Catalysis: an integrated textbook for students
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| Other Authors: | , |
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| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH
[2018]
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| Subjects: | |
| Online Access: | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34159-7/ Inhaltsverzeichnis |
| Physical Description: | xiii, 370 Seiten Illustrationen, Diagramme |
| ISBN: | 9783527341597 3527341595 |
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| 245 | 1 | 0 | |a Catalysis |b an integrated textbook for students |c Edited by Ulf Hanefeld and Leon Lefferts |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c [2018] | |
| 264 | 4 | |c © 2018 | |
| 300 | |a xiii, 370 Seiten |b Illustrationen, Diagramme | ||
| 336 | |b txt |2 rdacontent | ||
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Record in the Search Index
| _version_ | 1804178081179500544 |
|---|---|
| adam_text | CONTENTS
PREFACE XIII
1 INTRODUCTION 1
LEON LEFFERTS, ULFHANEFELD, AND HARRY BITTER
1.1 A FEW WORDS AT THE BEGINNING 1
1.2 CATALYSIS IN A NUTSHELL 1
1.3 HISTORY OF CATALYSIS 3
1.3.1 INDUSTRIAL CATALYSIS 4
1.3.2 ENVIRONMENTAL CATALYSIS 5
1.4 INTEGRATION HOMO-HETERO-BIOCATALYSIS 5
1.5 RESEARCH IN CATALYSIS 10
1.5.1 S-CURVE, OLD PROCESSES IMPROVEMENT IS KNOWLEDGE INTENSIVE 10
1.5.2 INTERDEPENDENCE WITH OTHER FIELDS 11
1.5.3 RECENT AND FUTURE ISSUES 12
1.5.3.1 BIOMASS 12
1.5.3.2 C 0 2 AS A FEEDSTOCK 13
1.6 CATALYSIS AND INTEGRATED APPROACH OR HOW TO USE THIS BOOK 14
REFERENCES 14
2 HETEROGENEOUS CATALYSIS 15
LEON LEFFERTS; EMIEL HENSEN, AND HANS NIEMANTSVERDRIET
2.1 INTRODUCTION 15
2.1.1 CONCEPT OF HETEROGENEOUS CATALYSIS 15
2.1.2 APPLICATIONS OF HETEROGENEOUS CATALYSIS 16
2.1.2.1 TRANSPORTATION FUELS 17
2.1.2.2 CHEMICALS 20
2.1.2.3 ENVIRONMENTAL POLLUTION CONTROL 21
2.1.3 CATALYTIC CYCLE 23
2.2 ADSORPTION ON SURFACES 23
2.2.1 PHYSISORPTION AND CHEMISORPTION 24
2.2.2 ADSORPTION ISOTHERMS 26
2.2.3 CHEMISORPTION AND CHEMICAL BONDING 28
2.2.4 CONNECTING KINETIC AND THERMODYNAMIC FORMULATIONS 33
2.3 SURFACE REACTIONS 35
2.3.1 REACTION MECHANISM AND KINETICS 35
2.4 TYPES OF HETEROGENEOUS CATALYSTS 41
2.4.1 SUPPORTED METALS 41
2.4.1.1 UNDERSTANDING TRENDS IN REACTIVITY 41
2.4.1.2 STRUCTURE SENSITIVITY 42
2.4.1.3 SUPPORT EFFECTS 47
2.4.2 OXIDES AND SULFIDES 51
2.4.2.1 MOLECULAR ASPECTS 51
2.4.2.2 PROCESSES 52
2.4.2.3 TRANSITION METAL SULFIDES 59
2.4.3 SOLID ACID CATALYSTS 62
QUESTION 1 69
QUESTION 2 69
REFERENCES 70
3 HOMOGENEOUS CATALYSIS 73
ELISABETH BOUWMAN, MARTIN C. FEITERS, AND ROBERTAS J. M. KLEIN GEBBINK
3.1 FRAMEWORK AND OUTLINE 73
3.1.1 OUTLINE OF THIS CHAPTER 73
3.1.2 DEFINITIONS AND TERMINOLOGY 74
3.2 COORDINATION AND ORGANOMETALLIC CHEMISTRY 75
