Holdings: Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding

Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding:

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Bibliographic Details
Main Author:	Peng, Zirong 1988- (Author)
Format:	Thesis Book
Language:	English
Published:	Aachen Shaker Verlag 2018
Series:	Berichte aus der Materialwissenschaft
Subjects:	Nanostrukturiertes Material Iridium Degradation > Technik Presswerkzeug Diffusion Schutzschicht Blankpressen Optisches Glas Wolframcarbide Werkzeugverschleiß Zwischenschicht Platin Atom probe tomography Grain boundary Multilayer coating transmission electron microscopy Hochschulschrift
Online Access:	Inhaltsverzeichnis Inhaltsverzeichnis
Physical Description:	vii, 145 Seiten Illustrationen 21 cm, 236 g
ISBN:	9783844060218 3844060219

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MARC


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Record in the Search Index

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adam_text	CONTENTS ACKNOWLEDGEMENTS.................................................................................................I CONTENTS................................................................................................................. III LIST OF SYMBOLS AND ABBREVIATIONS.......................................................................V 1. INTRODUCTION........................................................................................................ 1 1.1. ORGANIZATION OF THE DISSERTATION THESIS ........................................................................... 4 2. FUNDAMENTALS..................................................................................................... 7 2.1. COATING DEPOSITION AND STRUCTURE ................................................................................... 7 2.2. THERMAL STABILITY AND DEGRADATION OF MULTILAYER COATING..............................................10 2.2.1. GRAIN BOUNDARY DIFFUSION........................................................................................11 2.2.2. INTERDIFFUSION, REACTION AND COMPOUND FORMATION..................................................15 2.3. STRATEGIES TO REDUCE AND CONTROL THE DEGRADATION PROCESS.............................................18 3. MATERIALS AND METHODS................................................................................... 21 3.1. SAMPLE PREPARATION...................................................................................................... 21 3.2. DEGRADATION TREATMENT.................................................................................................. 23 3.2.1. LABORATORY EXPOSURE TREATMENT FOR THERMAL - ENVIRONMENTAL DEGRADATION TESTING 23 3.2.2. INDUSTRIAL PRECISION GLASS MOLDING PROCESS ............................................................ 24 3.3. CHARACTERIZATION METHODS............................................................................................. 25 3.3.1. SCANNING ELECTRON MICROSCOPY............................................................................... 25 3.3.2. WHITE LIGHT INTERFEROMETRY..................................................................................... 27 3.3.3. ATOM PROBE TOMOGRAPHY........................................................................................ 28 3.3.4. AUGER ELECTRON SPECTROSCOPY ................................................................................. 33 3.3.5. (SCANNING) TRANSMISSION ELECTRON MICROSCOPY ....................................................... 34 4. RESULTS, DISCUSSIONS AND CONCLUSIONS ............................................................ 39 4.1. EVALUATION OF ANALYSIS CONDITION AND INSTRUMENT PERFORMANCE OF ATOM PROBE TOMOGRAPHY .............................................................................................................................................. 39 4.1.1. MASS SPECTRUM........................................................................................................ 42 4.1.2. QUANTITY OF MULTIPLE EVENT......................................................................................47 4.1.3. CHEMICAL COMPOSITION............................................................................................49 4.1.4. COMPARISON BETWEEN LASER ENERGY SETTINGS IN THE 3000X HR AND 5000 XS ATOM PROBE INSTRUMENTS............................................................................................................. 50 4.1.5. DISCUSSION............................................................................................................... 52 4.1.6. CONCLUSIONS............................................................................................................ 67 4.2. DEGRADATION OF PROTECTIVE COATINGS ON MOLDS USED FOR PRECISION GLASS MOLDING .......... 69 4.2.1. SAMPLES IN DIFFERENT DEGRADATION STATE....................................................................69 4.2.2. DEGRADATION MECHANISM......................................................................................... 81 4.2.3. METHODS TO IMPEDE THE DEGRADATION PROCESS......................................................... 88 4.2.4. CONCLUSIONS.......................................................................................................... 100 4.3. DIRECT HIGH RESOLUTION STUDY OF GRAIN BOUNDARY DIFFUSION, SEGREGATION AND PRECIPITATION ...........................................................................................................................................102 4.3.1. APT DATA TREATMENT............................................................................................... 105 4.3.2. GRAIN BOUNDARY DIFFUSION...................................................................................... 108 4.3.3. GRAIN BOUNDARY SEGREGATION AND PRECIPITATION...................................................... 111 4.3.4. CONCLUSIONS.......................................................................................................... 116 5. OUTLOOK......................................................................................................... 119 BIBLIOGRAPHY....................................................................................................... 121 ABSTRACT............................................................................................................... 139 ZUSAMMENFASSUNG..............................................................................................141 CURRICULUM VITAE............................................................................................... 143
