Bioceramic coatings for medical implants: trends and techniques
Saved in:
| Main Authors: | , |
|---|---|
| Format: | Book |
| Language: | English |
| Published: |
Weinheim
Wiley-VCH-Verl.
2015
|
| Subjects: | |
| Online Access: | Inhaltstext Inhaltsverzeichnis |
| Item Description: | Literaturangaben |
| Physical Description: | XXII, 467 S. Ill., graph. Darst. |
| ISBN: | 9783527337439 3527337431 9783527684021 9783527684007 9783527684014 9783527682294 |
Staff View
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Record in the Search Index
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CONTENTS
PREFACE XI
GLOSSARY XVII
1 BIOCERAMICS - A HISTORICAL PERSPECTIVE 1
1.1 ALUMINA 1
1.2 ZIRCONIA 3
1.3 CALCIUM PHOSPHATES 4
REFERENCES 6
2 SOCIO-ECONOMIC ASPECTS AND SCOPE OF BIOCERAMIC MATERIALS AND
BIOMEDICAL IMPLANTS 11
2.1 TYPES OF BIOMATERIAL 11
2.2 THE GROWING GLOBAL AND REGIONAL MARKETS FOR BIOMEDICAL
IMPLANTS 14
2.2.1 A WORLDWIDE NEED FOR IMPLANTS 14
2.2.2 MARKET PROJECTIONS AND FORECASTS FOR BIOMATERIALS AND BIOMEDICAL
IMPLANTS 17
2.2.2.1 BIOMATERIALS 17
2.2.2.2 LARGE-JOINT RECONSTRUCTIVE IMPLANTS (HIP AND KNEE) 19
2.2.2.3 SMALL JOINTS AND EXTREMITIES IMPLANTS 20
2.2.2.4 SPINAL IMPLANTS 21
2.2.2.5 DENTAL IMPLANTS 21
2.3 ROLE OF BIOCERAMIC COATINGS IN ARTHROPLASTY 22
2.4 CERAMIC FEMORAL BALL HEADS 26
2.4.1 MECHANICAL AND FUNCTIONAL PROPERTIES 26
2.4.2 MANUFACTURING OF CERAMIC FEMORAL BALL HEADS 27
2.4.3 DISCOLOURATION OF ZIRCONIA BY IONISING RADIATION 30
REFERENCES 35
3 FUNDAMENTALS OF INTERACTION OF BIOCERAMICS AND LIVING MATTER 41
3.1 PRINCIPLE OF BIOCOMPATIBILITY 41
3.2 HIERARCHICAL STRUCTURE OF BONE AND TEETH 44
3.2.1 BONE STRUCTURE 44
HTTP://D-NB.INFO/1059940299
VII / CONTENTS
3.2.2 TOOTH STRUCTURE 47
3.3 BIOCERAMIC/BONE INTERFACE 49
3.3.1 ELASTICITY MISMATCH 49
3.3.2 INTERFACIAL LOOSENING SO
3.4 BASIC ASPECTS OF BIOMINERALISATION 52
3.5 INTERACTION AT A CELLULAR LEVEL S3
3.6 INTERACTION AT A TISSUE LEVEL 55
3.7 ADVANTAGES OF HYDROXYAPATITE AND BIOGLASS COATINGS 60
3.8 THE PROMISE OF CYTOKINES 62
REFERENCES 64
4 STRUCTURE AND PROPERTIES OF BIOCERAMICS USED IN ORTHOPAEDIC
AND DENTAL IMPLANTS 69
4.1 BIOINERT CERAMICS 69
4.1.1 ALUMINA 69
4.1.2 STABILISED ZIRCONIA 74
4.1.2.1 TRANSFORMATION TOUGHENING OF ZIRCONIA CERAMICS 75
4.1.2.2 MECHANICAL PROPERTIES OF ZIRCONIA 81
4.1.2.3 BIOCOMPATIBILITY AND HYDROLYTIC STABILITY OF ZIRCONIA 81
4.2 BIOACTIVE CERAMICS 83
4.2.1 SURFACE-ACTIVE BIOGLASSES 84
4.2.2 HYDROXYAPATITE 89
4.2.3 TRANSITION METAL-SUBSTITUTED CALCIUM ORTHOPHOSPHATES 95
4.2.4 RESORBABLE CALCIUM ORTHOPHOSPHATES 98
4.2.4.1 TRICALCIUM PHOSPHATES 99
4.2.4.2 TETRACALCIUM PHOSPHATE 102
4.2.4.3 CA-P0
4
SHEET STRUCTURES 103
4.2.4.4 HIGHLY SOLUBLE ALKALI-CONTAINING CALCIUM ORTHOPHOSPHATES 103