3.2.1 COORDINATION CHEMISTRY: D ORBITALS, GEOMETRIES, CRYSTAL FIELD
THEORY 75
3.2.2 O AND
% DONORS AND BACK-DONATION: CO, ALKENE, PHOSPHANE, H2 77
3.2.3 ORGANOMETALLICS: HAPTICITY, METAL-ALKYL/ALLYL, AGOSTIC
INTERACTION,
CARBENES 80
3.2.4 ELECTRON COUNTING: IONOGENIC OR DONOR-PAIR VERSUS COVALENT OR
NEUTRAL-LIGAND 81
3.2.5 EFFECT OF BINDING ON LIGANDS AND METAL IONS, STABILIZATION OF
OXIDATION
STATES 83
3.3 ELEMENTARY STEPS IN HOMOGENEOUS CATALYSIS 84
3.3.1 FORMATION OF THE ACTIVE CATALYST SPECIES 84
3.3.2 OXIDATIVE ADDITION AND REDUCTIVE ELIMINATION 85
3.3.2.1 CONCERTED ADDITION 85
3.3.2.2 SN2 MECHANISM 86
3.3.2.3 IONIC MECHANISM 86
3.3.2.4 RADICAL MECHANISM 87
3.3 2.5 REDUCTIVE ELIMINATION 87
3.3.3 MIGRATION AND ELIMINATION 87
3.3.4 OXIDATIVE COUPLING AND REDUCTIVE CLEAVAGE 90
3.3.5 ALKENE OR ALKYNE METATHESIS AND A-BOND METATHESIS 90
3.3.6 NUCLEOPHILIC AND ELECTROPHILIC ATTACK 92
3.4 HOMOGENEOUS HYDROGENATION 95
3.4.1 BACKGROUND AND SCOPE 95
3.4.2 H2 DIHYDRIDE MECHANISM: WILKINSON*S CATALYST 96
3.4.3 H2 MONOHYDRIDE MECHANISM AND HETEROLYTIC CLEAVAGE 97
3.4.4 ASYMMETRIC HOMOGENEOUS HYDROGENATION
98
3.4.5 TRANSFER HYDROGENATION WITH 2-PROPANOL 100
3.4.6 OTHER ALKENE ADDITION REACTIONS 102
3.5 HYDROFORMYLATION 104
3.5.1 SCOPE AND IMPORTANCE OF THE REACTION AND ITS PRODUCTS 104
3.5.2 COBALT-CATALYZED HYDROFORMYLATION 105
3.5.3 RHODIUM-CATALYZED HYDROFORMYLATION 107
3.5.4 ASYMMETRIC HYDROFORMYLATION 110
3.6 OLIGOMERIZATION AND POLYMERIZATION OF ALKENES 112
3.6.1 SCOPE AND IMPORTANCE OF OLIGOMERIZATION AND POLYMERIZATION 112
3.6.2 OLIGOMERIZATION OF ETHENE (NI, CR) 113
3.6.3 STEREOCHEMISTRY AND MECHANISM OF PROPENE POLYMERIZATION 115
3.6.4 METALLOCENE CATALYSIS 117
3.6.5 POLYMERIZATION WITH NON-METALLOCENES (PD, NI, FE, CO) 118
3.7 MISCELLANEOUS HOMOGENEOUSLY CATALYZED REACTIONS 118
3.7.1 CROSS-COUPLING REACTIONS: PD-CATALYZED C-C BOND FORMATION 118
3.7.2 METATHESIS REACTIONS 120
QUESTION 1 (TOTAL 20 POINTS) 122
QUESTION 2 (TOTAL 20 POINTS) 122
REFERENCES 123
FURTHER READING 124
4 BIOCATALYSIS 127
GUZMAN TORRELO, FRANK HOLLMANN, AND ULFHANEFELD
4.1 INTRODUCTION 127
4.2 WHY ARE ENZYMES SO HUGE? 129
4.3 CLASSIFICATION OF ENZYMES 137
4.3.1 OXIDOREDUCTASES (EC 1) 139
4.3.1.1 FLAVOMONOOXYGENASES 144
4.3.1.2 P450 MONOOXYGENASES 144
4.3.1.3 DIIRON-DEPENDENT MONOOXYGENASES 145
4.3.1.4 PEROXIDASES (EC 1.11.1) AND PEROXYGENASES (EC 1.11.2) 146
4.3.2 TRANSFERASES (EC 2) 147
4.3.3 HYDROLASES (EC 3) 147
4.3.4 LYASES (EC 4) 157
4.4 CONCEPTS AND METHODS 157
4.4.1 COFACTOR REGENERATION SYSTEMS 158
4.4.2 METHODS TO SHIFT UNFAVORABLE EQUILIBRIA 159
4.4.2.1 KINETIC VERSUS THERMODYNAMIC CONTROL 159
4.4.2.2 WORKING IN ORGANIC SOLVENTS 161
4.4.3 TWO-LIQUID-PHASE SYSTEMS (AND RELATED)
164
4.4.4 (DYNAMIC) KINETIC RESOLUTIONS AND DESYMMETRIZATION 164
4.4.5 ENANTIOMERIC RATIO E 168
4.5 APPLICATIONS AND CASE STUDIES 169
