Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Göttingen
Cuvillier
2014
|
| Edition: | 1. Aufl. |
| Series: | Schriftenreihe Keramische Werkstoffe
6 |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | 159 S. Ill., graph. Darst. |
| ISBN: | 9783954048496 |
Staff View
MARC
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| 100 | 1 | |a Flores, Octavio |d 1982- |e Verfasser |0 (DE-588)106266373X |4 aut | |
| 245 | 1 | 0 | |a Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes |c vorgelegt von Octavio-Jun Flores Urushima |
| 250 | |a 1. Aufl. | ||
| 264 | 1 | |a Göttingen |b Cuvillier |c 2014 | |
| 300 | |a 159 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
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| 490 | 1 | |a Schriftenreihe Keramische Werkstoffe |v 6 | |
| 502 | |a Zugl.: Bayreuth, Univ., Diss., 2014 | ||
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Record in the Search Index
| _version_ | 1804152730740064256 |
|---|---|
| adam_text | CONTENTS
1 INTRODUCTION 5
2 PROBLEM STATEMENTS 7
3 OBJECTIVE 9
4 LITERATURE REVIEW 12
4.1 PRECERAMIC POLYMERS 12
4.1.1 HISTORY OF PRECERAMIC POLYMERS 12
4.1.2 SYNTHESIS OF POIYSIIAZANES FOR PRECURSOR DERIVED CERAMICS (PDCS)
13
4.1.3 COPOLYMERIZATION TO POLYORGANOSILAZANES 16
4.1.4 CROSS-LINKING OF OLIGOSILAZANES TO MODIFIED POIYSIIAZANES 19
4.1.5 CONVERSION BEHAVIOUR OF POLYMER DERIVED CERAMICS (PDCS) 24
4.2 NON-OXIDE CERAMIC FIBRES 27
4.2.1 PROCESSING, STRUCTURE AND PROPERTIES OF NON-OXIDE CERAMIC FIBRES
27
4.2.2 CVD DERIVED SIC FIBRES 27
4.2.3 POLYMER DERIVED FIBRES 31
4.2.3.1 CERAMIC FIBRES BASED ON SIC SYSTEMS 31
4.2.3.2 CERAMIC FIBRES BASED ON SICN SYSTEMS. 43
5 EXPERIMENTAL PROCEDURE 49
5.1 CHEMICALS USED FOR THE SYNTHESIS OF
POIYSIIAZANES 49
5.2 SELECTIVE CHEMICAL CROSS-LINKING
OF LIQUID OLIGOSILAZANES TO TAILORED
MELTABLE POIYSIIAZANES 50
5.3 POLYMER CHARACTERIZATION 51
5.3.1 CHEMICAL ANALYSIS 51
5.3.2 THERMAL ANALYSIS 53
5.3.3 RHEOLOGY 54
5.4 CURING OF POLYMERS WITH ELECTRON
BEAM IRRADIATION 59
5.5 PROCESSING OF GREEN (POLYMER) FIBRES 60
5.6 CURING AND PYROLYSIS OF GREEN (POLYMER) FIBRES 61
5.7 MECHANICAL AND THERMAL PROPERTIES OF FIBRES 63
5.7.1 TENSILE TEST OF SINGLE FIBRES AT ROOM TEMPERATURE 63
HTTP://D-NB.INFO/1062736869
5.7.2 STATISTICAL ANALYSIS OF FIBRE TENSILE STRENGTH 64
5.7.3 BSR-TEST 65
5.7.4 OXIDATION BEHAVIOUR OF CERAMIC SICN FIBRES 66
6 RESULTS AND DISCUSSION 67
6.1 TAILORED MELTABLE POLYSILAZANES 67
6.2 THERMAL STABILITY AND VISCOELASTICITY OF POLYSILAZANES 74
6.2.1 THERMAL PROPERTIES 74
6.2.2 RHEOLOGICAL PROPERTIES 79
6.3 CURING BEHAVIOUR OF POLYSILAZANES IRRADIATED WITH ELECTRON
BEAM 94
6.4 MELT SPINNING PROCESS OF GREEN
(POLYMER) FIBRES 99
6.5 MECHANICAL STABILITY OF CURED GREEN (POLYMER)
FIBRES 102
6.6 PYROLYSIS OF CURED GREEN (POLYMER)
FIBRES 105
6.7 MECHANICAL AND THERMAL PROPERTIES
OF CERAMIC SICN FIBRES 108
6.7.1 TENSILE STRENGTH AT ROOM TEMPERATURE 109
6.7.2 CREEP RESISTANCE 115
6.7.3 OXIDATION BEHAVIOUR OF CERAMIC SICN FIBRES 120
7 CONCLUSIONS 125
8 ZUSAMMENFASSUNG 129
9 LIST OF ABBREVIATIONS AND SYMBOLS 133
10 REFERENCES 136
PUBLICATIONS 156
ACKNOWLEDGMENTS 157
CURRICULUM VITAE 159
|
| any_adam_object | 1 |
| author | Flores, Octavio 1982- |
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| bvnumber | BV042209565 |
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| classification_tum | WER 518d |
| ctrlnum | (OCoLC)897507841 (DE-599)BVBBV042209565 |
| dewey-full | 620 |
| dewey-hundreds | 600 - Technology (Applied sciences) |
| dewey-ones | 620 - Engineering and allied operations |
| dewey-raw | 620 |
| dewey-search | 620 |
