Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs): = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs)
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Erlangen ; Nürnberg
2016
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Item Description: | Aus: ChemPhysChem ; 12. 2011 unter dem Titel: Density Gradient Ultracentrifugation on Carbon Nanotubes According to Structural Integrity as a Foundation for an Absolute Purity Evaluation / Claudia Backes, Sebastian Bosch ... - Enthalten 5 weitere Sonderdrucke |
| Physical Description: | IV, 171 Seiten Illustrationen, Diagramme |
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| 245 | 1 | 0 | |a Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) |b = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |c vorgelegt von Sebastian Bosch |
| 246 | 1 | 1 | |a Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| 264 | 1 | |a Erlangen ; Nürnberg |c 2016 | |
| 300 | |a IV, 171 Seiten |b Illustrationen, Diagramme | ||
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| 500 | |a Aus: ChemPhysChem ; 12. 2011 unter dem Titel: Density Gradient Ultracentrifugation on Carbon Nanotubes According to Structural Integrity as a Foundation for an Absolute Purity Evaluation / Claudia Backes, Sebastian Bosch ... - Enthalten 5 weitere Sonderdrucke | ||
| 502 | |b Dissertation |c Friedrich-Alexander-Universität Erlangen-Nürnberg |d 2016 | ||
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| adam_text | SELECTIVE COVALENT FUNCTIONALIZATION SEQUENCES OF
SINGLE-WALLED CARBON NANOTUBES (SWCNTS)
SELEKTIVE KOVALENTE FUNKTIONALISIERUNGSSEQUENZEN
VON EINWANDIGEN KOHLENSTOFFNANOROEHREN (SWCNTS)
DER NATURWISSENSCHAFTLICHEN FAKUELTAET DER FRIEDRICH-ALEXANDER-UNIVERSITAET
ERLANGEN-NUERNBERG
ZUR
ERLANGUNG DES DOKTORGRADES DR. RER. NAT.
VORGELEGT VON
SEBASTIAN BOSCH
AUS
TREUCHTLINGEN
LIST OF
ABBREVIATIONS..........................................................................................................................ILL
1.
INTRODUCTION...................................................................................................................
1
1.1. SWCNT
PHYSICS...............................................................................................................2
1.1.1. STRUCTURE AND PROPERTIES OF
SWCNTS.........................................................................2
1.1.2. SPECIFIC ISSUES FOR SWCNT
APPLICATIONS.....................................................................4
1.1.3. CHARACTERIZATION OF
SWCNTS........................................................................................
5
1.1.3.1. ABSORPTION AND FLUORESCENCE
SPECTROSCOPY.......................................................6
1.1.3.2. RAMAN
SPECTROSCOPY..............................................................................................7
1.1.3.3. THERMOGRAVITOOL ANALYSIS
...................................................................................
9
1.2. SWCNT
CHEMISTRY.......................................................................................................10
1.2.1. FUNCTIONALIZATION OF
SWCNTS.....................................................................................10
1.2.2. COVALENT FUNCTIONALIZATION OF
SWCNTS.....................................................................11
1.2.3. SELECTIVE FUNCTIONALIZATION OF
SWCNTS.....................................................................14
1.2.3.1. SELECTIVE FUNCTIONALIZATION OF SWCNTS BY DIAZONIUM
CHEMISTRY.................15
1.2.3.2. SELECTIVE FUNCTIONALIZATION OF SWCNTS BY REDUCTIVE
CHEMISTRY..................17
1.2.3.3. OVERVIEW OF SPECIFIC EFFECTS INFLUENCING SWCNT SELECTIVITY
.........................
19
1.2.4. SPECIFIC ISSUES FOR SWCNT
SEPARATION......................................................................23
2.
PROPOSAL.......................................................................................................................
25
3. INDEX OF
PUBLICATIONS...................................................................................................26
4. RESULTS AND
DISCUSSION...............................................................................................
27
4.1. DEVELOPMENT OF NEW ANALYTICAL CHARACTERIZATION TOOLS FOR
SWCNTS....................27
4.1.1. DENSITY GRADIENT ULTRACENTRIFUGATION ON CARBON NANOTUBES
ACCORDING TO
STRUCTURAL INTEGRITY AS A FOUNDATION FOR AN ABSOLUTE PURITY EVALUATION
.............
29
4.1.1.1.
PREFACE..................................................................................................................
29
4.1.1.2.
MANUSCRIPT............................................................................................................32
4.1.1.3. ELECTRONIC SUPPORTING
INFORMATION....................................................................38
4.1.2. STATISTICAL RAMAN SPECTROSCOPY: A METHOD FOR THE CHARACTERIZATION
OF
COVALENTLY FUNCTIONALIZED SINGLE-WALLED CARBON NANOTUBES
..............................
