Sensorial and analytical profiling of orange juice and apple juice: development and validation of shelf-life prediction models
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | German |
| Published: |
München
Herbert Utz Verlag
[2018]
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | VIII, 238 Seiten Diagramme |
| ISBN: | 9783831646982 3831646988 |
Staff View
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| 245 | 1 | 0 | |a Sensorial and analytical profiling of orange juice and apple juice |b development and validation of shelf-life prediction models |c Sabrina Kotter-Seel |
| 264 | 1 | |a München |b Herbert Utz Verlag |c [2018] | |
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Record in the Search Index
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| adam_text | INDEX OF CONTENT
ACKNOWLEDGEMENTS I
INDEX OF CONTENT II
LIST OF ABBREVIATIONS VI
GENERAL REMARKS VIII
1 INTRODUCTION AND OBJECTIVES 1
2 BACKGROUND 3
2.1 ACCELERATED SHELF-LIFE TESTING (ASLT) 3
2.1.1 PRACTICAL APPLICATION - ACCELERATED STORAGE CONDITIONS 3
2.1.2 EVALUATION STRATEGIES 4
2.1.3 UNCERTAINTY OF MEASUREMENT 5
2.2 MARKET ANALYSIS 6
2.3 LEGAL REQUIREMENTS FOR JUICES 7
2.4 ORANGE JUICE 7
2.4.1 JUICE PRODUCTION 7
2.4.2 FLAVOUR PROFILE 8
2.4.3 CHANGES IN THE VOLATILES PROFILE DURING STORAGE 9
2.4.4 EXISTING SHELF-LIFE PREDICTION MODELS 10
2.5 APPLE JUICE 12
2.5.1 APPLE VARIETIES AND FRUIT RIPENING 12
2.5.2 JUICE PRODUCTION 12
2.5.3 FLAVOUR PROFILE 13
2.5.4 ANALYTICAL INDICES 14
2.5.4.1 SUM OF ESTERS 14
2.5.4.2 SUM OF C6-ALDEHYDES AND -ALCOHOLS 15
2.5.4.3 AROMA INDEX 15
2.5.5 EXISTING SHELF-LIFE PREDICTION MODELS 16
2.6 UNIVARIATE AND MULTIVARIATE EXPLORATORY AND CONFIRMATORY STATISTICAL
APPROACHES 17
2.6.1 EXPLORATORY STATISTICAL APPROACHES 17
2.6.1.1 SPIDER CHARTS AND XY-DIAGRAMS AS UNIVARIATE EXPLORATORY
STATISTICAL
APPROACHES 17
2.6.1.2 PRINCIPAL COMPONENT ANALYSIS (PCA) AS MULTIVARIATE EXPLORATORY
STATISTICAL APPROACH 17
2.6.1.3 MULTIPLE FACTOR ANALYSIS (MFA) AS MULTIVARIATE EXPLORATORY
STATISTICAL
APPROACH 18
2.6.1.4 CLUSTER ANALYSIS AS MULTIVARIATE EXPLORATORY STATISTICAL
APPROACH 19
2.6.2 CONFIRMATORY STATISTICAL APPROACHES 20
2.6.2.1 AN OVA AS UNIVARIATE CONFIRMATORY STATISTICAL APPROACH 20
2.6.2.2 TUKEY S HSD POST-HOC TEST AS UNIVARIATE CONFIRMATORY STATISTICAL
APPROACH 22
2.6.2.3 MAHALANOBIS DISTANCE AS MULTIVARIATE CONFIRMATORY STATISTICAL
APPROACH 23
2.7 ARRHENIUS KINETIC 23
2.7.1 ORDER OF REACTION AND REACTION RATE 24
2.7.2 DETERMINATION OF THE ACCELERATION FACTOR 25
2.7.3 DETERMINATION OF THE ACTIVATION ENERGY 26
3 MATERIALS AND METHODS 27
3.1 JUICE SAMPLES 27
3.2 CHEMICALS/GASES 27
3.3 EQUIPMENT 27
3.4 SENSORIAL EVALUATION 28
3.4.1 QUANTITATIVE DESCRIPTIVE ANALYSIS (QDA) 28
3.4.1.1 SELECTION OF DESCRIPTORS FOR QDA QUESTIONNAIRE 28
3.4.1.2 EVALUATION PROTOCOL 29
3.4.2 DEGREE OF DIFFERENCE (DOD) TESTING 30
3.5 DETERMINATION OF THE COMPOSITION OF VOLATILES 30
3.5.1 SAMPLE EXTRACTION PROCEDURES 30
3.5.1.1 STIR BAR SORPTIVE EXTRACTION (SBSE) 30
3.5.1.2 SIMULTANEOUS-DISTILLATION-EXTRACTION (SDE) 30
3.5.2 GAS CHROMATOGRAPHY - MASS SPECTROMETRY (GC-MS) 31
3.5.2.1 GC-MS SYSTEM 1 WITH THERMAL DESORPTION UNIT (TDU) 31
3.5.2.2 GC-MS SYSTEM 2 31
3.5 2.3 MULTI-DIMENSIONAL GAS CHROMATOGRAPHY (MDGC) 32
3.S.2.4 IDENTIFICATION AND QUANTITATION OF VOLATILE COMPONENTS 32
3.5.3 DETERMINATION OF ESSENTIAL OILS (BROMATE METHOD) 34
3.6 CHEMICAL-PHYSICAL PARAMETERS 34
3.6.1 PH-VALUE AND TITRATABLE ACIDITY 34
