Catalytic reactors:
Saved in:
| Main Author: | |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Berlin
De Gruyter
2016
|
| Series: | De Gruyter Graduate
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XVIII, 338 Seiten Illustrationen, graphische Darstellungen |
| ISBN: | 9783110332964 |
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Record in the Search Index
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| adam_text |
CONTENTS
LIST OF CONTRIBUTING
AUTHORS * V
ABOUT THE EDITOR VII
PREFACE * VIII
SANJAY M. MAHAJANI AND BASUDEB SAHA
1 CATALYSIS IN MULTIFUNCTIONAL
REACTORS * 1
1.1 INTRODUCTION * 1
1.2 REACTIVE DISTILLATION (RD) 1
1.2.1 HOMOGENEOUS CATALYSIS 2
1.2.2 HETEROGENEOUS CATALYSIS 3
1.2.3 CATALYSTS USED IN REACTIVE DISTILLATION 8
1.3 REACTIVE STRIPPING 13
1.3.1 ESTERIFICATION 14
1.3.2 AQUEOUS PHASE REFORMING (APR) OF SORBITOL 17
1.3.3 DEHYDRATION OF XYLOSE TO FURFURAL 17
1.3.4 CATALYTIC EXCHANGE OF HYDROGEN ISOTOPES *18
1.4 CATALYTIC MEMBRANE REACTORS *19
1.4.1 BIODIESEL PRODUCTION 20
1.4.2 DEHYDROGENATION 24
1.4.3 OXIDATIVE COUPLING OF METHANE (OCM) 25
1.4.4 PARTIAL OXIDATION OF METHANE TO SYNTHESIS GAS 26
1.5 CHROMATOGRAPHIC REACTOR * 26
1.5.1 CONCEPT OF A CHROMATOGRAPHIC REACTOR 27
1.5.2 TYPES OF CHROMATOGRAPHIC REACTOR 28
1.5.3 APPLICATIONS OF LIQUID CHROMATOGRAPHIC REACTOR 34
1.6 SUMMARY 41
GORAN T. VLADISAVLJEVIC
2 BIOCATALYTIC MEMBRANE REACTORS
(BMR) 51
2.1 INTRODUCTION 52
2.2 ROLE OF MEMBRANE IN BIOCATALYTIC MEMBRANE REACTORS (BMRS)
2.3 MEMBRANE SEPARATION REACTORS (MSRS) 57
2.3.1 CONCEPT 57
2.3.2 APPLICATION 60
2.4 MEMBRANE AERATION BIOREACTORS (MABR) 64
2.5 EXTRACTIVE MEMBRANE BIOREACTORS (EMBR) 65
2.5.1 CONCEPT 65
2.5.2 APPLICATION 67
HTTP://D-NB.INFO/1061099067
XIV
CONTENTS
2.6 ENZYME IMMOBILIZATION TECHNIQUES IN MEMBRANE REACTOR SYSTEMS 70
2.6.1 PHYSICAL ADSORPTION 72
2.6.2 ENTRAPMENT 72
2.6.3 CROSS-LINKING 73
2.6.4 ENCAPSULATION 73
2.6.5 SEGREGATION BY MEMBRANES * 77
2.6.6 COVALENT BINDING 77
2.7 LAMINATED (MULTILAYER) ENZYME MEMBRANE REACTORS * 81
2.7.1 CONCEPT 81
2.7.2 APPLICATION 83
2.8 BIPHASIC (MULTIPHASE) MEMBRANE BIOREACTORS 86
2.8.1 CONCEPT-*86
2.8.2 APPLICATION 88
2.9 PHASE TRANSFER CATALYSIS IN MULTIPHASE MEMBRANE REACTORS 92
2.9.1 CONCEPT 92
2.9.2 APPLICATION 93
2.10 CONCLUSIONS 94
ELNAZ SHAHBAZALI, VOLKER HESSEL, TIMOTHY NOSL, AND QI WANG
3 METALLIC NANOPARTICLES MADE
IN FLOW AND THEIR CATALYTIC APPLICATIONS
IN
MICRO-FLOW REACTORS FOR ORGANIC SYNTHESIS *103
3.1 INTRODUCTION 103
3.2 METAL NANOPARTICLES IN A MICROFLUIDIC REACTOR 105
3.2.1 GOLD 105
3.2.2 SILVER 114
3.2.3 PALLADIUM *117
3.2.4 PLATINUM 120
3.2.5 COPPER 122
3.3 METAL NANOPARTICLES IN A MILLIFLUIDIC REACTOR 123
3.4 OUTLOOK - METAL NANOPARTICLES GENERATED IN FLOW AND USED
IN SITU 127
3.5 CONCLUSIONS 128
STANISLAV Y. IVANOV AND AJAY K. RAY
