Analytical chemistry:
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| Main Authors: | , , |
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| Format: | Book |
| Language: | English |
| Published: |
Hoboken, NJ
Wiley
2014
|
| Edition: | 7. ed. |
| Subjects: | |
| Online Access: | Inhaltsverzeichnis |
| Physical Description: | XXII, 826 S. Ill., graph. Darst. |
| ISBN: | 9780470887578 |
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| 020 | |a 9780470887578 |9 978-0-470-88757-8 | ||
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| 100 | 1 | |a Christian, Gary D. |e Verfasser |0 (DE-588)133493083 |4 aut | |
| 245 | 1 | 0 | |a Analytical chemistry |c Gary D. Christian , Purnendu K. (Sandy) Dasgupta , Kevin A. Schug |
| 250 | |a 7. ed. | ||
| 264 | 1 | |a Hoboken, NJ |b Wiley |c 2014 | |
| 300 | |a XXII, 826 S. |b Ill., graph. Darst. | ||
| 336 | |b txt |2 rdacontent | ||
| 337 | |b n |2 rdamedia | ||
| 338 | |b nc |2 rdacarrier | ||
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| 700 | 1 | |a Dasgupta, Purnendu K. |e Verfasser |0 (DE-588)1028192460 |4 aut | |
| 700 | 1 | |a Schug, Kevin A. |e Verfasser |4 aut | |
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| adam_text |
Titel: Analytical chemistry
Autor: Christian, Gary D
Jahr: 2014
Contents
Chapter1
Rnalqtical Objectives. or: What Rnaliftitai
Chemists Do [
1.1 What Is Analytical Science?, 2
1.2 Qualitative and Quantitative Analysis:
What Does Each Teil Us?, 3
1.3 Getting Started: The Analytical Process, 6
1.4 Validation of a Method—You Have to
Prove It Works!, 15
1.5 Analyze Versus Determine—They Are
Different, 16
1.6 Some Useful Websites, 16
Chapter2
Basic Tools and Operations of Rnalqtical
Ctiemistni 20
2.1 The Laboratory Notebook—Your Critical
Record, 20
2.2 Laboratory Materials and Reagents, 23
2.3 The Analytical Balance—The
Indispensible Tool, 23
2.4 Volumetrie Glassware—Also Indispensible, 30
2.5 Preparation of Standard Base Solutions, 42
2.6 Preparation of Standard Acid Solutions, 42
2.7 Other Apparatus—Handling and Treating
Samples, 43
2.8 Igniting Precipitates—Gravimetrie Analysis, 48
2.9 Obtaining the Sample—Is It Solid, Liquid,
or Gas?, 49
2.10 Operations of Drying and Preparing a
Solution of the Analyte, 51
2.11 Laboratory Safety, 57
Chapter 3
Statistics and Data Handling in Bnalgtical
Chemistrg 62
3.1 Accuracy and Precision: There Is a
Difference, 62
3.2 Determinate Errors—They Are Systematic, 63
3.3 Indeterminate Errors—They Are Random, 64
3.4 Significant Figures: How Many Numbers
Do You Need?, 65
3.5 Rounding Off, 71
3.6 Ways of Expressing Accuracy, 71
3.7 Standard Deviation—The Most Important
Statistic, 72
3.8 Propagation of Errors—Not Just Additive, 75
3.9 Significant Figures and Propagation of Error, 81
3.10 Control Charts, 83
3.11 The Confidence Limit—How Sure Are You?. 84
3.12 Tests of Significance—Is There a
Difference?, 86
3.13 Rejection of a Result: The Q Test, 95
3.14 Statistics for Small Data Sets, 98
3.15 Linear Least Squares—How to Plot the
Right Straight Line, 99
3.16 Correlation Coefficient and Coefficient of
Determination, 104
3.17 Detection Limits—There Is No Such
Thing as Zero, 105
3.18 Statistics of Sampling—How Many
Samples, How Large?, 107
3.19 Powering a Study: Power Analysis. 110
3.20 Use of Spreadsheets in Analytical
Chemistry, 112
3.21 Using Spreadsheets for Plotting Calibration
Curves, 117
iii
iv
CONTENTS
3.22 Slope, Interccpt, and Coefficient of
Determination, 118
3.23 LINEST for Additional Statistics, 119
3.24 Statistics Software Packages, 120
ChapfeM
Good Lahofatorq Praclice: Ooaliti] flssurance and
Hetliod Validation 132
4.1 What Is Good Laboratory Practice?, 133
4.2 Validation oi'Analytical Methods, 134
4.3 Quality Assurance—Does the Method Still
Work?, 143
4.4 Laboratory Accreditation, 144
4.5 Electronic Records and Electronic
Signatures: 21 CFR, Part 11, 145
4.6 Some Official Organizations, 146
Chapter 5
Sfoichiometric Calculations: The Worhhorse of
the Rnalqst 143
5.1 Review of the Fundamentals, 149