3.6.2 RELATIVE DENSITY 35
3.6.3 REFRACTION INDEX EXPRESSED AS BRIX 35
3.7 STATISTICAL ANALYSIS 35
4 ORANGE JUICE - RESULTS AND DISCUSSION 37
4.1 EXPERIMENTAL TEST DESIGN 37
4.2 SENSORIAL EVALUATION 37
4.2.1 EVALUATION STRATEGY FOR THE DEVELOPMENT OF THE SENSORIAL
PREDICTION MODEL 37
4.2.2 EXPLORATORY STATISTICAL APPROACHES 39
4.2.2.1 SPIDER CHARTS 39
4.2.2.2 RCA 47
4.2 2.3 CLUSTER ANALYSIS 51
4.2.3 CONFIRMATORY STATISTICAL APPROACHES 54
4.2.3.1 ANOVA 54
4.2.3 2 TUKEY S HSD POST-HOC TEST 62
4.2.3 3 MAHALANOBIS DISTANCE 72
4.2.4 DERIVATION OF THE SENSORY-RELATED PREDICTION MODEL 75
4.3 COMPOSITION OF VOLATILES 79
4.3.1 EVALUATION STRATEGY FOR THE DEVELOPMENT OF THE VOLATILES-RELATED
PREDICTION
MODEL 79
4.3.2 VOLATILE COMPONENTS 80
4.3.3 EXPLORATORY STATISTICAL APPROACHES 84
4.3.3.1 PCA 84
4.3.3.2 CLUSTER ANALYSIS 89
4.3.3.3 XY-DIAGRAMS (KINETIC BEHAVIOUR) 91
4.3.3.3.1 TERPENES 92
4.3.3.3.2 PHENOLIC COMPONENTS 114
4.3.3.3.3 ALDEYHDES 116
4.3.3.3.4 ESTERS 118
4.3.3.3.5 ALCOHOLS 119
4.3.4 ARRHENIUS APPROACH 120
4.3.4.1 REACTION ORDERS AND REACTION RATES K(T) 120
4.3.4.2 ACCELERATION FACTORS (AFS) 123
4.3.5 MAHALANOBIS DISTANCE 126
4.3.6 DERIVATION OF THE VOLATILES-RELATED PREDICTION MODEL 130
4.4 FINAL PREDICTION MODEL INCLUDING SENSORIAL AND ANALYTICAL ASPECTS
132
4.4.1 EVALUATION STRATEGY FOR THE FINAL PREDICTION MODEL 132
4.4.2 MFA FOR COMBINATION OF SENSORIAL AND VOLATILE DATA SETS 133
4.4.3 DERIVATION OF THE FINAL PREDICTION MODEL 136
4.5 VALIDATION OF THE PREDICTION MODEL BY USING MARKET SAMPLES 138
4.5.1 EXPERIMENTAL TEST DESIGN 138
4.5.2 SENSORIAL EVALUATION: SPIDER CHARTS 139
4.5.3 VOLATILE COMPONENTS: KINETIC BEHAVIOUR AND ARRHENIUS APPROACH 141
4.5.4 FINAL VALIDATION OF THE PREDICTION MODEL 147
5 APPLE JUICE - RESULTS AND DISCUSSION 149
5.1 EXPERIMENTAL TEST DESIGN 149
5.2 SENSORIAL EVALUATION 149
5.2.1 EXPLORATORY STATISTICAL APPROACHES 150
5.2.1.1 SPIDER CHARTS 150
5.2.1.2 PCA 155
5.2.1.3 CLUSTER ANALYSIS 159
5.2.2 CONFIRMATORY STATISTICAL APPROACHES 162
5.2.2.1 ANOVA 162
5 2.2.2 TUKEY S HSD POST-HOC TEST 166
5.2.2.3 MAHALANOBIS DISTANCE 176
5.2.3 DERIVATION OF THE SENSORY-RELATED PREDICTION MODEL 178
5.3 COMPOSITION OF VOLATILES 180
5.3.1 VOLATILE COMPONENTS 180
5.3.2 EXPLORATORY STATISTICAL APPROACHES 183
5.3.2.1 PCA 183
5.3.2.2 XY-DIAGRAMS (KINETIC BEHAVIOUR) 185
5.3.2.2.1 ESTERS 186
5.3.2.2.2 ACIDS 189
53.2.2.3 ALDEHYDES 190
53.2.2.4 ALCOHOLS 190
5.3.3 ARRHENIUS APPROACH 191
53.3.1 REACTION ORDERS AND REACTION RATES K(T) 192
5.33.2 ACCELERATION FACTORS (AFS) 193
5.3.4 DERIVATION OF THE VOLATILES-RELATED PREDICTION MODEL 195
5.4 FINAL PREDICTION MODEL INCLUDING SENSORIAL AND ANALYTICAL ASPECTS
196
5.4.1 MFA FOR COMBINATION OF SENSORIAL AND VOLATILE DATA SETS 196
5.4.2 DERIVATION OF THE FINAL PREDICTION MODEL 199
5.5 VALIDATION OF THE PREDICTION MODEL BY USING APPLE-SPECIFIC INDICES
200
5.5.1 APPLE-SPECIFIC INDICES: KINETIC BEHAVIOUR AND ARRHENIUS APPROACH
200
5.5.2 FINAL VALIDATION OF THE PREDICTION MODEL 204
6 CONCLUDING COMPARISONS OF THE PREDICTION MODELS DEVELOPED FOR
ORANGE JUICE AND APPLE JUICE 206
7 SUMMARY 209
8 ZUSAMMENFASSUNG 211
9 REFERENCES 213
10 APPENDIX 222
11 CURRICULUM VITAE 249
|
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| author_GND | (DE-588)1155177002 |
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| ctrlnum | (OCoLC)1028907122 (DE-599)DNB1152025023 |
| discipline | Chemie / Pharmazie Lebensmitteltechnologie Chemie |
| format | Thesis Book |