4 APPLICATION OF MULTI-OBJECTIVE OPTIMIZATION
IN THE
DESIGN AND OPERATION OF
INDUSTRIAL
CATALYTIC REACTORS AND PROCESSES *134
4.1 INTRODUCTION 134
4.2 MULTI-OBJECTIVE OPTIMIZATION 136
4.2.1 CONCEPT OF MULTI-OBJECTIVE OPTIMIZATION 136
4.2.2 MOO METHODS 137
4.3 NO-PREFERENCE METHODS 138
4.3.1 NEUTRAL COMPROMISED SOLUTION 138
CONTENTS
* XV
4.4
A PRIORI METHODS 139
4.4.1
METHOD OF WEIGHTED GLOBAL CRITERION 139
4.4.2
LEXICOGRAPHIC METHOD 140
4.4.3
GOAL PROGRAMMING (GP) 141
4.5
A POSTERIORI METHODS 141
4.5.1
-CONSTRAINT METHOD 141
4.6
INTERACTIVE METHODS 142
4.7
GENETIC ALGORITHMS 142
4.7.1
ABOUT BINARY-CODED VARIABLES 143
4.7.2
SIMPLE GENETIC ALGORITHM (SGA) 144
4.7.3
USE OF GA IN MOO 145
4.7.4
CONSTRAINT HANDLING IN GA 146
4.8
SIMULATED ANNEALING 148
4.9
MOO PROBLEMS IN CHEMICAL ENGINEERING 148
4.9.1
PETROLEUM PROCESSING ENGINEERING 149
4.9.2
STEAM REFORMING 150
4.9.3
POLYMER INDUSTRY 152
4.10
CONCLUSIONS 168
VOLKAN DEGIRMENCI AND EVGENY V. REBROV
5 DESIGN OF CATALYTIC MICRO TRICKLE BED REACTORS 174
5.1
INTRODUCTION 175
5.2
HYDRODYNAMICS 179
5.2.1
FLOW REGIMES 179
5.2.2
PRESSURE DROP 187
5.2.3
LIQUID HOLDUP 191
5.2.4
FLOW MALDISTRIBUTION AND START-UP EFFECTS 193
5.2.5
AXIAL DISPERSION 194
5.3
MASS AND HEAT TRANSFER IN MICRO TRICKLE BED REACTORS 197
5.3.1
MASS TRANSFER 197
5.3.2
HEAT TRANSFER 201
5.3.3
SCALE UP 204
5.4
PERIODIC OPERATION * 206
5.5
APPLICATIONS 207
5.5.1
MICRO TRICKLE BED REACTORS 208
5.5.2
SEMI-STRUCTURED AND STRUCTURED TRICKLE BED REACTORS
212
5.6
OUTLOOK 212
JOSEPH WOOD
6
THREE-PHASE CATALYTIC REACTORS
FOR HYDROGENATION AND OXIDATION
REACTIONS 220
6.1 INTRODUCTION 222
XVI
CONTENTS
6.2 SLURRY REACTORS 223
6.2.1 THEORY: DETERMINATION OF CONTROLLING RESISTANCE 223
6.2.2 MIXING AND MASS TRANSFER IN THE STIRRED TANK SLURRY REACTOR 226
6.2.3 HYDROGENATION REACTIONS IN THE STIRRED TANK SLURRY REACTOR:
KINETICS AND
EFFECT OF OPERATING VARIABLES 235
6.2.4 CATALYSTS FOR HYDROGENATION REACTIONS: OVERVIEW AND NOVEL BIOMASS
SUPPORTED METAL CATALYSTS 238
6.2.5 OXIDATION REACTIONS IN THE SLURRY REACTOR * 245
6.2.6 BUBBLE COLUMN REACTORS 248
6.3 TRICKLE BED REACTORS 253
6.3.1 THEORY AND FLOW REGIMES 253
6.3.2 OVERALL RATE MODEL 255
6.3.3 IMAGING OF GAS-LIQUID FLOWS 256
6.3.4 SCALE UP AND
MODELING 258
6.3.5 ENANTIOSELECTIVE HYDROGENATION REACTIONS 261
6.3.6 INDUSTRIAL APPLICATIONS IN HEAVY OIL UPGRADING 264
6.4 STRUCTURED MONOLITH REACTORS 267
6.4.1 FLOW PATTERNS IN THE SINGLE CAPILLARY 268
6.4.2 APPLICATIONS IN HYDROGENATION REACTIONS 271
6.5 CONCLUSIONS 274
TEUVO KILPIO, VINCENZO RUSSO, KARI ERSNEN,
AND TAPIO SALMI
7 DESIGN AND MODELING
OF LABORATORY SCALE THREE-PHASE
FIXED BED
REACTORS 283
7.1 BACKGROUND 285
7.2 REACTOR SET-UP 287
7.3 PHYSICAL AND CHEMICAL PHENOMENA IN FIXED BED REACTORS * 288
7.3.1 OVERVIEW 288
