Electroanalysis in biomedical and pharmaceutical sciences: voltammetry, amperometry, biosensors, applications
Saved in:
| Format: | Book |
|---|---|
| Language: | English |
| Published: |
Berlin [u.a.]
Springer
2015
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| Series: | Monographs in electrochemistry
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| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Physical Description: | XIII, 350 S. Ill., graph. Darst. 235 mm x 155 mm, 0 g |
| ISBN: | 9783662471371 9783662471388 |
Staff View
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| 653 | |a Polarography | ||
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| 653 | |a Chronoamperometry | ||
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Record in the Search Index
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CONTENTS
1 INTRODUCTION 1
1.1 INTRODUCTION 1
REFERENCES 3
2 POLAROGRAPHY IN STUDIES OF PHARMACEUTICALS 7
2.1 PRINCIPLES OF POLAROGRAPHY 7
2.1.1 COMPARISON WITH VOLTAMMETRIC METHODS 22
2.2 VARIANTS OF POLAROGRAPHY 25
2.3 RECORD KEEPING 26
2.4 SUPPORTING ELECTROLYTES 27
2.5 THE HALF-WAVE POTENTIALS AND LIMITING CURRENTS 29
2.6 IDENTIFICATION OF THE TYPE OF THE LIMITING CURRENT 31
2.7 ROLE OF PH 33
2.8 INVESTIGATION OF A NEW COMPOUND 37
2.9 STRUCTURE OF ORGANIC COMPOUNDS AND POLAROGRAPHIC ACTIVITY . 39
2.10 CONCLUSION 41
REFERENCES 42
3 ELECTROANALYTICAL TECHNIQUES MOST FREQUENTLY USED IN DRUG
ANALYSIS 45
3.1 INTRODUCTION 45
3.2 LINEAR SWEEP AND CYCLIC VOLTAMMETRY 49
3.3 STEP AND PULSE VOLTAMMETRY 55
3.3.1 STAIRCASE VOLTAMMETRY 57
3.3.2 NORMAL PULSE VOLTAMMETRY 58
3.3.3 DIFFERENTIAL PULSE VOLTAMMETRY 59
3.3.4 SQUARE WAVE VOLTAMMETRY 62
3.4 ALTERNATING CURRENT VOLTAMMETRY 65
3.5 STRIPPING TECHNIQUES 67
3.5.1 ANODIC STRIPPING VOLTAMMETRY 69
3.5.2 CATHODIC STRIPPING VOLTAMMETRY 72
3.5.3 ADSORPTIVE STRIPPING VOLTAMMETRY 73
XI
HTTP://D-NB.INFO/1069299057
XII
CONTENTS
3.5.4 ABRASIVE STRIPPING VOLTAMMETRY 75
3.5.5 POTENTIOMETRIC STRIPPING ANALYSIS 76
3.6 CONCLUSIONS 77
REFERENCES 78
4 SOLID ELECTRODES IN DRUG ANALYSIS 83
4.1 INTRODUCTION 83
4.2 WHY SOLID ELECTRODE MATERIALS? 84
4.3 PROPERTIES OF SOLID ELECTRODE MATERIALS 85
4.4 SURFACE CLEANING PRE-TREATMENTS 87
4.5 SOLID ELECTRODE MATERIALS 88
4.5.1 METAL ELECTRODES 88
4.5.2 CARBON ELECTRODES 92
4.5.3 SCREEN-PRINTED ELECTRODES 108
4.5.4 CHEMICALLY MODIFIED ELECTRODES 110
4.6 CONCLUSION 114
REFERENCES 114
5 SCREEN-PRINTED ELECTRODES (SPE) FOR DRUG COMPOUNDS
DETERMINATION 119
5.1 INTRODUCTION 119
5.2 SPE PROPERTIES 120
5.3 SPE MODIFICATIONS 122
5.4 SPE APPLICATIONS (TABLE 5.1) 123
5.4.1 UNMODIFIED SPE 124
5.4.2 MODIFIED SPE SURFACE 129
5.5 SCREEN-PRINTED ELECTRODE AND ASCORBIC ACID DETERMINATION . . . 136
5.6 CONCLUSION 138
REFERENCES 138
6 ELECTROCHEMICAL BIOSENSORS FOR DRUG ANALYSIS 141
6.1 INTRODUCTION 144
6.2 IMMOBILIZATION TECHNIQUES 145
6.3 ELECTROCHEMICAL-BASED BIOSENSOR 151
6.3.1 AMPEROMETRY AND VOLTAMMETRY 151
6.3.2 POTENTIOMETRIC BIOSENSORS 175
6.3.3 IMPEDIMETRIC BIOSENSORS 180
REFERENCES 181
7 ELECTROCHEMICAL AND HYPHENATED ELECTROCHEMICAL DETECTORS
IN LIQUID CHROMATOGRAPHY AND FLOW INJECTION SYSTEMS FOR DRUG
COMPOUND ANALYSIS 187
7.1 INTRODUCTION 188
7.2 BASIC ANALYTICAL STRATEGY FOR IMPLEMENTING AN AMPEROMETRIC
DETECTOR UNDER HYDRODYNAMIC CONDITIONS 189
7.3 BASIC THEORETICAL ASPECTS [1, 52] 193
CONTENTS XIII
7.3.1 LC-AMPEROMETRIC DETECTION (LC-AD) 193
7.3.2 WALL-JET 194
7.3.3 THIN-LAYER 195
7.3.4 "COULOMETRIC" 195
7.4 LC-PULSED AMPEROMETRIC DETECTION (LC-PAD) [53, 54] 195