4.2.4.5 OTHER RESORBABLE BIOCERAMICS 104
REFERENCES 105
5 TECHNOLOGY OF COATING DEPOSITION 113
5.1 OVERVIEW 113
5.2 NON-THERMAL DEPOSITION METHODS 115
5.2.1 BIOMIMETIC ROUTE 115
5.2.1.1 GENERAL ASPECTS 115
5.2.1.2 CHEMISTRY OF BIOMIMETIC PRECIPITATION 117
5.2.1.3 BIOMIMETIC CALCIUM PHOSPHATE COATINGS DEPOSITED ON VARIOUS
SUBSTRATES 123
5.2.2 SOL-GEL DEPOSITION 132
5.2.2.1 TITANIA FILMS AND COATINGS 133
5.2.2.2 HYDROXYAPATITE 135
5.2.2.3 OTHER TYPES OF COATING 141
5.2.3 DIP AND SPIN COATING 143
5.2.3.1 DIP COATING 143
5.2.3.2 SPIN COATING 145
CONTENTS
| VII
5.2.4 ELECTROCHEMICAL DEPOSITION (ECD) 146
5.2.4.1 ELECTROCHEMICAL REACTIONS 147
5.2.4.2 ACID-BASE REACTIONS 147
5.2.4.3 PRECIPITATION REACTIONS 148
5.2.5 ELECTROPHORETIC DEPOSITION (EPD) 152
5.2.5.1 GENERAL ASPECTS 152
5.2.5.2 ELECTROPHORETIC DEPOSITION OF CALCIUM PHOSPHATE COATINGS 154
5.2.6 THERMAL SUBSTRATE DEPOSITION (HYDROPROCESSING) 158
5.2.7 HYDROTHERMAL COATING DEPOSITION 162
5.2.8 ELECTRON-AND ION BEAM-ASSISTED DEPOSITION (EB AD, IB AD) 163
5.2.9 RADIO FREQUENCY (R.F.) MAGNETRON SPUTTERING 167
5.3 THERMAL DEPOSITION METHODS 172
5.3.1 ATMOSPHERIC PLASMA SPRAYING (APS) 173
5.3.1.1 THE PHYSICS BEHIND THE PROCESS 173
5.3.1.2 MICRO-PLASMA SPRAYING (MPS) AND LOW ENERGY PLASMA
SPRAYING (LEPS) 179
5.3.2 LOW-PRESSURE (VACUUM) PLASMA SPRAYING (LPPS, VPS) 182
5.3.3 SUSPENSION PLASMA SPRAYING (SPS) 185
5.3.3.1 HYDROXYAPATITE COATINGS 188
5.3.3.2 TITANIUM OXIDE COATINGS 190
5.3.3.3 BIOGLASS COATINGS 191
5.3.3.4 OTHER TYPES OF COATING 192
5.3.4 HIGH VELOCITY SUSPENSION FLAME SPRAYING (HVSFS) 193
5.3.4.1 HYDROXYAPATITE COATINGS 194
5.3.4.2 TITANIUM OXIDE COATINGS 196
5.3.4.3 BIOGLASS COATINGS 197
5.3.4.4 OTHER COATINGS 199
5.3.5 SOLUTION PRECURSOR PLASMA SPRAYING (SPPS) 200
5.3.6 COLD GAS DYNAMIC SPRAYING (CGDS) 201
5.3.6.1 FUNDAMENTALS 201
5.3.6.2 BIOCERAMIC COATINGS 204
5.3.7 PLASMA ELECTROLYTIC OXIDATION (PEO) 209
5.3.7.1 MAGNESIUM SUBSTRATES 212
5.3.7.2 TITANIUM SUBSTRATES 214
5.3.8 PULSED LASER DEPOSITION (PLD) 219
5.4 OTHER TECHNIQUES 222
5.4.1 FLAME SPRAYING 222
5.4.1.1 OXYGEN/ACETYLENE FLAME SPRAYING 222
5.4.1.2 HIGH VELOCITY OXYFUEL SPRAYING (HVOF) 222
5.4.2 INDUCTIVELY COUPLED PLASMA SPRAYING (ICPS) 224
5.4.3 CHEMICAL VAPOUR DEPOSITION (CVD) 224
5.4.4 LASER ALLOYING 226
5.4.5 PHASE INVERSION TECHNIQUE 226
REFERENCES 227
VIIII
1 CONTENTS
6 DEPOSITION, STRUCTURE, PROPERTIES AND BIOLOGICAL FUNCTION
OF PLASMA-SPRAYED BIOCERAMIC COATINGS 253
6.1 GENERAL REQUIREMENTS AND PERFORMANCE PROFILE OF PLASMA-SPRAYED
BIOCERAMIC COATINGS 253
6.2 STRUCTURE AND BIOMEDICAL FUNCTIONS OF BIOCERAMIC COATINGS 258
6.2.1 HYDROXYAPATITE COATINGS 258
6.2.1.1 MICROSTRUCTURAL AND COMPOSITIONAL CHANGES DURING PLASMA
SPRAYING AND INCUBATION IN SBF 258
6.2.1.2 THERMAL DECOMPOSITION OF HYDROXYAPATITE DURING PLASMA