4.5.1 OXIDOREDUCTASES (E.C. 1) 169
4.5.1.1 DEHYDROGENASES 169
4.5.1.2 OXIDASES 173
4.5.1.3 OLD YELLOW ENZYMES 174
4.5.1.4 MONOOXYGENASES (EC 1.14.13) 175
4.5.1.5 PEROXIDASES/PEROXYGENASES 177
4.5.1.6 DIOXYGENASES 177
4.5.2 TRANSFERASES (EC 2) 177
4.5.3 HYDROLASES (EC 3) 179
4.5.3.1 LIPASES AND ESTERASES (EC 3.1.1) 179
4.5.4 LYASES (EC 4) 181
4.5.4.1 NITRILE HYDRATASE (EC 4.2.1) 181
QUESTION 1 186
QUESTION 2 186
QUESTION 3 187
QUESTION 4 188
FURTHER READING 188
5 CHEMICAL KINETICS OF CATALYZED REACTIONS 191
FREEK KAPTEIJN, JORGE GASCON, AND T. ALEXANDER NIJHUIS
5.1 INTRODUCTION 191
5.2 RATE EXPRESSIONS - QUASI-STEADY-STATE APPROXIMATION AND
QUASI-EQUILIBRIUM ASSUMPTION 193
5.3 ADSORPTION ISOTHERMS 198
5.3.1 ONE-COMPONENT ADSORPTION 198
5.3.2 MULTICOMPONENT ADSORPTION 199
5.3.3 DISSOCIATIVE ADSORPTION 200
5.4 RATE EXPRESSIONS - OTHER MODELS AND GENERALIZATIONS 200
5.5 LIMITING CASES - REACTANT AND PRODUCT CONCENTRATIONS 202
5.6 TEMPERATURE AND PRESSURE DEPENDENCE 206
5.6.1 TRANSITION-STATE THEORY 207
5.6.2 FORWARD REACTION - TEMPERATURE AND PRESSURE DEPENDENCE 208
5.6.3 FORWARD REACTION - LIMITING CASES 209
5.6.3.1 STRONG ADSORPTION OF A 209
5.6.3.2 WEAK ADSORPTION OF A AND B 209
5.6.3.3 STRONG ADSORPTION OF B 210
5.6.3.4 INTERMEDIATE ADSORPTION OF A AND B 210
5.7 SABATIER PRINCIPLE - VOLCANO PLOT 213
5.8 CONCLUDING REMARKS 214
NOTATION 216
GREEK 217
SUBSCRIPTS 217
SUPERSCRIPTS 217
QUESTION 1 217
QUESTION 2 218
QUESTION 3 218
REFERENCES 219
6 CATALYTIC REACTION ENGINEERING 221
FREEK KAPTEIJN, JORGE GASCON, AND T ALEXANDER NIJHUIS
6.1 INTRODUCTION 221
6.2 CHEMICAL REACTORS 222
6.2.1 BALANCE AND DEFINITIONS 222
6.2.2 BATCH REACTOR 224
6.2.2.1 MULTIPLE REACTIONS 226
6.2.3 CONTINUOUS FLOW STIRRED TANK REACTOR (CSTR) 228
6.2.4 PLUG-FLOW REACTOR (PFR) 231
6.2.5 COMPARISON BETWEEN PLUG-FLOW AND CSTR REACTOR 233
6.2.5.1 REACTOR SIZE 233
6.2.5.2 REACTOR SELECTIVITY 235
6.3 REACTION AND MASS TRANSPORT 236
6.3.1 EXTERNAL MASS TRANSFER 237
6.3.2 INTERNAL MASS TRANSPORT 242
6.3.2.1 EFFECTIVENESS FACTOR FOR INTERNAL MASS TRANSFER 244
6.3.3 GAS-LIQUID MASS TRANSFER 248
6.3.3.1 GAS-LIQUID MASS TTRANSFER FOLLOWED BY REACTION (HETEROGENEOUSLY
CATALYZED) 249
6.3.3.2 GAS-LIQUID MASS TRANSFER SIMULTANEOUSLY WITH A REACTION
(HOMOGENEOUSLY CATALYZED) 250
6.3.4 HEAT TRANSFER 254
6.3.4.1 EXTERNAL HEAT TRANSFER 255
6.3.4.2 INTERNAL HEAT TRANSPORT 256
6.4 CRITERIA TO CHECK FOR TRANSPORT LIMITATIONS 257
6.4.1 NUMERICAL CHECKS 257
6.4.1.1 EXTERNAL MASS TRANSFER; CARBERRY NUMBER 257
6.4.1.2 INTERNAL MASS TRANSFER; WHEELER-WEISZ MODULUS 257
6.4.1.3 EXTERNAL HEAT TRANSFER 258
6.4.1.4 INTERNAL HEAT TRANSFER 258
6.4.1.5 RADIAL PROFILES AND DISTRIBUTIONS IN CONCENTRATION AND
TEMPERATURE 259
6.4.2 EXPERIMENTAL CHECKS 260
NOTATION 264
GREEK SYMBOLS 265
SUBSCRIPTS 265
QUESTION 1 265
QUESTION 2 266
QUESTION 3 267