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| indexdate | 2024-07-10T08:03:08Z |
| institution | BVB |
| institution_GND | (DE-588)36241-4 (DE-588)1065500602 |
| isbn | 9783831646982 3831646988 |
| language | German |
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| publisher | Herbert Utz Verlag |
| record_format | marc |
| spelling | Kotter-Seel, Sabrina 1987- Verfasser (DE-588)1155177002 aut Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models Sabrina Kotter-Seel München Herbert Utz Verlag [2018] VIII, 238 Seiten Diagramme txt rdacontent n rdamedia nc rdacarrier Dissertation Technische Universität München 2017 Lebensmittelanalyse (DE-588)4167032-2 gnd rswk-swf Haltbarkeit (DE-588)4220913-4 gnd rswk-swf Sensorische Prüfung (DE-588)4054562-3 gnd rswk-swf Orangensaft (DE-588)4172699-6 gnd rswk-swf Apfelsaft (DE-588)4142771-3 gnd rswk-swf Aromastoff (DE-588)4130237-0 gnd rswk-swf Aroma Index Flavor profile analytical chemistry (DE-588)4113937-9 Hochschulschrift gnd-content Orangensaft (DE-588)4172699-6 s Apfelsaft (DE-588)4142771-3 s Haltbarkeit (DE-588)4220913-4 s Sensorische Prüfung (DE-588)4054562-3 s Lebensmittelanalyse (DE-588)4167032-2 s Aromastoff (DE-588)4130237-0 s b DE-604 Technische Universität München (DE-588)36241-4 dgg Herbert Utz Verlag (DE-588)1065500602 pbl X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=f4f43f0a0a15432d9a0fc45d71eebaea&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030256357&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Kotter-Seel, Sabrina 1987- Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models Lebensmittelanalyse (DE-588)4167032-2 gnd Haltbarkeit (DE-588)4220913-4 gnd Sensorische Prüfung (DE-588)4054562-3 gnd Orangensaft (DE-588)4172699-6 gnd Apfelsaft (DE-588)4142771-3 gnd Aromastoff (DE-588)4130237-0 gnd |
| subject_GND | (DE-588)4167032-2 (DE-588)4220913-4 (DE-588)4054562-3 (DE-588)4172699-6 (DE-588)4142771-3 (DE-588)4130237-0 (DE-588)4113937-9 |
| title | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models |
| title_auth | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models |
| title_exact_search | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models |
| title_full | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models Sabrina Kotter-Seel |
| title_fullStr | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models Sabrina Kotter-Seel |
| title_full_unstemmed | Sensorial and analytical profiling of orange juice and apple juice development and validation of shelf-life prediction models Sabrina Kotter-Seel |
| title_short | Sensorial and analytical profiling of orange juice and apple juice |
| title_sort | sensorial and analytical profiling of orange juice and apple juice development and validation of shelf life prediction models |
| title_sub | development and validation of shelf-life prediction models |
| topic | Lebensmittelanalyse (DE-588)4167032-2 gnd Haltbarkeit (DE-588)4220913-4 gnd Sensorische Prüfung (DE-588)4054562-3 gnd Orangensaft (DE-588)4172699-6 gnd Apfelsaft (DE-588)4142771-3 gnd Aromastoff (DE-588)4130237-0 gnd |
| topic_facet | Lebensmittelanalyse Haltbarkeit Sensorische Prüfung Orangensaft Apfelsaft Aromastoff Hochschulschrift |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=f4f43f0a0a15432d9a0fc45d71eebaea&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030256357&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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