Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems:
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Dresden
2015
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| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XII, 139 Seiten Illustrationen, Diagramme |
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| 245 | 1 | 0 | |a Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems |c von Dipl.-Ing. Martin Lustfeld |
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Record in the Search Index
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|---|---|
| adam_text | CONTENTS
ABSTRACT I
KURZFASSUNG ILL
ACKNOWLEDGMENT V
CONTENTS VII
ABBREVIATIONS X
NOMENCLATURE XI
1 INTRODUCTION 1
2 SAFETY ENHANCEMENT OF NUCLEAR POWER FACILITIES 3
2.1 SAFETY DESIGN OF NUCLEAR POWER PLANTS 3
2.2 LIGHT WATER REACTORS 5
2.2.1 CURRENT NUCLEAR FUELS IN LIGHT WATER REACTORS 6
2.2.2 ACCIDENT TOLERANT FUELS IN LIGHT WATER REACTORS 7
2.3 GRAPHITE MODERATED, GAS COOLED REACTORS 8
2.3.1 REACTOR DESIGN FEATURES 8
2.3.2 COATED PARTICLE FUEL 10
2.4 SILICON CARBIDE FOR ENHANCED NUCLEAR FUEL SYSTEMS 11
2.4.1 SIC PERFORMANCE AS A NUCLEAR MATERIAL 11
2.4.2 COMBINATION OF SIC AND GRAPHITE FOR NUCLEAR APPLICATIONS 12
2.4.3 SIC COMPOSITE MATERIALS FOR ATF CLADDINGS 13
2.4.4 SIC COATINGS IN TRISO PARTICLES 15
2.4.5 NANOCRYSTALLINE SIC FOR THE ENHANCEMENT OF FUEL SYSTEMS 17
3 DESIGN AND PREPARATION OF NANOCRYSTALLINE SIC AND SIC-PYC COATINGS 19
3.1 COATING TECHNOLOGIES FOR THE DEPOSITION OF SIC COATINGS 19
3.1.1 PREPARATION OF COARSE-GRAINED SIC BY CHEMICAL VAPOR DEPOSITION 19
3.1.2 PREPARATION OF NANOCRYSTALLINE SIC BY PULSED LASER DEPOSITION 21
3.2 CHARACTERISTICS OF THE PLD COATING TECHNOLOGY 22
3.3 PROPERTIES OF PLD COATINGS 25
3.3.1 DEPOSITION AND GROWTH OF PLD THIN FILMS 25
3.3.2 RESIDUAL STRESSES AND MECHANICAL STABILITY OF PLD COATINGS 27
VII
HTTP://D-NB.INFO/1081648392
3.3.3 THERMAL STABILITY OF PLD COATING 31
3.3.4 STABILITY OF PLD-SIC COATINGS UNDER IRRADIATION 34
3.3.5 CHEMICAL STABILITY OF PLD-SIC THIN FILMS 36
3.3.6 STATE OF THE ART OF SIC THIN FILM PREPARATION BY PLD 37
3.4 CONCLUSIONS OF THE LITERATURE STUDY 41
3.5 DESIGN OF EXPERIMENTS 42
3.5.1 SETTINGS OF THE PLD SETUP 42
3.5.2 PARAMETERS OF THERMAL ANNEALING EXPERIMENTS 44
3.5.3 APPLIED MEASUREMENT METHODOLOGIES 45
4 EXPERIMENTAL PROCEDURE AND PARAMETER CHOICE FOR SAMPLE PREPARATION 48
4.1 PLD EXPERIMENTAL SETUP 48
4.1.1 GENERAL DESCRIPTION OF THE PLD COATING SETUP 48
4.1.2 VACUUM CHAMBER SETUP 50
4.1.3 TARGET MATERIAL ABLATION BY THE PULSED EXCIMER LASER 51
4.1.4 SUBSTRATE MATERIALS 53
4.1.5 PROPERTIES OF THE DIODE INFRARED LASER FOR SUBSTRATE HEATING 54
4.2 DIODE LASER SETTINGS FOR THE PREPARATION OF SIC AND SIC-PYC COATINGS
55
4.3 SUBSTRATE TEMPERATURE MEASUREMENT AND PROCESS CONTROL 57
4.3.1 CORRELATION FOR THE SUBSTRATE THERMAL EMISSIVITY 57
4.3.2 ESTIMATION OF THE SUBSTRATE TEMPERATURES DURING PLD COATING 59
4.3.3 SPATIAL DISTRIBUTION OF THE SUBSTRATE TEMPERATURE 61
4.3.4 CONCLUSIONS ON SUBSTRATE TEMPERATURES IN THE PRESENT WORK 62
4.4 PLD PROCESS CONTROL BY INFRARED CAMERA 63
4.4.1 RELATION BETWEEN COATING THICKNESS AND INFRARED CAMERA SIGNAL....
63
4.4.2 PROCESS CONTROL BY INFRARED CAMERA 65
4.5 EXPERIMENTAL PROCEDURE AND MATRICES 66
4.5.1 PLD COATING PROCEDURE 66
4.5.2 DEFINITION OF EXPERIMENTAL SERIES AND EXPERIMENTAL MATRICES 67
5 CHARACTERIZATION OF THE PLD-SIC AND PLD-SIC-PYC COATINGS 73
5.1 CHARACTERIZATION OF PLD-SIC SINGLE-LAYER COATINGS 73
5.1.1 GENERAL APPEARANCE AND INTEGRITY OF THE COATINGS 73
5.1.2 COATING THICKNESS AND DEPOSITION RATE 77
5.1.3 RESIDUAL COATING STRESSES 79
5.1.4 SIC PHASE ANALYSIS BY XRD 83
5.1.5 COATING COMPOSITION ANALYSIS BY XPS 86
5.1.6 CONCLUSIONS ON SINGLE-LAYER PLD-SIC COATING PROPERTIES 88
