The highly sterically demanding cpBIG:
Saved in:
| Main Author: | |
|---|---|
| Format: | Thesis Book |
| Language: | English |
| Published: |
Regensburg
Univ.-Verl.
2014
|
| Edition: | 1. Aufl. |
| Series: | Dissertationsreihe der Fakultät für Chemie und Pharmazie
2 |
| Subjects: | |
| Online Access: | Volltext https://nbn-resolving.org/urn:nbn:de:bvb:355-epub-304031 Inhaltsverzeichnis |
| Physical Description: | XIII, 271 S. graph. Darst. |
| ISBN: | 9783868451122 |
Staff View
MARC
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| 245 | 1 | 0 | |a The highly sterically demanding cpBIG |c Sebastian Heinl |
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| 264 | 1 | |a Regensburg |b Univ.-Verl. |c 2014 | |
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| 490 | 1 | |a Dissertationsreihe der Fakultät für Chemie und Pharmazie |v 2 | |
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Record in the Search Index
| _version_ | 1804152605472980992 |
|---|---|
| adam_text | TABLE OF CONTENTS IX
TABLE OF CONTENTS
1. INTRODUCTION 1
1.1 WHITE PHOSPHORUS, OTHER MAIN GROUP ELEMENTS AND CAGE COMPOUNDS 1
1.2 SUBSTITUENT-FREE P* LIGAND COMPLEXES 3
1.3 REACTIVITY OF P* LIGAND COMPLEXES 6
1.4 CP
R
LIGANDS
WITH HIGH STERIC DEMAND 9
1.5 REFERENCES 13
2. RESEARCH OBJECTIVES 17
3.THE HIGHLY STERICALLY DEMANDING CP
BIG
LIGAND 19
3.1 SOLUBILITY 19
3.2 GEOMETRICAL CONSIDERATIONS 20
3.3 THE CP
BIG
LIGAND
IN CRYSTAL STRUCTURES 21
3.4 REFERENCES 23
4. INTACT P
4
TETRAHEDRA AS TERMINAL AND BRIDGING LIGANDS IN
NEUTRAL COMPLEXES OF MANGANESE 24
4.1 INTRODUCTION 25
4.2 RESULTS AND DISCUSSION 26
4.3 EXPERIMENTAL PART 32
4.4 ADDITIONAL NOTES 34
4.5 REFERENCES 35
4.6 SUPPLEMENTARY INFORMATION 37
5. SYNTHESIS OF THE HETEROCUBANE CLUSTER [{CPMNMPA-PM AS A
STARTING MATERIAL FOR THE FORMATION OF POLYMERIC COORDINATION
COMPOUNDS 54
5.1 INTRODUCTION 55
5.2 RESULTS AND DISCUSSION 55
5.3 EXPERIMENTAL PART 60
HTTP://D-NB.INFO/1059717735
X TABLE OF CONTENTS
5.4 REFERENCES 64
5.5 SUPPLEMENTARY INFORMATION 66
6. SYNTHESIS AND CHARACTERIZATION OF MANGANESE TRIPLE-DECKER
COMPLEXES 84
6.1 INTRODUCTION 85
6.2 RESULTS AND DISCUSSION 86
6.3 EXPERIMENTAL PART 91
6.4 REFERENCES 93
6.5 SUPPLEMENTARY INFORMATION 94
7. ACTIVATION OF COORDINATED P4 TETRAHEDRA WITH 14 VALENCE
ELECTRON {CP CO} FRAGMENTS 104
7.1 INTRODUCTION 105
7.2 RESULTS AND DISCUSSION 106
7.3 EXPERIMENTAL PART 110
7.4 REFERENCES 112
7.5 SUPPLEMENTARY INFORMATION 114
8. LOW TEMPERATURE ACTIVATION OF SS,
SE
RE
D
AND A-TE WITH
[CP
B,G
FE(CO)
2
] RADICALS 120
8.1 INTRODUCTION 121
8.2 RESULTS AND DISCUSSION 121
8.3 EXPERIMENTAL PART 126
8.4 REFERENCES 129
8.5 SUPPLEMENTARY INFORMATION 131
9. ACTIVATION OF GROUP 15 BASED CAGE COMPOUNDS BY
[CP
BIG
FE(CO)
2
] RADICALS 143
9.1 INTRODUCTION 144
9.2 RESULTS AND DISCUSSION 145
TABLE OF CONTENTS XI
9.3 EXPERIMENTAL PART 149
9.4 REFERENCES 152
9.5 SUPPLEMENTARY INFORMATION 153
10. DIFFERENCES IN THE REACTION BEHAVIOUR OF THE BUTTERFLY
COMPLEXES [{CP
BIG
FE(CO)2 2(HFN
11
E4 ]
(E = P, AS) - IRRADIATION AND