7.4 RESEARCH TARGETS AND TOPICS 289
7.4.1 CATALYST SELECTION 289
7.4.2 REACTION KINETICS 290
7.4.3 MASS TRANSFER EFFECTS 290
7.4.4 HEAT EFFECTS 290
7.4.5 PHYSICAL PROPERTIES OF GASES AND LIQUIDS 290
7.4.6 REACTOR DESIGN AND OPERATION POLICY 290
7.4.7 MODELING OPTIONS 291
7.5 EXPERIMENTAL DESIGN 291
7.5.1 TARGETED PRODUCTS 292
7.5.2 CATALYST SCREENING 292
7.5.3 EXPERIMENTAL PRODUCTIVITY AND SELECTIVITY OPTIMIZATION 292
7.5.4 PARTICLE GEOMETRY 293
7.5.5 FEED DISTRIBUTION AND FLOW REGIMES 293
CONTENTS
XVII
7.5.6 BED DILUTION 294
7.5.7 RESIDENCE TIME DISTRIBUTION 294
7.6 CHEMICAL KINETICS 295
7.6.1 TOPICS OF THE KINETIC STUDIES 295
7.6.2 REACTION SCHEME SIMPLIFICATIONS 295
7.6.3 RATE EXPRESSIONS 296
7.6.4 QUALITATIVE REACTION RATE COMPARISON: FIXED BED AGAINST BATCH
REACTORS 297
7.6.5 CATALYST DEACTIVATION 298
7.6.6 TRULY INTRINSIC KINETICS 299
7.7 MASS AND HEAT TRANSFER EFFECTS 299
7.7.1 MASS TRANSFER RESISTANCES 299
7.7.2 GAS-LIQUID MASS TRANSFER 300
7.7.3 LIQUID-SOLID MASS AND HEAT TRANSFER 301
7.7.4 INTERNAL DIFFUSION - PORE DIFFUSION 302
7.7.5 EFFECTIVENESS FACTORS FOR PARTICLES 303
7.8 PHYSICAL PROPERTIES OF GAS MIXTURES AND SOLUTIONS 303
7.8.1 DENSITY AND VISCOSITY 303
7.8.2 DIFFUSIVITY 304
7.8.3 GAS SOLUBILITY 305
7.8.4 THERMAL CONDUCTIVITY 305
7.8.5 REACTION ENTHALPY 306
7.9 LIQUID FLOW EFFECTS 306
7.9.1 QUALITATIVE FLOW ARRANGEMENT COMPARISON 306
7.9.2 EXTERNAL WETTING OF THE CATALYST 307
7.9.3 RADIAL FLOW 307
7.9.4 PRESSURE DROP 308
7.9.5 LIQUID SATURATION (HOLD-UP) 309
7.10 REACTOR MODELING STEPS 311
7.10.1 OVERVIEW 311
7.10.2 SELECTED MODELING POLICY 311
7.10.3 STUDIES OF SIMPLIFIED REACTION SYSTEMS 311
7.10.4 WAYS HOW TO RULE OUT PHENOMENA BY EXPERIMENTAL DESIGN * 312
7.10.5 SENSITIVITY STUDIES 312
7.11 BALANCES FOR THE GENERIC THREE-PHASE FIXED BED MODEL 312
7.11.1 MASS BALANCES FOR GAS, LIQUID AND SOLID PHASES 312
7.11.2 ENERGY BALANCES FOR GAS-, LIQUID- AND SOLID PHASES 313
7.11.3 BOUNDARY CONDITIONS 314
7.11.4 SUB-MODEL EXAMPLES 315
7.12 AXIAL DISPERSION MODELING AND EXPERIMENTS 315
7.12.1 CLASSICAL AXIAL DISPERSION MODEL 315
7.12.2 ALTERNATIVE MODELING APPROACHES FOR BACK-MIXING 316
XVIII
CONTENTS
7.13 NUMERICAL STRATEGIES 316
7.13.1 MODEL CLASSIFICATION 316
7.13.2 BENEFITS OF DYNAMIC MODELS 317
7.13.3 SOLVERS AND SOLUTION ALGORITHMS 317
7.13.4 NUMERICAL METHOD OF LINES 318
7.13.5 HOYOS METHOD FOR PARTICLES 318
7.13.6 PARAMETER OPTIMIZATION METHODS 319
7.13.7 PARAMETER NUMBER REDUCTION * 319
7.14 SCALE-UP ISSUES OF FIXED BEDS 320
7.14.1 OVERVIEW 320
7.14.2 LARGE SCALE OPERATION 320
7.14.3 GRADIENTS IN SCALE UP 321
7.14.4 FLOW REGIME IN SCALE-UP 321
7.14.5 BACK MIXING IN SCALE-UP 321
7.15 EXAMPLES 322
7.15.1 CITRAL HYDROGENATION 322
7.15.2 DIRECT SYNTHESIS OF HYDROGEN PEROXIDE 323
7.16 CONCLUSIONS 327
INDEX 333 |
| any_adam_object | 1 |
