Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission: = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Erlangen ; Nürnberg
[2017]
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis Inhaltsverzeichnis |
| Beschreibung: | XI, 254 Seiten Illustrationen, Diagramme 21 cm |
Internformat
MARC
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| 100 | 1 | |a Hetzer, Constantin |e Verfasser |4 aut | |
| 245 | 1 | 0 | |a Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission |b = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |c vorgelegt von Constantin Hetzer |
| 246 | 1 | 3 | |a Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| 246 | 1 | 1 | |a Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| 264 | 1 | |a Erlangen ; Nürnberg |c [2017] | |
| 300 | |a XI, 254 Seiten |b Illustrationen, Diagramme |c 21 cm | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2017 | ||
| 650 | 0 | 7 | |a Oligomere |0 (DE-588)4212195-4 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Fluoreszenz-Resonanz-Energie-Transfer |0 (DE-588)4773018-3 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Pentacenderivate |0 (DE-588)4456571-9 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Singulettzustand |0 (DE-588)4310962-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Dimere |0 (DE-588)4149937-2 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Pentacen |0 (DE-588)4348150-4 |2 gnd |9 rswk-swf |
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Pentacenderivate |0 (DE-588)4456571-9 |D s |
| 689 | 0 | 1 | |a Singulettzustand |0 (DE-588)4310962-7 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Pentacen |0 (DE-588)4348150-4 |D s |
| 689 | 1 | 1 | |a Dimere |0 (DE-588)4149937-2 |D s |
| 689 | 1 | 2 | |a Singulettzustand |0 (DE-588)4310962-7 |D s |
| 689 | 1 | |5 DE-604 | |
| 689 | 2 | 0 | |a Pentacen |0 (DE-588)4348150-4 |D s |
| 689 | 2 | 1 | |a Oligomere |0 (DE-588)4212195-4 |D s |
| 689 | 2 | 2 | |a Fluoreszenz-Resonanz-Energie-Transfer |0 (DE-588)4773018-3 |D s |
| 689 | 2 | |5 DE-604 | |
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| 856 | 4 | 2 | |m DNB Datenaustausch |q application/pdf |u http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030259140&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |3 Inhaltsverzeichnis |
| 999 | |a oai:aleph.bib-bvb.de:BVB01-030259140 | ||
Datensatz im Suchindex
| _version_ | 1804178390874324992 |
|---|---|
| adam_text | TABLE OF CONTENTS
LIST OF SYMBOLS AND
ABBREVIATIONS...........................................................................................
IV
ZUSAMMENFASSUNG....................................................................................................................VIII
SUMM
ARY.........................................................................................................................................X
1
INTRODUCTION.......................................................................................................................1
1.1 PENTACENE - AN EXCITING REPRESENTATIVE OF THE PAH
CLASS.....................................1
1.2 FROM CLAR TO TODAY - SYNTHESIS OF PENTACENE
...........................................................
1
1.3 PROPERTIES AND FUNCTIONALIZATION OF
PENTACENE.........................................................3
1.4 PENTACENE BASED OLIGOMERS AND
POLYMERS..............................................................5
1.5 PENTACENE DIMERS AND OLIGOMERS FOR THE INVESTIGATION OF
INTRAMOLECULAR
SINGLET
FISSION................................................................................................................13
1.5.1 2,2*-LINKED PENTACENE DIMERS
.............................................................................
17
1.5.1 6,6*-LINKED PENTACENE
DIMERS..............................................................................24
1.5.2
CONCLUSION..............................................................................................................
30
1.6 REFERENCES
...........................................................................................
31
2 MOTIVATION AND G
OALS..................................................................................................
39
2.1 NON-CONJUGATED, FLEXIBLE
DIMERS...............................................................................
42
2.2 XANTHENE-LINKED DIM
ERS.............................................................................................
44
2.3 NON-CONJUGATED, RIGID
DIMERS....................................................................................46
2.4 PT-LINKED DIM
ERS............................................................................................................47
2.5 PENTACENE
OLIGOMERS..................................................................................................
49
2.6
REFERENCES....................................................................................................................
51
3 RESULTS AND
DISCUSSION...............................................................................................54
3.1 SYNTHESIS, STRUCTURE, AND REACTIVITY OF PENTACENE OLIGOMERS 54
3.1.1 GENERAL SYNTHETIC APPROACH TOWARDS PENTACENES AND SYNTHESIS OF
PRECURSOR
MOLECULES.............................................................................................54
3.1.2 SYNTHESIS OF NON-CONJUGATED, FLEXIBLE PENTACENE DIMERS 2 2 1 -2 2
4
........
55
3.1.3 SYNTHESIS OF XANTHENE-LINKED PENTACENE DIMERS 2 2 5 -2 2 8
........................
64
3.1.4 SYNTHESIS OF NON-CONJUGATED, RIGID DIMERS 214, 229, AND 2 3 0
..................
69
3.1.5 SYNTHESIS OF PT-LINKED DIMERS 2 3 1 -2 3 4
.........................................................74
3.1.6 SYNTHESIS OF PENTACENE OLIGOMERS 2 3 5 -2 3 9
................................................. 78
3.2 X-RAY CRYSTALLOGRAPHIC
ANALYSIS.............................................................................95
3.2.1 SOLID-STATE ANALYSIS OF PRECURSORS 274 AND 2 7 5
............................................
95
3.2.2 SOLID-STATE ANALYSIS OF OLIGOMERS 214, 226, 227, 231, AND 239
...............
