New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization:
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| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Aachen
Shaker
2014
|
| Series: | Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung
2014,2 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis Inhaltstext Inhaltsverzeichnis |
| Item Description: | Mit engl. und dt. Zsfassung |
| Physical Description: | XIX, 176 S. Ill., graph. Darst. |
| ISBN: | 9783844030044 |
Staff View
MARC
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| 245 | 1 | 0 | |a New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization |c Alireza Hosseini |
| 246 | 1 | 3 | |a New approaches in modeling and control of the PSD in emulsion polymerization |
| 264 | 1 | |a Aachen |b Shaker |c 2014 | |
| 300 | |a XIX, 176 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
| 490 | 1 | |a Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung |v 2014,2 | |
| 500 | |a Mit engl. und dt. Zsfassung | ||
| 502 | |a Zugl.: Dortmund, Techn. Univ., Diss., 2014 | ||
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Record in the Search Index
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CONTENTS
1 INTRODUCTION 1
1.1 OVERVIEW 1
1.2 INGREDIENTS AND THE PROCESS OF EMULSION POLYMERIZATION 2
1.3 PRODUCTION MODES 3
1.4 ADVANTAGES AND DISADVANTAGES OF EMULSION POLYMERIZATION 5
1.5 CONTROL OF THE PARTICLE SIZE DISTRIBUTION 5
1.6 DISSERTATION OUTLINE 6
2 EMULSION POLYMERIZATION MODEL 9
2.1 INTRODUCTION 9
2.2 EMULSION POLYMERIZATION THEORY 10
2.3 EMULSION POLYMERIZATION MODEL 11
2.3.1 KINETICS 11
2.3.2 REACTION RATE 13
2.3.3 MONOMER BALANCE 14
2.3.4 INITIATOR BALANCE 14
2.3.5 EMULSIFIER BALANCE 15
2.3.6 WATER FRACTION BALANCE 15
2.3.7 RADICALS IN THE WATER PHASE BALANCE 15
2.3.8 VOLUME BALANCE 17
2.3.9 HEAT BALANCE REACTOR SIDE 17
2.3.10 HEAT BALANCE JACKET SIDE 17
2.3.11 MONOMER CONCENTRATION IN THE DIFFERENT PHASES 17
VII
HTTP://D-NB.INFO/1054928444
VIII CONTENTS
2.4 LUMPED MODEL OF EMULSION POLYMERIZATION 20
2.5 CONCLUDING REMARKS 21
3 POPULATION BALANCE EQUATION AND THE NUMERICAL SOLUTION 23
3.1 DEVELOPING A POPULATION BALANCE EQUATION 23
3.1.1 PARTICLE STATE 24
3.1.2 REYNOLDS TRANSPORT THEOREM 25
3.1.3 DERIVATION OF THE POPULATION BALANCE EQUATION 26
3.2 THE POPULATION BALANCE EQUATION IN EMULSION POLYMERIZATION 27
3.2.1 ZERO-ONE MODEL 28
3.2.2 PSEUDO-BULK MODEL 32
3.2.3 AVERAGE NUMBER OF RADICALS PER PARTICLE 33
3.2.4 RADICALS ABSORPTION AND DESORPTION RATES (USED IN THE ZERO-ONE
MODEL) 33
3.2.5 RADICALS ABSORPTION AND DESORPTION RATES (USED IN THE PSEUDO-BULK
MODEL) 35
3.2.6 TERMINATION RATE CONSTANT AND GEL EFFECT 36
. 3.2.7 NUCLEATION RATE 36
3.2.8 GROWTH RATE 38
3.2.9 COAGULATION RATE 40
3.3 NUMERICAL SOLUTION 43
3.4 CONCLUDING REMARKS 49
4 EXPERIMENTAL VALIDATION 51
4.1 EXPERIMENTS 51
4.2 CHARACTERIZATION TECHNIQUES 54
4.2.1 SOLID CONTENT (CONVERSION) 54
4.2.2 PARTICLE SIZE DISTRIBUTION 54
4.3 MODEL PREDICTIONS AGAINST EXPERIMENTAL DATA 55
4.4 CONCLUDING REMARKS 61
CONTENTS IX
5 INVESTIGATION OF THE POTENTIAL SOURCES OF THE INADEQUACY OF THE PBE
MODEL FOR THE PREDICTION OF THE EXPERIMENTAL DATA 63
5.1 EXPERIMENTS-RELATED ERRORS 66