| author | Saha, Basudeb |
| author_facet | Saha, Basudeb |
| author_role | aut |
| author_sort | Saha, Basudeb |
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| dewey-full | 660 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 660 - Chemical engineering |
| dewey-raw | 660 |
| dewey-search | 660 |
| dewey-sort | 3660 |
| dewey-tens | 660 - Chemical engineering |
| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV042997859 |
| illustrated | Illustrated |
| indexdate | 2024-09-10T01:56:41Z |
| institution | BVB |
| isbn | 9783110332964 |
| language | English |
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| open_access_boolean | |
| owner | DE-29T DE-92 DE-83 DE-703 |
| owner_facet | DE-29T DE-92 DE-83 DE-703 |
| physical | XVIII, 338 Seiten Illustrationen, graphische Darstellungen |
| publishDate | 2016 |
| publishDateSearch | 2016 |
| publishDateSort | 2016 |
| publisher | De Gruyter |
| record_format | marc |
| series2 | De Gruyter Graduate |
| spelling | Saha, Basudeb Verfasser aut Catalytic reactors edited by Basudeb Saha Berlin De Gruyter 2016 XVIII, 338 Seiten Illustrationen, graphische Darstellungen txt rdacontent n rdamedia nc rdacarrier De Gruyter Graduate Katalyse (DE-588)4029921-1 gnd rswk-swf Chemischer Reaktor (DE-588)4121085-2 gnd rswk-swf Chemische Verfahrenstechnik (DE-588)4069941-9 gnd rswk-swf Chemischer Reaktor (DE-588)4121085-2 s Katalyse (DE-588)4029921-1 s DE-604 Chemische Verfahrenstechnik (DE-588)4069941-9 s Erscheint auch als Online-Ausgabe, EPUB 978-3-11-039012-4 Erscheint auch als Online-Ausgabe, PDF 978-3-11-033298-8 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4828496&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028423142&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Saha, Basudeb Catalytic reactors Katalyse (DE-588)4029921-1 gnd Chemischer Reaktor (DE-588)4121085-2 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| subject_GND | (DE-588)4029921-1 (DE-588)4121085-2 (DE-588)4069941-9 |
| title | Catalytic reactors |
| title_auth | Catalytic reactors |
| title_exact_search | Catalytic reactors |
| title_full | Catalytic reactors edited by Basudeb Saha |
| title_fullStr | Catalytic reactors edited by Basudeb Saha |
| title_full_unstemmed | Catalytic reactors edited by Basudeb Saha |
| title_short | Catalytic reactors |
| title_sort | catalytic reactors |
| topic | Katalyse (DE-588)4029921-1 gnd Chemischer Reaktor (DE-588)4121085-2 gnd Chemische Verfahrenstechnik (DE-588)4069941-9 gnd |
| topic_facet | Katalyse Chemischer Reaktor Chemische Verfahrenstechnik |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4828496&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028423142&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT sahabasudeb catalyticreactors |