THERMOLYSIS 161
10.1 INTRODUCTION 162
10.2 RESULTS AND DISCUSSION 162
10.3 EXPERIMENTAL PART 169
10.4 REFERENCES 171
10.5 SUPPLEMENTARY INFORMATION 172
11. SELECTIVE FUNCTIONALIZATION OF P4
BY METAL-MEDIATED C-P
BOND FORMATION 184
11.1 INTRODUCTION 185
11.2 RESULTS AND DISCUSSION 186
11.3 EXPERIMENTAL PART 193
11.4 REFERENCES 196
11.5 SUPPLEMENTARY INFORMATION 198
12. NOVEL POLYMERIC AGGREGATES OF
PENTAPHOSPHAFERROCENES AND MONOCATIONIC COINAGE METAL SALTS
- SYNTHESIS OF [{CP
BIG
FE(N
5
-P5)}AG]
N
[AL(OC(CF
3
)3)4
]N
AND [{CP*FE(N
5
-
PS)}{CU(GACL
4
)}2]N
204
12.1 INTRODUCTION 205
12.2 RESULTS AND DISCUSSION 205
12.3 EXPERIMENTAL PART 211
12.4 REFERENCES 213
12.5 SUPPLEMENTARY INFORMATION 215
XII TABLE OF CONTENTS
13. THE SUPERBULKY PENTAPHOSPHAFERROCENE [CP
BIG
FE(N
5
-PS)]
AS BUILDING BLOCK FOR THE FORMATION OF MACROMOLECULES WITH
LENS-SHAPED SCAFFOLDS 221
13.1 INTRODUCTION 222
13.2 RESULTS AND DISCUSSION 222
13.3 EXPERIMENTAL PART 226
13.4 REFERENCES 228
13.5 SUPPLEMENTARY INFORMATION 230
14. A GIANT SPHERICAL CLUSTER WITH
L-CUO
FULLERENE TOPOLOGY.. 237
14.1 INTRODUCTION 238
14.2 RESULTS AND DISCUSSION 239
14.3 EXPERIMENTAL PART 242
14.4 REFERENCES 244
14.5 SUPPLEMENTARY INFORMATION 246
15. CONCLUSION 252
15.1 SYNTHESIS OF P* LIGAND COMPLEXES OF MANGANESE 252
15.2 ACTIVATION OF SMALL MOLECULES WITH [CP
BIG
FE(CO
)
2
]2
AND {CP
BIG
} RADICALS 254
15.3 FORMATION OF SUPRAMOLECULAR ASSEMBLIES USING P* LIGAND COMPLEXES
AND COINAGE METAL SALTS 257
16. ZUSAMMENFASSUNG 259
16.1 DARSTELLUNG VON P*-LIGANDKOMPLEXEN DES MANGANS 259
16.2 AKTIVIERUNG KLEINER MOLEKIILE MIT [CP
BIG
FE(CO
)
2
]2
UND {CP
BIG
}* RADIKALEN 261
16.3 BILDUNG SUPRAMOLEKULARER AGGREGATE UNTER VERWENDUNG VON P*-
LIGANDKOMPLEXEN UND MIINZMETALLSALZEN 264
17. APPENDICES 267
17.1 ALPHABETIC LIST OF ABBREVIATIONS 267
17.2 LIST OF USED PROGRAMS 269
17.3 ADDRESSES OF COOPERATION PARTNERS 270
TABLE OF CONTENTS XIII
.4 ACKNOWLEDGMENTS 271
|
| any_adam_object | 1 |
| author | Heinl, Sebastian 1984- |
| author_GND | (DE-588)1059717689 |
| author_facet | Heinl, Sebastian 1984- |
| author_role | aut |
| author_sort | Heinl, Sebastian 1984- |
| author_variant | s h sh |
| building | Verbundindex |
| bvnumber | BV042127205 |
| classification_rvk | VH 5075 |
| collection | ebook |
| ctrlnum | (OCoLC)894911056 (DE-599)BVBBV042127205 |
| dewey-full | 541.2242 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 541 - Physical chemistry |
| dewey-raw | 541.2242 |
| dewey-search | 541.2242 |
| dewey-sort | 3541.2242 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie |
| edition | 1. Aufl. |
| format | Thesis Book |
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| id | DE-604.BV042127205 |
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| indexdate | 2024-07-10T01:13:22Z |
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| isbn | 9783868451122 |
| language | English |
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| physical | XIII, 271 S. graph. Darst. |