any_adam_object	1
author	Peng, Zirong 1988-
author_GND	(DE-588)1164975803
author_facet	Peng, Zirong 1988-
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author_sort	Peng, Zirong 1988-
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ctrlnum	(OCoLC)1060984050 (DE-599)DNB1160499993
dewey-full	681.42 621.98
dewey-hundreds	600 - Technology (Applied sciences)
dewey-ones	681 - Precision instruments and other devices 621 - Applied physics
dewey-raw	681.42 621.98
dewey-search	681.42 621.98
dewey-sort	3681.42
dewey-tens	680 - Manufacture of products for specific uses 620 - Engineering and allied operations
discipline	Handwerk und Gewerbe / Verschiedene Technologien Werkstoffwissenschaften / Fertigungstechnik
format	Thesis Book
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series2	Berichte aus der Materialwissenschaft
spelling	Peng, Zirong 1988- Verfasser (DE-588)1164975803 aut Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding Zirong Peng Aachen Shaker Verlag 2018 vii, 145 Seiten Illustrationen 21 cm, 236 g txt rdacontent n rdamedia nc rdacarrier Berichte aus der Materialwissenschaft Dissertation RWTH Aachen University 2018 Nanostrukturiertes Material (DE-588)4342626-8 gnd rswk-swf Iridium (DE-588)4162402-6 gnd rswk-swf Degradation Technik (DE-588)4206992-0 gnd rswk-swf Presswerkzeug (DE-588)4175674-5 gnd rswk-swf Diffusion (DE-588)4012277-3 gnd rswk-swf Schutzschicht (DE-588)4180280-9 gnd rswk-swf Blankpressen (DE-588)4557709-2 gnd rswk-swf Optisches Glas (DE-588)4172682-0 gnd rswk-swf Wolframcarbide (DE-588)4127450-7 gnd rswk-swf Werkzeugverschleiß (DE-588)4196525-5 gnd rswk-swf Zwischenschicht (DE-588)4338137-6 gnd rswk-swf Platin (DE-588)4174856-6 gnd rswk-swf Atom probe tomography Diffusion Grain boundary Multilayer coating transmission electron microscopy (DE-588)4113937-9 Hochschulschrift gnd-content Optisches Glas (DE-588)4172682-0 s Blankpressen (DE-588)4557709-2 s Presswerkzeug (DE-588)4175674-5 s Wolframcarbide (DE-588)4127450-7 s Nanostrukturiertes Material (DE-588)4342626-8 s Zwischenschicht (DE-588)4338137-6 s Diffusion (DE-588)4012277-3 s Schutzschicht (DE-588)4180280-9 s Platin (DE-588)4174856-6 s Iridium (DE-588)4162402-6 s DE-604 Werkzeugverschleiß (DE-588)4196525-5 s Degradation Technik (DE-588)4206992-0 s Shaker Verlag (DE-588)1064118135 pbl B:DE-101 application/pdf http://d-nb.info/1160499993/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030604357&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis
spellingShingle	Peng, Zirong 1988- Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding Nanostrukturiertes Material (DE-588)4342626-8 gnd Iridium (DE-588)4162402-6 gnd Degradation Technik (DE-588)4206992-0 gnd Presswerkzeug (DE-588)4175674-5 gnd Diffusion (DE-588)4012277-3 gnd Schutzschicht (DE-588)4180280-9 gnd Blankpressen (DE-588)4557709-2 gnd Optisches Glas (DE-588)4172682-0 gnd Wolframcarbide (DE-588)4127450-7 gnd Werkzeugverschleiß (DE-588)4196525-5 gnd Zwischenschicht (DE-588)4338137-6 gnd Platin (DE-588)4174856-6 gnd
subject_GND	(DE-588)4342626-8 (DE-588)4162402-6 (DE-588)4206992-0 (DE-588)4175674-5 (DE-588)4012277-3 (DE-588)4180280-9 (DE-588)4557709-2 (DE-588)4172682-0 (DE-588)4127450-7 (DE-588)4196525-5 (DE-588)4338137-6 (DE-588)4174856-6 (DE-588)4113937-9
title	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding
title_auth	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding
title_exact_search	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding
title_full	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding Zirong Peng
title_fullStr	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding Zirong Peng
title_full_unstemmed	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding Zirong Peng
title_short	Nano-scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding
title_sort	nano scale investigation of the degradation mechanism of multilayer protective coating for precision glass molding
topic	Nanostrukturiertes Material (DE-588)4342626-8 gnd Iridium (DE-588)4162402-6 gnd Degradation Technik (DE-588)4206992-0 gnd Presswerkzeug (DE-588)4175674-5 gnd Diffusion (DE-588)4012277-3 gnd Schutzschicht (DE-588)4180280-9 gnd Blankpressen (DE-588)4557709-2 gnd Optisches Glas (DE-588)4172682-0 gnd Wolframcarbide (DE-588)4127450-7 gnd Werkzeugverschleiß (DE-588)4196525-5 gnd Zwischenschicht (DE-588)4338137-6 gnd Platin (DE-588)4174856-6 gnd
topic_facet	Nanostrukturiertes Material Iridium Degradation Technik Presswerkzeug Diffusion Schutzschicht Blankpressen Optisches Glas Wolframcarbide Werkzeugverschleiß Zwischenschicht Platin Hochschulschrift
url	http://d-nb.info/1160499993/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030604357&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA
work_keys_str_mv	AT pengzirong nanoscaleinvestigationofthedegradationmechanismofmultilayerprotectivecoatingforprecisionglassmolding AT shakerverlag nanoscaleinvestigationofthedegradationmechanismofmultilayerprotectivecoatingforprecisionglassmolding

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