98
3.2.1 SUMMARY X-RAY CRYSTALLOGRAPHIC
ANALYSIS...................................................110
3.3 UV-VIS
SPECTROSCOPY..................................................................................................112
3.4 ELECTROCHEMICAL
ANALYSIS...........................................................................................121
3.5 DIFFERENTIAL SCANNING
CALORIMETRY.............................................................................131
3.6
MISCELLANEOUS.............................................................................................................
133
3.6.1 SYNTHESIS AND PROPERTIES OF A PENTACENE WITH A TERMINAL ACETYLENE
APPENDED...............................................................................................................133
3.6.2 SYNTHETIC EFFORTS TOWARDS A CYANOACRYLIC ACID FUNCTIONALIZED
PENTACENE
D IM
ER......................................................................................................................137
3.7 R
EFERENCES..................................................................................................................
143
4 SUM M
ARY.....................................................................................................................147
5. EXPERIMENTAL
DATA......................................................................................................
151
5.1 GENERAL PROCEDURES AND METHODS. 151
TABLE OF CONTENTS
5.2 EXPERIMENTAL DATA AND COMPOUND CHARACTERIZATION
...........................................
152
5.3 R
EFERENCES..................................................................................................................199
SPECTRAL
DATA...............................................................................................................
201
6.1 NMR DATA OF SELECTED
COMPOUNDS.......................................................................
201
6.2 UV-VIS DATA OF SELECTED COMPOUNDS. 252
|
| any_adam_object | 1 |
| author | Hetzer, Constantin |
| author_facet | Hetzer, Constantin |
| author_role | aut |
| author_sort | Hetzer, Constantin |
| author_variant | c h ch |
| building | Verbundindex |
| bvnumber | BV044864561 |
| ctrlnum | (OCoLC)1048010737 (DE-599)DNB1152103784 |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| genre_facet | Hochschulschrift |
| id | DE-604.BV044864561 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T08:03:13Z |
| institution | BVB |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030259140 |
| oclc_num | 1048010737 |
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| owner | DE-29T DE-29 DE-355 DE-BY-UBR |
| owner_facet | DE-29T DE-29 DE-355 DE-BY-UBR |
| physical | XI, 254 Seiten Illustrationen, Diagramme 21 cm |
| publishDate | 2017 |
| publishDateSearch | 2017 |
| publishDateSort | 2017 |
| record_format | marc |
| spelling | Hetzer, Constantin Verfasser aut Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung vorgelegt von Constantin Hetzer Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung Erlangen ; Nürnberg [2017] XI, 254 Seiten Illustrationen, Diagramme 21 cm txt rdacontent n rdamedia nc rdacarrier Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2017 Oligomere (DE-588)4212195-4 gnd rswk-swf Fluoreszenz-Resonanz-Energie-Transfer (DE-588)4773018-3 gnd rswk-swf Pentacenderivate (DE-588)4456571-9 gnd rswk-swf Singulettzustand (DE-588)4310962-7 gnd rswk-swf Dimere (DE-588)4149937-2 gnd rswk-swf Pentacen (DE-588)4348150-4 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Pentacenderivate (DE-588)4456571-9 s Singulettzustand (DE-588)4310962-7 s DE-604 Pentacen (DE-588)4348150-4 s Dimere (DE-588)4149937-2 s Oligomere (DE-588)4212195-4 s Fluoreszenz-Resonanz-Energie-Transfer (DE-588)4773018-3 s B:DE-101 application/pdf http://d-nb.info/1152103784/04 Inhaltsverzeichnis DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030259140&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hetzer, Constantin Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung Oligomere (DE-588)4212195-4 gnd Fluoreszenz-Resonanz-Energie-Transfer (DE-588)4773018-3 gnd Pentacenderivate (DE-588)4456571-9 gnd Singulettzustand (DE-588)4310962-7 gnd Dimere (DE-588)4149937-2 gnd Pentacen (DE-588)4348150-4 gnd |
| subject_GND | (DE-588)4212195-4 (DE-588)4773018-3 (DE-588)4456571-9 (DE-588)4310962-7 (DE-588)4149937-2 (DE-588)4348150-4 (DE-588)4113937-9 |
| title | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| title_alt | Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| title_auth | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| title_exact_search | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| title_full | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung vorgelegt von Constantin Hetzer |
| title_fullStr | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung vorgelegt von Constantin Hetzer |
| title_full_unstemmed | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung vorgelegt von Constantin Hetzer |
| title_short | Synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission |
| title_sort | synthesis and characterization of pentacene dimers and oligomers for the investigation of intramolecular singlet fission synthese und charakterisierung von pentacendimeren und oligomeren zur untersuchung der intramolekularen singulettspaltung |
| title_sub | = Synthese und Charakterisierung von Pentacendimeren und -oligomeren zur Untersuchung der intramolekularen Singulettspaltung |
| topic | Oligomere (DE-588)4212195-4 gnd Fluoreszenz-Resonanz-Energie-Transfer (DE-588)4773018-3 gnd Pentacenderivate (DE-588)4456571-9 gnd Singulettzustand (DE-588)4310962-7 gnd Dimere (DE-588)4149937-2 gnd Pentacen (DE-588)4348150-4 gnd |
| topic_facet | Oligomere Fluoreszenz-Resonanz-Energie-Transfer Pentacenderivate Singulettzustand Dimere Pentacen Hochschulschrift |
| url | http://d-nb.info/1152103784/04 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030259140&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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