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| series | Dissertationsreihe der Fakultät für Chemie und Pharmazie |
| series2 | Dissertationsreihe der Fakultät für Chemie und Pharmazie |
| spelling | Heinl, Sebastian 1984- Verfasser (DE-588)1059717689 aut The highly sterically demanding cpBIG Sebastian Heinl 1. Aufl. Regensburg Univ.-Verl. 2014 XIII, 271 S. graph. Darst. txt rdacontent n rdamedia nc rdacarrier Dissertationsreihe der Fakultät für Chemie und Pharmazie 2 Zugl.: Regensburg, Univ., Diss., 2014 Cyclopentadienylgruppe (DE-588)4148584-1 gnd rswk-swf Chemische Reaktion (DE-588)4009853-9 gnd rswk-swf Sterische Hinderung (DE-588)4183133-0 gnd rswk-swf Übergangsmetallkomplexe (DE-588)4131837-7 gnd rswk-swf Weißer Phosphor (DE-588)4336318-0 gnd rswk-swf (DE-588)4113937-9 Hochschulschrift gnd-content Übergangsmetallkomplexe (DE-588)4131837-7 s Cyclopentadienylgruppe (DE-588)4148584-1 s Sterische Hinderung (DE-588)4183133-0 s Weißer Phosphor (DE-588)4336318-0 s Chemische Reaktion (DE-588)4009853-9 s DE-604 Erscheint auch als Online-Ausgabe urn:nbn:de:bvb:355-epub-304031 Dissertationsreihe der Fakultät für Chemie und Pharmazie 2 (DE-604)BV041882260 2 http://epub.uni-regensburg.de/30403/ Verlag kostenfrei Volltext https://nbn-resolving.org/urn:nbn:de:bvb:355-epub-304031 Resolving-System DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027567386&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Heinl, Sebastian 1984- The highly sterically demanding cpBIG Dissertationsreihe der Fakultät für Chemie und Pharmazie Cyclopentadienylgruppe (DE-588)4148584-1 gnd Chemische Reaktion (DE-588)4009853-9 gnd Sterische Hinderung (DE-588)4183133-0 gnd Übergangsmetallkomplexe (DE-588)4131837-7 gnd Weißer Phosphor (DE-588)4336318-0 gnd |
| subject_GND | (DE-588)4148584-1 (DE-588)4009853-9 (DE-588)4183133-0 (DE-588)4131837-7 (DE-588)4336318-0 (DE-588)4113937-9 |
| title | The highly sterically demanding cpBIG |
| title_auth | The highly sterically demanding cpBIG |
| title_exact_search | The highly sterically demanding cpBIG |
| title_full | The highly sterically demanding cpBIG Sebastian Heinl |
| title_fullStr | The highly sterically demanding cpBIG Sebastian Heinl |
| title_full_unstemmed | The highly sterically demanding cpBIG Sebastian Heinl |
| title_short | The highly sterically demanding cpBIG |
| title_sort | the highly sterically demanding cpbig |
| topic | Cyclopentadienylgruppe (DE-588)4148584-1 gnd Chemische Reaktion (DE-588)4009853-9 gnd Sterische Hinderung (DE-588)4183133-0 gnd Übergangsmetallkomplexe (DE-588)4131837-7 gnd Weißer Phosphor (DE-588)4336318-0 gnd |
| topic_facet | Cyclopentadienylgruppe Chemische Reaktion Sterische Hinderung Übergangsmetallkomplexe Weißer Phosphor Hochschulschrift |
| url | http://epub.uni-regensburg.de/30403/ https://nbn-resolving.org/urn:nbn:de:bvb:355-epub-304031 http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027567386&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| volume_link | (DE-604)BV041882260 |
| work_keys_str_mv | AT heinlsebastian thehighlystericallydemandingcpbig |