SPRAYING 263
6.2.1.3 PARAMETRIC STUDY OF THERMAL DECOMPOSITION OF
HYDROXYAPATITE 269
6.2.1.4 THE OXYAPATITE PROBLEM 272
6.2.1.5 BIOLOGICAL RESPONSES TO HYDROXYAPATITE COATINGS 275
6.2.2 COMPOSITE COATINGS 278
6.2.2.1 HYDROXYAPATITE/TITANIA COMPOSITE COATINGS 278
6.2.2.2 HYDROXYAPATITE/ZIRCONIA COMPOSITE COATINGS 278
6.2.2.3 HYDROXYAPATITE/ALUMINA/CARBON NANOTUBE COMPOSITE
COATINGS 280
6.2.3 BIPHASIC HYDROXYAPATITE/TRICALCIUM PHOSPHATE COATINGS 280
6.2.4 TRANSITION METAL-SUBSTITUTED CALCIUM ORTHOPHOSPHATE
COATINGS 281
6.2.4.1 COATING THICKNESS 281
6.2.4.2 COATING POROSITY 282
6.2.4.3 TENSILE ADHESION AND SHEAR STRENGTHS 283
6.3 THE ROLE OF BOND COATS 283
6.3.1 ENGINEERING THE SUBSTRATE-COATING INTERFACE 283
6.3.2 SELECTED BOND COATS 285
6.3.2.1 CALCIUM SILICATE BOND COATS 285
6.3.2.2 TITANIA BOND COATS 288
6.3.2.3 ZIRCONIA BOND COATS 292
6.3.2.4 MIXED ZIRCONIA/TITANIA BOND COATS 294
REFERENCES 298
7 CHARACTERISATION AND TESTING OF BIOCERAMIC COATINGS 309
7.1 PHASE COMPOSITION: X-RAY DIFFRACTION 310
7.1.1 FUNDAMENTALS 310
7.1.2 X-RAY DIFFRACTION OF PLASMA-SPRAYED HYDROXYAPATITE COATINGS 312
7.2 PHASE COMPOSITION: VIBRATIONAL (INFRARED AND RAMAN)
SPECTROSCOPY 314
7.2.1 FUNDAMENTALS 314
7.2.1.1 INFRARED SPECTROSCOPY 314
7.2.1.2 RAMAN SPECTROSCOPY 3JS
7.2.2 RAMAN MICROSCOPY OF BIOCERAMIC AND PHOTOACTIVE TITANIA
COATINGS 316
CONTENTS
IIX
7.2.3 INFRARED AND RAMAN SPECTRA OF HYDROXYAPATITE COATINGS 318
7.2.3.1 FOURIER TRANSFORM INFRARED (FTIR) SPECTROSCOPY 318
7.2.3.2 RAMAN SPECTROSCOPY 321
7.3 PHASE COMPOSITION: NUCLEAR MAGNETIC RESONANCE
SPECTROSCOPY 325
7.3.1 FUNDAMENTALS 325
7.3.2 NMR SPECTRA OF HYDROXYAPATITE COATINGS 326
7.4 PHASE COMPOSITION: CATHODOLUMINESCENCE 333
7.4.1 FUNDAMENTALS 333
7.4.2 CATHODOLUMINESCENCE MICROSCOPY OF PLASMA-SPRAYED
HYDROXYAPATITE COATINGS 334
7.5 ADHESION OF COATINGS TO THE SUBSTRATE 340
7.5.1 FUNDAMENTALS 340
7.5.1.1 TENSILE PULL TEST 342
7.5.1.2 MODIFIED PEEL TEST 343
7.5.1.3 SCRATCH TESTING 346
7.5.1.4 ULTRASONIC TESTING 349
7.5.2 ADHESION OF PLASMA-SPRAYED HYDROXYAPATITE COATINGS 351
7.5.2.1 MODIFIED PEEL TEST ACCORDING TO ASTM D3167-10 351
7.5.2.2 TENSILE TEST 353
7.5.2.3 SCRATCH TEST 354
7.5.2.4 LASER SHOCK ADHESION TEST (LASAT) 356
7.6 RESIDUAL COATING STRESSES 358
7.6.1 FUNDAMENTALS 358
7.6.2 X-RAY DIFFRACTION MEASUREMENTS (SIN
2
V-TECHNIQUE) 361
7.6.3 STRESS DETERMINATION BY CURVATURE MEASUREMENT
(ALMEN-TYPE TEST) 363
7.6.4 HOLE-DRILLING STRAIN GAUGE METHOD 365
7.6.5 PHOTOLUMINESCENCE PIEZOSPECTROSCOPY 367
7.6.6 RESIDUAL STRESSES IN PLASMA-SPRAYED HYDROXYAPATITE COATINGS 370
7.6.6.1 STRESS ANALYSIS BY X-RAY DIFFRACTION 370
7.6.6.2 STRESS ANALYSIS BY CURVATURE MEASUREMENT 374
7.6.6.3 STRESS ANALYSIS BY THE HOLE-DRILLING STRAIN GAUGE METHOD 376