| dewey-sort | 3620 |
| dewey-tens | 620 - Engineering and allied operations |
| discipline | Physik Werkstoffwissenschaften Werkstoffwissenschaften / Fertigungstechnik |
| edition | 1. Aufl. |
| format | Thesis Book |
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| genre | (DE-588)4113937-9 Hochschulschrift gnd-content |
| genre_facet | Hochschulschrift |
| id | DE-604.BV042209565 |
| illustrated | Illustrated |
| indexdate | 2024-07-10T01:15:22Z |
| institution | BVB |
| isbn | 9783954048496 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027648293 |
| oclc_num | 897507841 |
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| owner_facet | DE-703 DE-12 DE-634 DE-91 DE-BY-TUM DE-83 DE-29T |
| physical | 159 S. Ill., graph. Darst. |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | Cuvillier |
| record_format | marc |
| series | Schriftenreihe Keramische Werkstoffe |
| series2 | Schriftenreihe Keramische Werkstoffe |
| spelling | Flores, Octavio 1982- Verfasser (DE-588)106266373X aut Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes vorgelegt von Octavio-Jun Flores Urushima 1. Aufl. Göttingen Cuvillier 2014 159 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Schriftenreihe Keramische Werkstoffe 6 Zugl.: Bayreuth, Univ., Diss., 2014 Ausgangsmaterial (DE-588)4143518-7 gnd rswk-swf Siliciumcarbonitrid (DE-588)7737346-7 gnd rswk-swf Keramikfaser (DE-588)4163579-6 gnd rswk-swf Silazane (DE-588)4181301-7 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Keramikfaser (DE-588)4163579-6 s Siliciumcarbonitrid (DE-588)7737346-7 s Ausgangsmaterial (DE-588)4143518-7 s Silazane (DE-588)4181301-7 s DE-604 Erscheint auch als Online-Ausgabe 978-3-7369-4849-5 Schriftenreihe Keramische Werkstoffe 6 (DE-604)BV036058101 6 DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027648293&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Flores, Octavio 1982- Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes Schriftenreihe Keramische Werkstoffe Ausgangsmaterial (DE-588)4143518-7 gnd Siliciumcarbonitrid (DE-588)7737346-7 gnd Keramikfaser (DE-588)4163579-6 gnd Silazane (DE-588)4181301-7 gnd |
| subject_GND | (DE-588)4143518-7 (DE-588)7737346-7 (DE-588)4163579-6 (DE-588)4181301-7 (DE-588)4113937-9 |
| title | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes |
| title_auth | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes |
| title_exact_search | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes |
| title_full | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes vorgelegt von Octavio-Jun Flores Urushima |
| title_fullStr | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes vorgelegt von Octavio-Jun Flores Urushima |
| title_full_unstemmed | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes vorgelegt von Octavio-Jun Flores Urushima |
| title_short | Development of large diameter amorphous ceramic SiCN fibres from selective chemical cross-linked oligosilazanes |
| title_sort | development of large diameter amorphous ceramic sicn fibres from selective chemical cross linked oligosilazanes |
| topic | Ausgangsmaterial (DE-588)4143518-7 gnd Siliciumcarbonitrid (DE-588)7737346-7 gnd Keramikfaser (DE-588)4163579-6 gnd Silazane (DE-588)4181301-7 gnd |
| topic_facet | Ausgangsmaterial Siliciumcarbonitrid Keramikfaser Silazane Hochschulschrift |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027648293&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV036058101 |
| work_keys_str_mv | AT floresoctavio developmentoflargediameteramorphousceramicsicnfibresfromselectivechemicalcrosslinkedoligosilazanes |