5.1.1 THE QUALITY OF THE PSD MEASUREMENT 66
5.1.2 COAGULATION AND NUCLEATION IN THE EXPERIMENTS 66
5.1.3 INSUFFICIENT MIXING 69
5.2 MODELING ERRORS AND UNCERTAIN PARAMETERS 70
5.2.1 IMPLEMENTATION OF THE MODEL 70
5.2.2 UNCERTAIN PARAMETERS 72
5.3 ANALYSIS OF THE GROWTH MODEL 78
5.4 STOCHASTIC BROADENING 79
5.5 CONCLUDING REMARKS 80
6 A NOVEL APPROACH TO OVERCOME THE DISCREPANCIES OF THE PBE MODELS FOR
THE PREDICTION OF THE EXPERIMENTAL RESULTS 81
6.1 INTRODUCTION 81
6.2 STOCHASTIC FORMULATION OF THE PARTICLE SIZE DISTRIBUTION 83
6.3 RESULTS AND DISCUSSION 87
6.3.1 MODEL VALIDATION 88
6.3.2 MODEL CONSISTENCY . 94
6.4 COMPARISON OF THE GROWTH KERNEL OF THE FPE MODEL WITH A
SEMI-CMPIRICAL
GROWTH KERNEL 101
6.5 CONCLUDING REMARKS 104
7 CONTROL OF THE PSD IN EMULSION POLYMERIZATION USING A MID-COURSE COR
RECTION CONTROL POLICY 107
7.1 INTRODUCTION 107
7.2 MID-COURSE CORRECTION CONTROL STRATEGY 109
7.2.1 OFFLINE OPTIMIZATION 110
7.2.2 STATE ESTIMATION 113
7.2.3 IMPLEMENTATION OF THE MID-COURSE CORRECTION 119
X
CONTENTS
7.2.4 HYBRID MODEL CONSIDERING THE PARAMETRIC PLANT-MODEL MISMATCH
(USING THE PSD IN THE FORMULATIONS) 119
7.2.5 RE-OPTIMIZATION TO COMPUTE THE MONOMER FLOW RATE TRAJECTORY FROM
THE MID-COURSE UNTIL THE END OF THE BATCH UNDER PARAMETRIC PLANT-
MODEL MISMATCH (CONSIDERING THE PSD IN FORMULATIONS) 123
7.2.6 HYBRID MODEL CONSIDERING THE PARAMETRIC PLANT-MODEL MISMATCH
(USING MOMENTS OF THE PSD IN THE FORMULATIONS) 126
7.2.7 RE-OPTIMIZATION TO COMPUTE THE MONOMER FLOW RATE TRAJECTORY FROM
THE MID-COURSE UNTIL THE END OF THE BATCH UNDER PARAMETRIC PLANT-
MODEL MISMATCH (CONSIDERING THE MOMENTS OF THE PSD IN FORMULA
TIONS) 126
7.2.8 HYBRID MODEL CONSIDERING THE STRUCTURAL PLANT-MODEL MISMATCH . .
131
7.2.9 RE-OPTIMIZATION TO COMPUTE THE MONOMER FLOW RATE TRAJECTORY FROM
THE MID-COURSE UNTIL THE END OF THE BATCH UNDER STRUCTURAL PLANT-
MODEL MISMATCH 132
7.3 CONCLUDING REMARKS 133
8 SUMMARY AND FUTURE PROSPECTS 135
8.1 SUMMARY 135
8.2 OUTLOOK 137
A PARTICLE SIZE DISTRIBUTION CONVERSION 139
B MOMENTS OF THE DISTRIBUTION 141
C ONLINE ESTIMATION OF THE DISPERSION COEFFICIENT 143
D EMPIRICAL MODEL 145
D.L RADIAL BASIS FUNCTION NETWORK (RBF) 145
D.L.L TRAINING OF THE RBF NETWORKS 146
D.2 PROJECTION TO LATENT STRUCTURE (PLS) 147
D.2.1 NONLINEAR ITERATIVE PARTIAL LEAST SQUARES (NIPALS) 149
D.3 PLS BASED RBF 149
D.3.1 TRAINING OF THE PLS BASED RBF 150
CONTENTS
XI
E K-MEANS CLUSTERING 153
F NOMENCLATURE 155 |
| any_adam_object | 1 |
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| ctrlnum | (OCoLC)888461874 (DE-599)DNB1054928444 |
| discipline | Werkstoffwissenschaften / Fertigungstechnik |
| format | Thesis Book |
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| id | DE-604.BV042288180 |
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| indexdate | 2024-09-10T01:34:19Z |
| institution | BVB |
| isbn | 9783844030044 |
| language | English |
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| physical | XIX, 176 S. Ill., graph. Darst. |
| publishDate | 2014 |
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| publisher | Shaker |
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| series | Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung |
| series2 | Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung |
| spelling | Hosseini, Alireza 1978- Verfasser (DE-588)1059873141 aut New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization Alireza Hosseini New approaches in modeling and control of the PSD in emulsion polymerization Aachen Shaker 2014 XIX, 176 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung 2014,2 Mit engl. und dt. Zsfassung Zugl.: Dortmund, Techn. Univ., Diss., 2014 Emulsionspolymerisation (DE-588)4121186-8 gnd rswk-swf Fed-batch-Verfahren (DE-588)4372478-4 gnd rswk-swf Prädiktive Regelung (DE-588)4271836-3 gnd rswk-swf Prozessmodell (DE-588)4237203-3 gnd rswk-swf Korngrößenverteilung (DE-588)4032495-3 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Emulsionspolymerisation (DE-588)4121186-8 s Fed-batch-Verfahren (DE-588)4372478-4 s Korngrößenverteilung (DE-588)4032495-3 s Prozessmodell (DE-588)4237203-3 s Prädiktive Regelung (DE-588)4271836-3 s DE-604 Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung 2014,2 (DE-604)BV035738045 2014,2 application/pdf http://d-nb.info/1054928444/04 Inhaltsverzeichnis text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4751341&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027725406&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Hosseini, Alireza 1978- New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization Schriftenreihe des Lehrstuhls für Systemdynamik und Prozessführung Emulsionspolymerisation (DE-588)4121186-8 gnd Fed-batch-Verfahren (DE-588)4372478-4 gnd Prädiktive Regelung (DE-588)4271836-3 gnd Prozessmodell (DE-588)4237203-3 gnd Korngrößenverteilung (DE-588)4032495-3 gnd |
| subject_GND | (DE-588)4121186-8 (DE-588)4372478-4 (DE-588)4271836-3 (DE-588)4237203-3 (DE-588)4032495-3 (DE-588)4113937-9 |
| title | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization |
| title_alt | New approaches in modeling and control of the PSD in emulsion polymerization |
| title_auth | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization |
| title_exact_search | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization |
| title_full | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization Alireza Hosseini |
| title_fullStr | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization Alireza Hosseini |
| title_full_unstemmed | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization Alireza Hosseini |
| title_short | New approaches in modeling and mid-course correction control of the particle size distribution in emulsion polymerization |
| title_sort | new approaches in modeling and mid course correction control of the particle size distribution in emulsion polymerization |
| topic | Emulsionspolymerisation (DE-588)4121186-8 gnd Fed-batch-Verfahren (DE-588)4372478-4 gnd Prädiktive Regelung (DE-588)4271836-3 gnd Prozessmodell (DE-588)4237203-3 gnd Korngrößenverteilung (DE-588)4032495-3 gnd |
| topic_facet | Emulsionspolymerisation Fed-batch-Verfahren Prädiktive Regelung Prozessmodell Korngrößenverteilung Hochschulschrift |
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| volume_link | (DE-604)BV035738045 |
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