REFERENCES 269
7 CHARACTERIZATION OF CATALYSTS 271
GUIDO MUI, FRANK DE GROOT, BARBARA MOJET-MOL, AND MONIEK TROMP
7.1 INTRODUCTION 271
7.1.1 IMPORTANCE OF CHARACTERIZATION OF CATALYSTS 271
7.1.2 OVERVIEW OF THE VARIOUS TECHNIQUES 271
7.2 TECHNIQUES BASED ON PROBE MOLECULES 273
7.2.1 TEMPERATURE-PROGRAMMED TECHNIQUES 273
7.2.2 PHYSISORPTION AND CHEMISORPTION 275
7.2.2.1 PHYSISORPTION 276
7.2.2.2 CHEMISORPTION 279
73 ELECTRON MICROSCOPY TECHNIQUES 280
7A TECHNIQUES FROM ULTRAVIOLET UP TO INFRARED RADIATION 283
7.4.1 UV/VIS SPECTROSCOPY 283
7A 3 INFRARED SPECTROSCOPY 286
7.4.2.1 PROBE MOLECULES 287
7A.2.2 IN SITU EXPERIMENTS 287
7.4.2.Z LIQUID-PHASE ANALYSIS 288
7.4.3 RAMAN SPECTROSCOPY 289
7.5 TECHNIQUES BASED ON X-RAYS 291
7.5.1 INTRODUCTION 291
7.5.2 INTERACTION OF X-RAYS WITH MATTER 293
7.5.3 X-RAY PHOTOELECTRON SPECTROSCOPY (XPS) 294
7.5.4 X-RAY ABSORPTION SPECTROSCOPY (XAS) 295
7.5.4.1 XANES 295
7.5.4.2 EXAFS 298
7.5.5 X-RAY SCATTERING 299
7.5.5.1 WAXS/XRD 299
7.5.5.2 SAXS 300
7.5.6 X-RAY MICROSCOPY
302
7.6 ION SPECTROSCOPIES 303
7.7 MAGNETIC RESONANCE SPECTROSCOPY TECHNIQUES 304
7.7.1 NMR 304
7.7.2 EPR 307
7.7.2.1 METAL-CENTERED RADICALS 308
7.7.2.2 LIGAND-CENTERED RADICALS 308
7.8 SUMMARY 310
QUESTION 1 310
QUESTION 2 311
QUESTION 3 312
REFERENCES 313
8 SYNTHESIS OF SOLID SUPPORTS AND CATALYSTS 315
PETRA DE JONGH AND KRIJN DE JONG
8.1 INTRODUCTION 315
8.2 SUPPORT MATERIALS 317
8.2.1 MESOPOROUS METAL OXIDES 318
8.2.1.1 FUMED OXIDES 319
8.2.1.2 SILICA GEL AND OTHER HYDROTHERMALLY PREPARED OXIDES 320
8.2.1.3 ALUMINA 322
8.2.1.4 ORDERED MESOPOROUS MATERIALS 324
8.2.1.5 EXTENDING THE ORDERED MESOPOROUS MATERIALS FAMILY 325
8.2.2 ORDERED MICROPOROUS MATERIALS 326
8.2.2.1 ZEOLITES 326
8.2.2.2 METAL ORGANIC FRAMEWORKS 330
8.2.2.3 ZEOLITIC AMIDIZOLATE FRAMEWORKS 331
8.2.3 CARBON MATERIALS 331
8.2.4 SHAPING 333
8.3 SYNTHESIS OF SUPPORTED CATALYSTS 333
8.3.1 COLLOIDAL SYNTHESIS ROUTES 334
8.3.2 CHEMICAL VAPOR DEPOSITION 337
8.3.3 ION ADSORPTION 338
8.3.4 DEPOSITION PRECIPITATION 341
8.3.5 CO-PRECIPITATION 345
8.3.6 IMPREGNATION AND DRYING 349
8.3.6.1 IMPREGNATION 350
83.6.2 DRYING 352
8.3.6.3 CALCINATION/THERMAL TREATMENT 354
5.3.6.4 ACTIVATION OF THE CATALYST 356
QUESTION 1 357
QUESTION 2 357
QUESTION 3 358
REFERENCES 358
INDEX 361
|
| any_adam_object | 1 |
| author2 | Hanefeld, Ulf 1966- Lefferts, Leon 1960- |
| author2_role | edt edt |
| author2_variant | u h uh l l ll |
| author_GND | (DE-588)113692536 (DE-588)1150258233 |
| author_facet | Hanefeld, Ulf 1966- Lefferts, Leon 1960- |
| building | Verbundindex |
| bvnumber | BV044651977 |
| classification_rvk | VE 7040 VE 7041 |
| ctrlnum | (OCoLC)987574362 (DE-599)DNB1131725026 |
| dewey-full | 540 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 540 - Chemistry and allied sciences |
| dewey-raw | 540 |
| dewey-search | 540 |