7.5 HYPHENATED TECHNIQUES FOR LC AND FIA 196
7.6 CONCLUSION 227
REFERENCES 227
8 ELECTROANALYTICAL METHOD VALIDATION IN PHARMACEUTICAL ANALYSIS
AND THEIR APPLICATIONS 235
8.1 METHOD VALIDATION IN DRUG ASSAY USING ELECTROANALYTICAL
TECHNIQUES 235
8.2 TYPES OF METHOD VALIDATION 237
8.3 ELECTROANALYTICAL METHOD VALIDATION CHARACTERISTICS AND THEIR
CALCULATIONS 242
8.3.1 VALIDATION CHARACTERISTICS 242
REFERENCES 263
9 APPLICATIONS FOR DRUG ASSAYS 267
9.1 INTRODUCTION 272
9.2 ASSAY OF DRUGS 272
9.3 EXAMPLES OF ELECTROCHEMICAL APPLICATION 276
9.3.1 CYCLIC, PULSED, AND STRIPPING VOLTAMMETRIC METHODS
USING SOLID ELECTRODES IN PHARMACEUTICAL ANALYSIS . 276
9.3.2 APPLICATIONS OF POLAROGRAPHY IN PHARMACEUTICAL
ANALYSIS 305
9.3.3 APPLICATIONS OF LC-EC DETECTION IN PHARMACEUTICAL
ANALYSIS 314
9.3.4 BIOSENSORS IN PHARMACEUTICAL ANALYSIS
(SEE ALSO CHAP. 6) 320
9.4 CONCLUSION 324
REFERENCES 325
ABOUT THE AUTHORS 337
ABOUT THE EDITOR 345
INDEX 347 |
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| physical | XIII, 350 S. Ill., graph. Darst. 235 mm x 155 mm, 0 g |
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| spelling | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications Sibel A. Ozkan ; Jean-Michel Kauffmann ; Petr Zuman Berlin [u.a.] Springer 2015 XIII, 350 S. Ill., graph. Darst. 235 mm x 155 mm, 0 g txt rdacontent n rdamedia nc rdacarrier Monographs in electrochemistry Arzneimittel (DE-588)4003115-9 gnd rswk-swf Elektroanalyse (DE-588)4014237-1 gnd rswk-swf Biomaterial (DE-588)4267769-5 gnd rswk-swf Research Pharmaceutical Analysis Voltammetry Polarography Chronopotentiometry Chronoamperometry Arzneimittel (DE-588)4003115-9 s Biomaterial (DE-588)4267769-5 s Elektroanalyse (DE-588)4014237-1 s DE-604 Ozkan, Sibel A. Sonstige oth Kauffmann, Jean-Michel Sonstige oth Zuman, Petr Sonstige oth Erscheint auch als Online-Ausgabe Ozkan, Sibel A. Electroanalysis in Biomedical and Pharmaceutical Sciences X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=5199112&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028259859&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications Arzneimittel (DE-588)4003115-9 gnd Elektroanalyse (DE-588)4014237-1 gnd Biomaterial (DE-588)4267769-5 gnd |
| subject_GND | (DE-588)4003115-9 (DE-588)4014237-1 (DE-588)4267769-5 |
| title | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications |
| title_auth | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications |
| title_exact_search | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications |
| title_full | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications Sibel A. Ozkan ; Jean-Michel Kauffmann ; Petr Zuman |
| title_fullStr | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications Sibel A. Ozkan ; Jean-Michel Kauffmann ; Petr Zuman |
| title_full_unstemmed | Electroanalysis in biomedical and pharmaceutical sciences voltammetry, amperometry, biosensors, applications Sibel A. Ozkan ; Jean-Michel Kauffmann ; Petr Zuman |
| title_short | Electroanalysis in biomedical and pharmaceutical sciences |
| title_sort | electroanalysis in biomedical and pharmaceutical sciences voltammetry amperometry biosensors applications |
| title_sub | voltammetry, amperometry, biosensors, applications |
| topic | Arzneimittel (DE-588)4003115-9 gnd Elektroanalyse (DE-588)4014237-1 gnd Biomaterial (DE-588)4267769-5 gnd |
| topic_facet | Arzneimittel Elektroanalyse Biomaterial |
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