7.6.6.4 STRESS ANALYSIS BY RAMAN PIEZOSPECTROSCOPY 377
7.7 FUNDAMENTALS OF ROUGHNESS AND POROSITY 377
7.8 MICROHARDNESS 382
7.8.1 FUNDAMENTALS 382
7.8.2 MICROHARDNESS OF HYDROXYAPATITE COATINGS 386
7.9 POTENTIODYNAMIC POLARISATION AND ELECTROCHEMICAL IMPEDANCE
SPECTROSCOPY (EIS) 387
7.9.1 FUNDAMENTALS 387
7.9.2 CORROSION PROTECTION OF METAL IMPLANTS THROUGH COATINGS 389
7.10 BIOLOGICAL PERFORMANCE TESTING OF BIOCERAMIC COATINGS 392
7.10.1 COMPOSITION OF SIMULATED BODY FLUIDS 393
7.10.2 INTERACTION OF SIMULATED BODY FLUIDS AND COATINGS 394
X | I CONTENTS
7.10.2.1 STRUCTURE AND TRANSFORMATION OF AMORPHOUS CALCIUM PHOSPHATE
(ACP) 395
7.10.2.2 EELS AND PIXE STUDIES 402
7.10.3 CELL PROLIFERATION AND VIABILITY TESTS 405
7.10.3.1 ALKALINE PHOSPHATASE (ALP) ACTIVITY 405
7.10.3.2 EXPRESSION OF NON-COLLAGENOUS PROTEINS 406
7.10.3.3 ALAMARBLUE AND MTT ASSAYS 409
7.10.3.4 FLUORESCENCE STAINING 411
7.10.4 IN VIVO TESTING OF BIOCERAMIC COATINGS USING ANIMAL MODELS 414
7.10.4.1 RAT MODEL 416
7.10.4.2 RABBIT MODEL 417
7.10.4.3 DOG MODEL 420
7.10.4.4 SHEEP MODEL 423
7.10.4.5 OTHER ANIMAL MODELS 429
REFERENCES 429
8 FUTURE DEVELOPMENTS AND OUTLOOK 445
REFERENCES 451
APPENDIX: RELEVANT SCIENTIFIC JOURNALS/BOOK SERIES WITH BIOCERAMIC
CONTENT 455
INDEX 459 |
| any_adam_object | 1 |
| author | Heimann, Robert B. 1938- Lehmann, Hans D. |
| author_GND | (DE-588)10837601X |
| author_facet | Heimann, Robert B. 1938- Lehmann, Hans D. |
| author_role | aut aut |
| author_sort | Heimann, Robert B. 1938- |
| author_variant | r b h rb rbh h d l hd hdl |
| building | Verbundindex |
| bvnumber | BV042591397 |
| classification_rvk | ZM 6290 ZM 7070 |
| ctrlnum | (OCoLC)908625484 (DE-599)DNB1059940299 |
| dewey-full | 617.693 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 617 - Surgery & related medical specialties |
| dewey-raw | 617.693 |
| dewey-search | 617.693 |
| dewey-sort | 3617.693 |
| dewey-tens | 610 - Medicine and health |
| discipline | Werkstoffwissenschaften / Fertigungstechnik Medizin |
| format | Book |
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| id | DE-604.BV042591397 |
| illustrated | Illustrated |
| indexdate | 2024-08-03T02:25:03Z |
| institution | BVB |
| isbn | 9783527337439 3527337431 9783527684021 9783527684007 9783527684014 9783527682294 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-028024616 |
| oclc_num | 908625484 |
| open_access_boolean | |
| owner | DE-83 DE-29 |
| owner_facet | DE-83 DE-29 |
| physical | XXII, 467 S. Ill., graph. Darst. |
| publishDate | 2015 |
| publishDateSearch | 2015 |
| publishDateSort | 2015 |
| publisher | Wiley-VCH-Verl. |
| record_format | marc |