5.2 How Do We Express Concentrations
of Solutions?, 152
5.3 Expressions of Analytical Results—So
Many Ways, 159
5.4 Volumetrie Analysis: Flow Do We Make
Stoichiometric Calculations?, 166
5.5 Volumetrie Calculations—Let's Use
Molarity, 169
5.6 Titer—How to Make Rapid Routine
Calculations, 179
5.7 Weight Relationships—You Need These
for Gravimetrie Calculations, 180
Chapter6
General Concepts of Chemical Equilihrium 188
6.1 Chemical Reactions: The Rate Concept, 188
6.2 Types of Equilibria, 190
6.3 Gibbs Free Energy and the Equilibrium
Constant, 191
6.4 Le Chätelier's Principle, 192
6.5 Temperature Effects on Equilibrium
Constants, 192
6.6 Pressure Effects on Equilibria, 192
6.7 Concentration Effects on Equilibria, 193
6.8 Catalysts, 193
6.9 Completeness of Reactions, 193
6.10 Equilibrium Constants for Dissociating or
Combining Species—Weak Electrolytes
and Precipitates, 194
6.11 Calculations Using Equilibrium
Constants—Composition at Equilibrium?, 195
6.12 The Common Ion Effect—Shilling the
Equilibrium, 203
6.13 Systematic Approach to Equilibrium
Calculations—How to Solve Any
Equilibrium Problem, 204
6.14 Some Hints for Applying the Systematic
Approach for Equilibrium Calculations, 208
6.15 Heterogeneous Equilibria—Solids Don't
Count, 211
6.16 Activity and Activity Coefficients—
Concentration Is Not the Whole Story, 211
6.17 The Diverse Ion Effect: The
Thermodynamic Equilibrium Constant and
Activity Coefficients, 217
Chapler 7
Heid—Base Equilibria 222
7.1 The Early History ofAcid—Base
Concepts, 222
7.2 Acid-Base Theories—Not All Are
Created Equal, 223
7.3 Acid-Base Equilibria in Water, 225
7.4 The pH Scale, 227
7.5 pH at Elevated Temperatures: Blood pH, 231
7.6 Weak Acids and Bases—What Is the pH?, 232
7.7 Salts of Weak Acids and Bases—They
Aren't Neutral, 234
7.8 Buffers—Keeping the pH Constant
(or Nearly So), 238
7.9 Polyprotic Acids and Their Salts, 245
7.10 Ladder Diagrams, 247
7.11 Fractions of Dissociating Species at a
Given pH: a Values—How Much of Each
Species?, 248
7.12 Salts of Polyprotic Acids—Acid, Base, or
Both?, 255
CONTENTS
v
7.13 Physiological Buffers—They Keep You
Alive, 261
7.14 Buffers for Biological and Clinical
Measurements, 263
7.15 Diverse Ion Effect on Acids and Bases: cKa
and'Xb—Salts Change the pH, 266
7.16 log C—pHDiagrams, 266
7.17 Exact pH Calculators, 269
Chapter8
Heid—Base Tilralions 281
8.1 Strong Acid versus Strong Base—The
Easy Titrations, 282
8.2 The Charge Balance Method—An Excel
Exercise for the Titration of a Strong Acid
and a Strong Base, 285
8.3 Detection of the End Point: Indicators, 288
8.4 Standard Acid and Base Solutions, 290
8.5 Weak Acid versus Strong Base—A Bit
Less Straightforward, 290
8.6 Weak Base versus Strong Acid, 295
8.7 Titration of Sodium Carbonate—A
Diprotic Base, 296
8.8 Using a Spreadsheet to Perform the
Sodium Carbonate—HCl Titration, 298
8.9 Titration of Polyprotic Acids, 300
8.10 Mixtures of Acids or Bases, 302
8.11 Equivalence Points from Derivatives of a
Titration Curve, 304
8.12 Titration of Amino Acids—They Are
Acids and Bases, 309
8.13 Kjeldahl Analysis: Protein Determination, 310
8.14 Titrations Without Measuring Volumes, 312
Chapter 9
Complexometric Beactions aad Tilralions 322
9.1 Complexes and Formation
Constants—How Stahle Are Complexes?, 322
9.2 Chelates: EDTA—The Ultimate Titrating
Agent for Metals, 325
9.3 Metal-EDTA Titration Curves, 331
9.4 Detection of the End Point:
Indicators—They Are Also Chelating
Agents, 334
9.5 Other Uses of Complexes, 336
9.6 Cumulative Formation Constants ß and
Concentrations of Specific Species in
Stepwise Formed Complexes, 336
Chapter10
Gravimetrie flnalqsis and Precipitation
Equilibria 342
10.1 How to Perform a Successful Gravimetrie
Analysis, 343
10.2 Gravimetrie Calculations—How Much
Analyte Is There?, 349
10.3 Examples of Gravimetrie Analysis, 353
10.4 Organic Precipitates, 353
10.5 Precipitation Equilibria: The Solubility
Product, 355
10.6 Diverse Ion Effect on Solubility: Ksp and
Activity Coefficients, 361
Chapter11
Precipitation Beactions and Titrations 3GG
