X-ray crystallography:
Saved in:
| Previous Title: | Crystal structure determination |
|---|---|
| Main Author: | |
| Format: | Book |
| Language: | German |
| Published: |
Oxford
Oxford Univ. Press
2015
|
| Edition: | 2. ed. |
| Series: | Oxford chemistry primers
|
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | VIII, 114 S. Ill., graph. Darst. |
| ISBN: | 9780198700975 |
Staff View
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Record in the Search Index
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| adam_text | Contents
1 Fundamentals of X-ray crystallography 1
1.1 Introduction 1
1.2 Crystallography compared with other structural techniques 1
1.3 The eye and microscope analogy 4
1.4 Fundamentals of the crystalline state 7
1.5 Diffraction of X-rays by molecules and crystals 13
1.6 The geometry and symmetry of X-ray diffraction 18
1.7 The intensities of diffracted X-rays 24
1.8 Sources of X-rays 29
1.9 Summary 31
1.10 Exercises 31
2 X-ray crystallography in practice 33
2.1 Introduction 33
2.2 The preparation and selection of samples 33
2.3 Measuring diffraction patterns 35
2.4 Obtaining unit cell geometry and symmetry 38
2.5 The measurement of intensities 39
2.6 Data reduction 41
2.7 Solving the structure 42
2.8 Completing the basic structure 52
2.9 Refining the structure 54
2.10 Disorder, twinning, and the determination of absolute structure’ 57
2.11 Presenting and interpreting the results 62
2.12 Archiving and reporting crystal structures 64
2.13 Summary 67
2.14 Exercises 69
3 X-ray crystallography case studies 71
3.1 Introduction 71
3.2 Case study 1: a mercury thiolate complex 71
3.3 Case study 2: a solvated chiral rhodium complex 76
3.4 Case study 3: a microcrystalline chiral organic compound 80
3.5 Case study 4: a metal coordination chain polymer 84
3.6 Case study 5: a palladium complex of a bulky phosphine
for catalysis studies
88
ViÜ CONTENTS
3.7 Summary 90
3.8 Exercises 91
4 Related topics 93
4.1 Introduction 93
4.2 Single-crystal neutron diffraction 93
4.3 Diffraction by powder samples 96
4.4 Biological macromolecular crystallography 98
4.5 Crystal structure prediction 102
4.6 Summary 103
4.7 Exercises 104
Glossary 107
Further reading 112
Index 113
|
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| discipline | Chemie / Pharmazie Physik |
| edition | 2. ed. |
| format | Book |
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| id | DE-604.BV042560046 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T01:24:55Z |
| institution | BVB |
| isbn | 9780198700975 |
| language | German |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027993758 |
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| physical | VIII, 114 S. Ill., graph. Darst. |
| publishDate | 2015 |
| publishDateSearch | 2015 |
| publishDateSort | 2015 |
| publisher | Oxford Univ. Press |
| record_format | marc |
| series2 | Oxford chemistry primers |
| spelling | Clegg, William 1949- Verfasser (DE-588)1055809317 aut X-ray crystallography William Clegg 2. ed. Oxford Oxford Univ. Press 2015 VIII, 114 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Oxford chemistry primers Röntgenstrukturanalyse (DE-588)4137203-7 gnd rswk-swf Kristall (DE-588)4033209-3 gnd rswk-swf Röntgenkristallographie (DE-588)4178310-4 gnd rswk-swf Kristall (DE-588)4033209-3 s Röntgenstrukturanalyse (DE-588)4137203-7 s DE-604 Röntgenkristallographie (DE-588)4178310-4 s 1.Aufl. Crystal structure determination (DE-604)BV012460882 Digitalisierung UB Regensburg - ADAM Catalogue Enrichment application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027993758&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Clegg, William 1949- X-ray crystallography Röntgenstrukturanalyse (DE-588)4137203-7 gnd Kristall (DE-588)4033209-3 gnd Röntgenkristallographie (DE-588)4178310-4 gnd |
| subject_GND | (DE-588)4137203-7 (DE-588)4033209-3 (DE-588)4178310-4 |
| title | X-ray crystallography |
| title_auth | X-ray crystallography |
| title_exact_search | X-ray crystallography |
| title_full | X-ray crystallography William Clegg |
| title_fullStr | X-ray crystallography William Clegg |
| title_full_unstemmed | X-ray crystallography William Clegg |
| title_old | Crystal structure determination |
| title_short | X-ray crystallography |
| title_sort | x ray crystallography |
| topic | Röntgenstrukturanalyse (DE-588)4137203-7 gnd Kristall (DE-588)4033209-3 gnd Röntgenkristallographie (DE-588)4178310-4 gnd |
| topic_facet | Röntgenstrukturanalyse Kristall Röntgenkristallographie |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027993758&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT cleggwilliam xraycrystallography |