| spelling | Heimann, Robert B. 1938- Verfasser (DE-588)10837601X aut Bioceramic coatings for medical implants trends and techniques Robert B. Heimann and Hans D. Lehmann Weinheim Wiley-VCH-Verl. 2015 XXII, 467 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Literaturangaben Calciumphosphatkeramik (DE-588)4140432-4 gnd rswk-swf Zahnimplantat (DE-588)4243751-9 gnd rswk-swf Biokeramik (DE-588)4371693-3 gnd rswk-swf Biokompatibilität (DE-588)4221531-6 gnd rswk-swf Beschichten (DE-588)4005996-0 gnd rswk-swf Biokeramik Biomaterial Implantat Nanomedizin TN000 Biokeramik (DE-588)4371693-3 s Calciumphosphatkeramik (DE-588)4140432-4 s Zahnimplantat (DE-588)4243751-9 s Beschichten (DE-588)4005996-0 s Biokompatibilität (DE-588)4221531-6 s DE-604 Lehmann, Hans D. Verfasser aut Erscheint auch als Online-Ausgabe Heimann, Robert B. Bioceramic Coatings for Medical Implants X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4809109&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028024616&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Heimann, Robert B. 1938- Lehmann, Hans D. Bioceramic coatings for medical implants trends and techniques Calciumphosphatkeramik (DE-588)4140432-4 gnd Zahnimplantat (DE-588)4243751-9 gnd Biokeramik (DE-588)4371693-3 gnd Biokompatibilität (DE-588)4221531-6 gnd Beschichten (DE-588)4005996-0 gnd |
| subject_GND | (DE-588)4140432-4 (DE-588)4243751-9 (DE-588)4371693-3 (DE-588)4221531-6 (DE-588)4005996-0 |
| title | Bioceramic coatings for medical implants trends and techniques |
| title_auth | Bioceramic coatings for medical implants trends and techniques |
| title_exact_search | Bioceramic coatings for medical implants trends and techniques |
| title_full | Bioceramic coatings for medical implants trends and techniques Robert B. Heimann and Hans D. Lehmann |
| title_fullStr | Bioceramic coatings for medical implants trends and techniques Robert B. Heimann and Hans D. Lehmann |
| title_full_unstemmed | Bioceramic coatings for medical implants trends and techniques Robert B. Heimann and Hans D. Lehmann |
| title_short | Bioceramic coatings for medical implants |
| title_sort | bioceramic coatings for medical implants trends and techniques |
| title_sub | trends and techniques |
| topic | Calciumphosphatkeramik (DE-588)4140432-4 gnd Zahnimplantat (DE-588)4243751-9 gnd Biokeramik (DE-588)4371693-3 gnd Biokompatibilität (DE-588)4221531-6 gnd Beschichten (DE-588)4005996-0 gnd |
| topic_facet | Calciumphosphatkeramik Zahnimplantat Biokeramik Biokompatibilität Beschichten |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4809109&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=028024616&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT heimannrobertb bioceramiccoatingsformedicalimplantstrendsandtechniques AT lehmannhansd bioceramiccoatingsformedicalimplantstrendsandtechniques |