Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties: = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften
Gespeichert in:
| 1. Verfasser: | |
|---|---|
| Format: | Abschlussarbeit Buch |
| Sprache: | English |
| Veröffentlicht: |
Aachen
Shaker
2016
|
| Schriftenreihe: | Berichte aus der Verfahrenstechnik
|
| Schlagworte: | |
| Online-Zugang: | Inhaltsverzeichnis |
| Beschreibung: | 244 Seiten 65 Illustrationen, Diagramme 21 cm x 14.8 cm, 404 g |
| ISBN: | 9783844046939 |
Internformat
MARC
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|---|---|---|---|
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| 003 | DE-604 | ||
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| 008 | 160912s2016 gw a||| m||| 00||| eng d | ||
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| 049 | |a DE-29 |a DE-29T |a DE-83 | ||
| 082 | 0 | |a 660 |2 23 | |
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| 100 | 1 | |a Machoke, Albert Gonche Fortunatus |d 1981- |e Verfasser |0 (DE-588)1113549920 |4 aut | |
| 245 | 1 | 0 | |a Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties |b = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |c Albert Gonche Fortunatus Machoke |
| 246 | 1 | 1 | |a Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| 264 | 1 | |a Aachen |b Shaker |c 2016 | |
| 300 | |a 244 Seiten |b 65 Illustrationen, Diagramme |c 21 cm x 14.8 cm, 404 g | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 0 | |a Berichte aus der Verfahrenstechnik | |
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2015 | ||
| 650 | 0 | 7 | |a Einkristall |0 (DE-588)4013901-3 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Herstellung |0 (DE-588)4159653-5 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Nanoporöser Stoff |0 (DE-588)4800345-1 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Zeolith ZSM5 |0 (DE-588)4336638-7 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Katalytische Aktivität |0 (DE-588)4279994-6 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a Katalytisches Kracken |0 (DE-588)4342085-0 |2 gnd |9 rswk-swf |
| 650 | 0 | 7 | |a MTO-Verfahren |0 (DE-588)4403285-7 |2 gnd |9 rswk-swf |
| 653 | |a MFI-type zeolites | ||
| 653 | |a Pt/ZSM-5 | ||
| 653 | |a bifunctional catalysts | ||
| 653 | |a catalytic cracking of cumene | ||
| 653 | |a hierarchical zeolites | ||
| 653 | |a layered zeolites | ||
| 653 | |a macroporous zeolites | ||
| 653 | |a methanol to olefins | ||
| 653 | |a multilamellar MFI | ||
| 653 | |a nanosized zeolites | ||
| 655 | 7 | |0 (DE-588)4113937-9 |a Hochschulschrift |2 gnd-content | |
| 689 | 0 | 0 | |a Zeolith ZSM5 |0 (DE-588)4336638-7 |D s |
| 689 | 0 | 1 | |a Nanoporöser Stoff |0 (DE-588)4800345-1 |D s |
| 689 | 0 | 2 | |a Einkristall |0 (DE-588)4013901-3 |D s |
| 689 | 0 | 3 | |a Herstellung |0 (DE-588)4159653-5 |D s |
| 689 | 0 | |5 DE-604 | |
| 689 | 1 | 0 | |a Zeolith ZSM5 |0 (DE-588)4336638-7 |D s |
| 689 | 1 | 1 | |a Katalytische Aktivität |0 (DE-588)4279994-6 |D s |
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Datensatz im Suchindex
| _version_ | 1804176576031490048 |
|---|---|
| adam_text | TABLE OF CONTENTS
1
INTRODUCTION.............................................................................................................1
1.1
MOTIVATION...........................................................................................................
1
1.2 GOALS OF THIS
THESIS..............................................................................................3
1.3 STRATEGY AND ORGANIZATION OF THIS
THESIS...............................................................3
2
ZEOLITES......................................................................................................................7
2.1
HISTORY................................................................................................................
7
2.2 DEFINITION, STRUCTURE AND CHEMICAL
COMPOSITION................................................8
2.3 MFI-TYPE
ZEOLITES...........................................................................................
11
2.4 SYNTHESIS OF
ZEOLITES..........................................................................................11
2.4.1 SYNTHESIS GEL PREPARATION
...........................................................................
13
2.4.2
CRYSTALLIZATION.............................................................................................16
2.4.3 PRODUCT
RECOVERY........................................................................................
20
2.4.4 POST-SYNTHESIS
MODIFICATIONS.....................................................................
