12.5 12.6 12.7 Introduction 316 Batch Crystallizers 316 Batch Crystallization Analysis 349 Factors Affecting Batch Crystallization Batch Crystallization Operations 368 Scale-Up of Batch Crystallization 373 Summary 376 References 377 336 I 3 Crystallization in the Pharmaceutical Industry 380 Simon N. Black 13.1 13.2 13.3 13.4 13.5 13.6 13.7 13.8 13.9 Introduction 380 Simple Systems 381 Increasing Complexity 385 Crystallization Kinetics 391 Particle Engineering 400 After the Crystallizer 405 Intermediates 407 Other Crystallizations 408 Summary 411 References 411 Crystallization of Proteins 414 Peter U. Vekiiov 14.1 14.2 14.3 14.4 14.5 14.6 14.7 14.8 14.9 14.10 Introduction 414 Protein and Protein Crystals 411 The Thermodynamics of Protein Crystallization 417 Methods of Protein Crystallization 421 The Role of Nonprotein Solution Components and the Intermolecular Interactions in Solution 424 Crystal Nucléation 430 Mechanisms of Crystal Growth 441 Impurities 448 Crystal Perfection 449 Concluding Remarks 454 References 454
Contents I5 Crystallization in Foods Richard VV. I lartel 15.1 15.2 15.3 15.4 460 Characteristics of Crystallization in Foods 460 Controlling Crystallization in Foods 463 Factors Affecting Control of Crystallization in Foods 474 Summary 477 References 477 6 Precipitation and Crystallization of Pigments Lars Victim, Marco Mazzoni, and Marlin Iggland 16.1 16.2 16.3 16.4 Index 479 Introduction 479 Types of Pigments, Pigment Chemistry, and Pigment Properties 479 On the Design of Pigment Synthesis Processes 489 Practical Applications and Special Aspects 502 References 511 513
Since publication of the first edition of this invaluable resource in 1993 and the second edition in 2001, interest in crystallization science and technology has increased dramatically, and with that interest has come major new developments in the field. This third edition builds on the increased interest in crystallization and incorporates new material in a number of areas, Including new chapters on crystal nucléation, molecular modeling applications, and precipitation and crystallization of pigments and dyes as well as completely revised chapters on crystallization of proteins, crystallizer selection and design, control of crystallization processes and process analytical technologies, and an updating of all the other chapters. This book continues to be the perfect reference for industrial and academic scientists and engineers, with this new edition making it even timelier and more important in the field. Allan S. Myerson is Professor of the Practice of Chemical Engineering in the Department of Chemical Engineering at the Massachusetts Institute of Technology. Professor Myerson’s research focuses on separations processes in the chemical and pharmaceutical industry with an emphasis on crystallization from solution, nucléation, polymorphism, and pharmaceutical manufacturing. Professor Myerson has received a number of awards including the American Chemical Society Award in Separations Science and Technology (2008), the AlChE Separations Division Clarence G. Gerhold Award (2015), and the AICHE Process Development Division Excellence in Process Development Research Award
(2015). Deniz Erdemir is a Principal Scientist at Bristol-Myers Squibb Company. Dr Erdemir’s research focus lies at the drug substance/drug product interface with emphasis on crystal polymorphism and design of materials via particle engineering to enable robust drug products. She has published twelve papers and she is the inventor on two US patents. Alfred Y. Lee is a Principal Scientist in the Department of Process Research and Development at Merck Co., Inc. Prior to his current position, Dr Lee was a Principal Scientist at GlaxoSmithKline pic. Dr Lee s scientific interests are in the area of crystal engineering, crystallization process development, materials characterization, polymorphism, and solid-state chemistry. Cover illustration: Original image © nevarpp / ¡Stock / Getty Images Plus Cambridge UNIVERSITY PRESS www.cambridge.org Cover designed by Hart McLeod Ltd ISBN 978-0-521-19618-5 9780521196185
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| spelling | Handbook of industrial crystallization edited by Allan S. Myerson, Deniz Erdemir, Alfred Y. Lee Third edition Cambridge, United Kingdom ; New York, NY ; Port Melbourne, Australia ; New Delhi, India ; Singapore Cambridge University Press [2019] xiii, 527 Seiten Illustrationen txt rdacontent n rdamedia nc rdacarrier Verfahrenstechnik (DE-588)4062781-0 gnd rswk-swf Kristallisation (DE-588)4033215-9 gnd rswk-swf Crystallization / Industrial applications Kristallisation (DE-588)4033215-9 s Verfahrenstechnik (DE-588)4062781-0 s DE-604 Myerson, Allan S. 1952- Sonstige (DE-588)140934839 oth Erdemir, Deniz edt Lee, Alfred Y. edt Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030868465&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis Digitalisierung UB Bayreuth - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030868465&sequence=000003&line_number=0002&func_code=DB_RECORDS&service_type=MEDIA Klappentext |
| spellingShingle | Handbook of industrial crystallization Verfahrenstechnik (DE-588)4062781-0 gnd Kristallisation (DE-588)4033215-9 gnd |
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| title | Handbook of industrial crystallization |
| title_auth | Handbook of industrial crystallization |
| title_exact_search | Handbook of industrial crystallization |
| title_full | Handbook of industrial crystallization edited by Allan S. Myerson, Deniz Erdemir, Alfred Y. Lee |
| title_fullStr | Handbook of industrial crystallization edited by Allan S. Myerson, Deniz Erdemir, Alfred Y. Lee |
| title_full_unstemmed | Handbook of industrial crystallization edited by Allan S. Myerson, Deniz Erdemir, Alfred Y. Lee |
| title_short | Handbook of industrial crystallization |
| title_sort | handbook of industrial crystallization |
| topic | Verfahrenstechnik (DE-588)4062781-0 gnd Kristallisation (DE-588)4033215-9 gnd |
| topic_facet | Verfahrenstechnik Kristallisation |
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