| dewey-sort | 3540 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| format | Book |
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| genre | (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV044651977 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:58:18Z |
| institution | BVB |
| institution_GND | (DE-588)16179388-5 |
| isbn | 9783527341597 3527341595 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-030049688 |
| oclc_num | 987574362 |
| open_access_boolean | |
| owner | DE-20 DE-703 DE-11 DE-19 DE-BY-UBM DE-29T DE-92 DE-634 DE-83 DE-384 |
| owner_facet | DE-20 DE-703 DE-11 DE-19 DE-BY-UBM DE-29T DE-92 DE-634 DE-83 DE-384 |
| physical | xiii, 370 Seiten Illustrationen, Diagramme |
| publishDate | 2018 |
| publishDateSearch | 2018 |
| publishDateSort | 2018 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Catalysis an integrated textbook for students Edited by Ulf Hanefeld and Leon Lefferts Weinheim Wiley-VCH [2018] © 2018 xiii, 370 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Katalyse (DE-588)4029921-1 gnd rswk-swf (DE-588)4123623-3 Lehrbuch gnd-content Katalyse (DE-588)4029921-1 s DE-604 Hanefeld, Ulf 1966- (DE-588)113692536 edt Lefferts, Leon 1960- (DE-588)1150258233 edt Wiley-VCH (DE-588)16179388-5 pbl Erscheint auch als Online-Ausgabe, ePDF 978-3-527-81090-1 Erscheint auch als Online-Ausgabe, ePub 978-3-527-81092-5 Erscheint auch als Online-Ausgabe, Mobi 978-3-527-81091-8 Erscheint auch als Online-Ausgabe, oBook 978-3-527-81093-2 X:MVB http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34159-7/ DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030049688&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Catalysis an integrated textbook for students Katalyse (DE-588)4029921-1 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4123623-3 |
| title | Catalysis an integrated textbook for students |
| title_auth | Catalysis an integrated textbook for students |
| title_exact_search | Catalysis an integrated textbook for students |
| title_full | Catalysis an integrated textbook for students Edited by Ulf Hanefeld and Leon Lefferts |
| title_fullStr | Catalysis an integrated textbook for students Edited by Ulf Hanefeld and Leon Lefferts |
| title_full_unstemmed | Catalysis an integrated textbook for students Edited by Ulf Hanefeld and Leon Lefferts |
| title_short | Catalysis |
| title_sort | catalysis an integrated textbook for students |
| title_sub | an integrated textbook for students |
| topic | Katalyse (DE-588)4029921-1 gnd |
| topic_facet | Katalyse Lehrbuch |
| url | http://www.wiley-vch.de/publish/dt/books/ISBN978-3-527-34159-7/ http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=030049688&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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