20
2.5 PROPERTIES AND APPLICATIONS OF
ZEOLITES.............................................................21
3 ZEOLITES IN
CATALYSIS................................................................................................23
3.1 INTRODUCTION TO
CATALYSIS...................................................................................
23
3.2 COMPOSITION AND CLASSIFICATION OF
CATALYSTS.....................................................24
3.3 ZEOLITES AS
CATALYSTS..........................................................................................
24
3.3.1 BRONSTED AND LEWIS ACIDITY OF
ZEOLITES......................................................25
3.3.2 MICROPOROSITY AND SHAPE
SELECTIVITY..........................................................28
3.3.3 CONCENTRATION OR CONFINEMENT OF
MOLECULES.............................................30
4 NANOSIZED AND HIERARCHICAL
ZEOLITES.....................................................................31
4.1 INTRODUCTION AND
MOTIVATION..............................................................................
31
4.2 NANOSIZED ZEOLITES 33
4.2.1 DEFINITION, APPLICATIONS AND LIMITATIONS
..................................................
33
4.2.2 PREPARATION OF NANOSIZED
ZEOLITES.............................................................35
4.3 HIERARCHICAL
ZEOLITES.........................................................................................
37
4.3.1 CLASSIFICATION OF HIERARCHICAL
ZEOLITES.....................................................38
4.3.2 SELECTED STRATEGIES TO PREPARE HIERARCHICAL ZEOLITES
..........................
40
4.4 SUMMARY ON NANOSIZED AND HIERARCHICAL ZEOLITES
..........................................
43
5
EXPERIMENTAL.........................................................................................................
45
5.1 PREPARATION OF MULTILAMELLAR MFI-TYPE
ZEOLITES...............................................45
5.1.1 TEMPLATE
PREPARATION.................................................................................
46
5.1.2 GEL
PREPARATION..........................................................................................
47
5.1.3 CRYSTALLIZATION OF THE SYNTHESIS GEL INTO ZEOLITE
........................................
49
5.1.4 PRODUCT
RECOVERY........................................................................................
50
5.1.5 CHARACTERIZATION AND POST-SYNTHETIC
MODIFICATIONS...................................50
5.2 PREPARATION OF MESOPOROUS SILICA
PARTICLES.......................................................51
5.2.1 PREPARATION OF MSPS BY USING GAO ET AL.
PROCEDURE..................................52
5.2.2 PREPARATION OF MSP BY USING AHMED ET AL. PROCEDURE
.............................
53
5.3 PREPARATION OF NANOSIZED ZEOLITES FROM
MSPS.................................................54
5.4 PREPARATION OF
PT@MFI....................................................................................
55
5.5 PREPARATION OF ZEOLITE CRYSTALS WITH IMBEDDED MACROPORES
.............................
56
5.6 CATALYTIC CRACKING OF
CUMENE..........................................................................58
5.6.1 CATALYSTS USED AND THEIR
PREPARATION..........................................................58
5.6.2 DESCRIPTION OF THE CATALYST TESTING
UNITS.....................................................61
5.7 CHARACTERIZATION
TECHNIQUES.............................................................................
69
5.7.1 X-RAY DIFFRACTION
(XRD)..........................................................................
69
5.7.2 SMALL ANGLE SCATTERING
(SAXS)................................................................71
5.7.3 ELEMENTAL
ANALYSIS.....................................................................................
72
5.7.4 GAS
SORPTION...............................................................................................
72
5.7.5 TEMPERATURE PROGRAMMED DESORPTION OF AMMONIA (NH3-TPD)
..............
73
5.7.6 THERMOGRAVIMETRIC ANALYSIS
(TOA).........................................................73
5.7.7 SCANNING ELECTRON MICROSCOPE
(SEM).......................................................74
5.7.8 TRANSMISSION ELECTRON MICROSCOPE
(TEM)................................................75
5.7.9 SOLID-STATE NUCLEAR MAGNETIC RESONANCE (MAS NMR)
.............................
76
6 PREPARATION OF MULTILAMELLAR MFI-TYPE
ZEOLITES...............................................77
6.1 INTRODUCTION AND LITERATURE
REVIEW.....................................................................
77
6.2 RESULTS AND
DISCUSSION......................................................................................
81
6.2.1 CRYSTALLIZATION KINETICS UNDER TUMBLING
CONDITIONS...................................82
6.2.2 CRYSTALLIZATION KINETICS UNDER STATIC
CONDITIONS.........................................87
6.2.3 THE ROLE OF THE SPECIAL DESIGNED TEMPLATE/SURFACTANT
...............................
94
6.2.4 VARIATION OF TEMPLATE
AMOUNT....................................................................