5.2 CHARACTERIZATION OF PLD-SIC-PYC MULTILAYER COATINGS 89
5.2.1 FE-SEM ANALYSIS OF SIC-PYC MULTILAYER COATINGS 91
5.2.2 TEM ANALYSIS OF SIC-PYC MULTILAYER CROSS SECTIONS 94
5.2.3 XPS ANALYSIS OF SIC-PYC MULTILAYER ELEMENTAL COMPOSITION 98
5.2.4 RELAXATION OF THE SIC SUBLAYERS DUE TO TEMPERATURE CYCLING 99
5.2.5 CONCLUSIONS ON PLD-SIC-PYC COATING PROPERTIES 102
6 HIGH-TEMPERATURE ANNEALING RESPONSE OF SIC AND SIC-PYC COATINGS 104
6.1 ANNEALING TESTING PROCEDURE 104
6.2 APPEARANCE OF THE COATINGS SUBSEQUENT TO ANNEALING 105
6.2.1 SAMPLE INTEGRITY SUBSEQUENT TO ANNEALING 105
6.2.2 SAMPLE BENDING AFTER ANNEALING 107
6.3 SIC GRAIN GROWTH UPON ANNEALING 108
6.4 MICROSTRUCTURAL FE-SEM AND TEM ANALYSIS OF ANNEALED COATINGS 110
6.4.1 FE-SEM ANALYSES OF ANNEALED SINGLE-LAYER COATINGS 111
6.4.2 FE-SEM ANALYSES OF ANNEALED MULTILAYER COATINGS 114
6.4.3 TEM ANALYSIS OF SAMPLE ESG12 117
6.5 CONCLUSION OF THE HIGH-TEMPERATURE ANNEALING TESTS 119
7 SUMMARY, CONCLUSION AND OUTLOOK 122
REFERENCES 126
IX
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| author_GND | (DE-588)1080040005 |
| author_facet | Lustfeld, Martin 1983- |
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| discipline | Werkstoffwissenschaften / Fertigungstechnik |
| format | Thesis Book |
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| indexdate | 2024-07-10T07:23:31Z |
| institution | BVB |
| language | English |
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| physical | XII, 139 Seiten Illustrationen, Diagramme |
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| spelling | Lustfeld, Martin 1983- Verfasser (DE-588)1080040005 aut Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems von Dipl.-Ing. Martin Lustfeld Dresden 2015 XII, 139 Seiten Illustrationen, Diagramme txt rdacontent n rdamedia nc rdacarrier Dresden Technische Universität Dresden 2015 Hochtemperaturwerkstoff (DE-588)4025280-2 gnd rswk-swf Siliciumcarbid (DE-588)4055009-6 gnd rswk-swf Mehrschichtsystem (DE-588)4244347-7 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Siliciumcarbid (DE-588)4055009-6 s Mehrschichtsystem (DE-588)4244347-7 s Hochtemperaturwerkstoff (DE-588)4025280-2 s DE-604 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028761787&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Lustfeld, Martin 1983- Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems Hochtemperaturwerkstoff (DE-588)4025280-2 gnd Siliciumcarbid (DE-588)4055009-6 gnd Mehrschichtsystem (DE-588)4244347-7 gnd |
| subject_GND | (DE-588)4025280-2 (DE-588)4055009-6 (DE-588)4244347-7 (DE-588)4113937-9 |
| title | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems |
| title_auth | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems |
| title_exact_search | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems |
| title_full | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems von Dipl.-Ing. Martin Lustfeld |
| title_fullStr | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems von Dipl.-Ing. Martin Lustfeld |
| title_full_unstemmed | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems von Dipl.-Ing. Martin Lustfeld |
| title_short | Assessment of nanocrystalline ceramic multilayer coatings for the application in high-temperature energy systems |
| title_sort | assessment of nanocrystalline ceramic multilayer coatings for the application in high temperature energy systems |
| topic | Hochtemperaturwerkstoff (DE-588)4025280-2 gnd Siliciumcarbid (DE-588)4055009-6 gnd Mehrschichtsystem (DE-588)4244347-7 gnd |
| topic_facet | Hochtemperaturwerkstoff Siliciumcarbid Mehrschichtsystem Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028761787&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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