44
4.1.2.1.
PREFACE..................................................................................................................
44
4.1.2.2.
MANUSCRIPT............................................................................................................49
4.1.2.3. ELECTRONIC SUPPORTING
INFORMATION....................................................................54
4.2. INVESTIGATION OF SELECTIVE COVALENT SWCNT FUNCTIONALIZATION
SEQUENCES
...........
63
4.2.1. A SUPRAMOLECULAR APPROACH FOR THE FACILE SOLUBILIZATION AND
SEPARATION OF
COVALENTLY FUNCTIONALIZED SINGLE-WALLED CARBON NANOTUBES
..............................
66
4.2.1.1.
PREFACE..................................................................................................................66
4.2.1.2.
MANUSCRIPT...........................................................................................................
69
4.2.1.3. ELECTRONIC SUPPORTING
INFORMATION...................................................................
75
4.2.2. REDUCTIVE ARYLATION OF SWCNTS: INFLUENCE OF THE REDUCING AGENT
AND THE
TRAPPING
ELECTROPHILE................................................................................................
80
4.2.2.1.
PREFACE..................................................................................................................80
4.2.2.2.
MANUSCRIPT...........................................................................................................
82
4.2.2.3. ELECTRONIC SUPPORTING INFORMATION
...................................................................
87
4.2.3. NEW BASIC INSIGHT INTO REDUCTIVE FUNCTIONALIZATION SEQUENCES OF
SINGLE-
WALLED CARBON NANOTUBES
(SWCNTS)........................................................................94
4.2.3.1.
PREFACE..................................................................................................................94
4.2.3.2.
MANUSCRIPT...........................................................................................................
97
4.2.3.3. ELECTRONIC SUPPORTING INFORMATION
.................................................................
109
4.2.4. SELECTIVE REDUCTION OF SWCNTS - CONCEPTS AND
INSIGHTS........................................134
4.2.4.1.
PREFACE...............................................................................................................134
4.2.4.2.
MANUSCRIPT..........................................................................................................137
4.2.4.3. ELECTRONIC SUPPORTING
INFORMATION..................................................................149
5.
SUMMARY....................................................................................................................
159
6.
ZUSAMMENFASSUNG....................................................................................................162
7.
LITERATURE....................................................................................................................
165
|
| any_adam_object | 1 |
| author | Bosch, Sebastian |
| author_GND | (DE-588)1095683306 |
| author_facet | Bosch, Sebastian |
| author_role | aut |
| author_sort | Bosch, Sebastian |
| author_variant | s b sb |
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| bvnumber | BV043498181 |
| ctrlnum | (OCoLC)947072762 (DE-599)BVBBV043498181 |
| dewey-full | 610 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 610 - Medicine and health |
| dewey-raw | 610 |
| dewey-search | 610 |
| dewey-sort | 3610 |
| dewey-tens | 610 - Medicine and health |
| discipline | Medizin |
| format | Thesis Book |
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| indexdate | 2024-07-10T07:27:19Z |
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| language | English |
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| physical | IV, 171 Seiten Illustrationen, Diagramme |
| publishDate | 2016 |
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| spelling | Bosch, Sebastian Verfasser (DE-588)1095683306 aut Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) vorgelegt von Sebastian Bosch Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) Erlangen ; Nürnberg 2016 IV, 171 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Aus: ChemPhysChem ; 12. 2011 unter dem Titel: Density Gradient Ultracentrifugation on Carbon Nanotubes According to Structural Integrity as a Foundation for an Absolute Purity Evaluation / Claudia Backes, Sebastian Bosch ... - Enthalten 5 weitere Sonderdrucke Dissertation Friedrich-Alexander-Universität Erlangen-Nürnberg 2016 (DE-588)4113937-9 Hochschulschrift gnd-content DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028914637&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Bosch, Sebastian Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| subject_GND | (DE-588)4113937-9 |
| title | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| title_alt | Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| title_auth | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| title_exact_search | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| title_full | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) vorgelegt von Sebastian Bosch |
| title_fullStr | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) vorgelegt von Sebastian Bosch |
| title_full_unstemmed | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) vorgelegt von Sebastian Bosch |
| title_short | Selective covalent functionalization sequences of single-walled carbon nanotubes (SWCNTs) |
| title_sort | selective covalent functionalization sequences of single walled carbon nanotubes swcnts selektive kovalente funktionalisierungssequenzen von einwandigen kohlenstoffnanorohren swcnts |
| title_sub | = Selektive kovalente Funktionalisierungssequenzen von einwandigen Kohlenstoffnanoröhren (SWCNTs) |
| topic_facet | Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028914637&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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