97
6.2.5 VARIATION OF SI/AL
RATIO..............................................................................
99
6.3
SUMMARY.........................................................................................................133
7 CATALYTIC PERFORMANCE OF NANOSIZED AND HIERARCHICAL ZEOLITES
.....................
135
7.1 GOALS AND
OVERVIEW..........................................................................................135
7.2 CHARACTERIZATION OF DIFFERENT CATALYSTS
............................................................
136
7.2.1 STANDARD AND NANOSIZED MFI-TYPE ZEOLITE CATALYSTS
.................................
136
7.2.2 MULTILAMELLAR MFI-TYPE ZEOLITE
CATALYSTS................................................ 139
7.3 CATALYTIC CRACKING OF CUMENE
.........................................................................
145
7.3.1 INTRODUCTION AND THE STATE OF THE ART
.........................................................
145
7.3.2 CATALYTIC CRACKING OF CUMENE OVER MFI CATALYSTS WITH DIFFERENT
CRYSTAL
DIMENSIONS...........................................................................................................
147
7.3.3 CATALYTIC CRACKING OF CUMENE OVER MULTILAMELLAR MFI-TYPE ZEOLITES
....
149
7.3.4 COMPARISON OF DIFFERENT CATALYSTS
............................................................
151
7.4 CONVERSION OF METHANOL TO HYDROCARBONS
(MTH)..........................................155
7.4.1 INTRODUCTION AND THE STATE OF THE ART
.........................................................
155
7.4.2 CATALYTIC RESULTS AND DISCUSSION
...............................................................
158
7.5
SUMMARY.........................................................................................................164
8 PREPARATION OF NOVEL ZEOLITIC MATERIALS FROM MESOPOROUS SILICA
PARTICLES.... 167
8.1 INTRODUCTION AND THE STATE OF THE ART
................................................................
167
8.2 RESULTS AND DISCUSSION
....................................................................................
169
8.2.1 STRATEGIES USED TO INCORPORATE THE MICROPOROGEN IN MSPS
.......................
169
8.2.2 SCREENING RESULTS AND
DISCUSSION.............................................................
171
8.2.3 TRANSFORMATION OF MSPS INTO SPHERICAL NANOSIZED
ZEOLITES....................174
8.2.4 TRANSFORMATION OF MSPS INTO MFI-TYPE ZEOLITE CRYSTALS WITH
EMBEDDED
MACROPORES............................................................................................................
200
8.3
SUMMARY........................................................................................................
213
9 SUMMARY AND
CONCLUSIONS................................................................................
215
9.1 SHORTENING OF DIFFUSION PATH LENGTH
.................................................................
216
9.1.1 SHORTENING OF DIFFUSION PATH LENGTH VIA THE REDUCTION OF 1 CRYSTAL
DIMENSION..............................................................................................................
216
9.1.2 SHORTENING OF DIFFUSION PATH LENGTH VIA THE REDUCTION OF ALL 3
CRYSTAL
DIMENSIONS AND THE INTRODUCTION OF
MACROPORES...................................................219
9.2 THE ROLE OF REDUCED DIFFUSION PATH LENGTHS IN
CATALYSIS...................................221
9.3 CLOSING REMARKS AND
OUTLOOK..........................................................................224
REFERENCES....................................................................................................................225
A
APPENDIX.............................................................................................................
239
A. 1 CHEMICALS USED IN THIS
WORK.............................................................................239
A.2 PREPARATION OF MULTILAMELLAR MFI-TYPE ZEOLITES
.............................................
240
A.3 PREPARATION OF DIFFERENT CATALYSTS
....................................................................
242
A.4 TRANSFORMATION OF MSPS INTO NANOSIZED ZEOLITES
...........................................
243
A.5 TRANSFORMATION OF MSPS INTO MACROPOROUS ZEOLITES
......................................
244
|
| any_adam_object | 1 |
| author | Machoke, Albert Gonche Fortunatus 1981- |
| author_GND | (DE-588)1113549920 |
| author_facet | Machoke, Albert Gonche Fortunatus 1981- |
| author_role | aut |
| author_sort | Machoke, Albert Gonche Fortunatus 1981- |
| author_variant | a g f m agf agfm |
| building | Verbundindex |
| bvnumber | BV043760694 |
| ctrlnum | (OCoLC)958384716 (DE-599)DNB1109759584 |
| dewey-full | 660 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660 |
| dewey-search | 660 |
| dewey-sort | 3660 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV043760694 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T07:34:22Z |
| institution | BVB |
| institution_GND | (DE-588)1064118135 |
| isbn | 9783844046939 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-029172054 |
| oclc_num | 958384716 |
| open_access_boolean | |
| owner | DE-29 DE-29T DE-83 |
| owner_facet | DE-29 DE-29T DE-83 |
| physical | 244 Seiten 65 Illustrationen, Diagramme 21 cm x 14.8 cm, 404 g |
| publishDate | 2016 |
| publishDateSearch | 2016 |
| publishDateSort | 2016 |
| publisher | Shaker |
| record_format | marc |
| series2 | Berichte aus der Verfahrenstechnik |
| spelling | Machoke, Albert Gonche Fortunatus 1981- Verfasser (DE-588)1113549920 aut Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Albert Gonche Fortunatus Machoke Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Aachen Shaker 2016 244 Seiten 65 Illustrationen, Diagramme 21 cm x 14.8 cm, 404 g txt rdacontent n rdamedia nc rdacarrier Berichte aus der Verfahrenstechnik Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2015 Einkristall (DE-588)4013901-3 gnd rswk-swf Herstellung (DE-588)4159653-5 gnd rswk-swf Nanoporöser Stoff (DE-588)4800345-1 gnd rswk-swf Zeolith ZSM5 (DE-588)4336638-7 gnd rswk-swf Katalytische Aktivität (DE-588)4279994-6 gnd rswk-swf Katalytisches Kracken (DE-588)4342085-0 gnd rswk-swf MTO-Verfahren (DE-588)4403285-7 gnd rswk-swf MFI-type zeolites Pt/ZSM-5 bifunctional catalysts catalytic cracking of cumene hierarchical zeolites layered zeolites macroporous zeolites methanol to olefins multilamellar MFI nanosized zeolites (DE-588)4113937-9 Hochschulschrift gnd-content Zeolith ZSM5 (DE-588)4336638-7 s Nanoporöser Stoff (DE-588)4800345-1 s Einkristall (DE-588)4013901-3 s Herstellung (DE-588)4159653-5 s DE-604 Katalytische Aktivität (DE-588)4279994-6 s MTO-Verfahren (DE-588)4403285-7 s Katalytisches Kracken (DE-588)4342085-0 s Shaker Verlag (DE-588)1064118135 pbl DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029172054&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Machoke, Albert Gonche Fortunatus 1981- Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Einkristall (DE-588)4013901-3 gnd Herstellung (DE-588)4159653-5 gnd Nanoporöser Stoff (DE-588)4800345-1 gnd Zeolith ZSM5 (DE-588)4336638-7 gnd Katalytische Aktivität (DE-588)4279994-6 gnd Katalytisches Kracken (DE-588)4342085-0 gnd MTO-Verfahren (DE-588)4403285-7 gnd |
| subject_GND | (DE-588)4013901-3 (DE-588)4159653-5 (DE-588)4800345-1 (DE-588)4336638-7 (DE-588)4279994-6 (DE-588)4342085-0 (DE-588)4403285-7 (DE-588)4113937-9 |
| title | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| title_alt | Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| title_auth | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| title_exact_search | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| title_full | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Albert Gonche Fortunatus Machoke |
| title_fullStr | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Albert Gonche Fortunatus Machoke |
| title_full_unstemmed | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften Albert Gonche Fortunatus Machoke |
| title_short | Synthesis of MFI-Type Zeolites with Nano-Sized Dimensions and Hierarchical Porosities and their Effects on the Catalytic Properties |
| title_sort | synthesis of mfi type zeolites with nano sized dimensions and hierarchical porosities and their effects on the catalytic properties synthese von mfi typ zeolithen mit nanodimensionen und hierarchischen porositaten und deren effekte auf die katalytischen eigenschaften |
| title_sub | = Synthese von MFI-Typ Zeolithen mit Nanodimensionen und Hierarchischen Porositäten und deren Effekte auf die katalytischen Eigenschaften |
| topic | Einkristall (DE-588)4013901-3 gnd Herstellung (DE-588)4159653-5 gnd Nanoporöser Stoff (DE-588)4800345-1 gnd Zeolith ZSM5 (DE-588)4336638-7 gnd Katalytische Aktivität (DE-588)4279994-6 gnd Katalytisches Kracken (DE-588)4342085-0 gnd MTO-Verfahren (DE-588)4403285-7 gnd |
| topic_facet | Einkristall Herstellung Nanoporöser Stoff Zeolith ZSM5 Katalytische Aktivität Katalytisches Kracken MTO-Verfahren Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=029172054&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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