11.1 Effect of Acidity on Solubility of
Precipitates: Conditional Solubility
Product, 366
11.2 Mass Balance Approach for Multiple
Equilibria, 368
11.3 Effect of Complexation on Solubility:
Conditional Solubility Product, 372
11.4 Precipitation Titrations, 374
Chapter12
Electrochemical Cetls and Electrode
Potentials 383
12.1 What Are Redox Reactions?, 384
12.2 Electrochemical Cells—What
Electroanalytical Chemists Use, 384
12.3 Nernst Equation—Effects of
Concentrations on Potentials, 390
12.4 Formal Potential—Use It for Defincd
Nonstandard Solution Conditions, 394
12.5 Limitations of Electrode Potentials, 395
vi
CONTENTS
Chapier13
Potentiometrie Electrodes and Potentiometri] 399
13.1 Metal Electrodes l'or Measuring
the Metal Cation, 400
13.2 Metal-Metal Salt Electrodes for
Measuring the Salt Anion, 401
13.3 Redox Electrodes—Inert Metals, 402
13.4 Voltaic Cells without Liquid
Junction—For Maximum Accuracy, 404
13.5 Voltaic Cells with Liquid Junction—The
Practical Kind, 405
13.6 Reference Electrodes: The Saturated
Calomel Electrode, 407
13.7 Measurement of Potential, 409
13.8 Determination of Concentrations from
Potential Measurements, 411
13.9 Residual Liquid-Junction Potential—It
Should Be Minimized, 411
13.10 Accuracy of Direct Potentiometrie
Measurements—Voltage Error versus
Activity Error, 412
13.11 Glass pH Electrode—Workhorse of
Chemists, 413
13.12 Standard Buffers—Reference for pH
Measurements, 418
13.13 Accuracy of pH Measurements, 420
13.14 Using the pH Meter—How Does It Work?, 421
13.15 pH Measurement of Blood—Temperature
Is Important, 422
13.16 pH Measurements in Nonaqueous Solvents, 423
13.17 Ion-Selective Electrodes, 424
13.18 Chemical Analysis on Mars using
Ion-Selective Electrodes, 432
Chapter14
HeJox and Potentiometrie Titraiions 437
14.1 First: Balance the Reduction-Oxidation
Reaction, 437
14.2 Calculation of the Equilibrium Constant of
a Reaction—Needed to Calculate
Equivalence Point Potentials, 438
14.3 Calculating Redox Titration Curves, 441
14.4 Visual Detection of the End Point, 445
14.5 Titrations Involving Iodine: Iodimetry and
Iodometry, 447
14.6 Titrations with Other Oxidizing Agents, 452
14.7 Titrations with Other Reducing Agents, 454
14.8 Preparing the Solution—Getting the
Analyte in the Right Oxidation State before
Titration, 454
14.9 Potentiometrie Titrations (Indirect
Potentiometry), 456
Chapter15
Voltammetfq and Electrochemical Sensors 466
15.1 Voltammetry, 467
15.2 Amperometric Electrodes—Measurement
of Oxygen, 472
15.3 Electrochemical Sensors: Chemically
Modified Electrodes, 472
15.4 Ultramicroelectrodes, 474
15.5 Microfabricated Electrochemical Sensors, 474
15.6 Micro and Ultramicroelectrode Arrays, 475
Chapter1B
Speclrochemical Hethods 477
16.1 Interaction of Electromagnetic Radiation
with Matter, 478
16.2 Electronic Spectra and Molecular Structure, 484
16.3 Infrared Absorption and Molecular
Structure, 489
16.4 Near-Infrared Spectrometry for
Nondestructive Testing, 491
16.5 Spectral Databases—Identifying
Unknowns, 493
16.6 Solvents for Spectrometry, 493
16.7 Quantitative Calculations, 494
16.8 Spectrometric Instrumentation, 504
16.9 Types of Instruments, 519
16.10 Array Spectrometers—Getting the Entire
Spectrum at Once, 522
16.11 Fourier Transform Infrared Spectrometers, 523
16.12 Near-IR Instruments, 525
16.13 Spectrometric Error in Measurements, 526
16.14 Deviation from Beer's Law, 527
16.15 Fluorometry, 530
16.16 Chemiluminescence, 538
16.17 Fiber-Optic Sensors, 540
CONTENTS
vii
Chapfer17
fltomic Spectrometric Mellrods S48
17.1 Principles: Distribution between Ground
and Excited States—Most Atoms Are in
the Ground State, 550
17.2 Flame Emission Spectrometry, 553
17.3 Atomic Absoiption Spectrometry, 556
17.4 Sample Preparation—Sometimes
Minimal, 567
17.5 Internal Standard and Standard Addition
Calibration, 567
17.6 Atomic Emission Spectrometry: The
Induction Coupled Plasma (ICP), 569
17.7 Atomic Fluorescence Spectrometry, 574
Chapler 20
Gas Chromatographg 619
20.1 Performing GC Separations, 620
20.2 Gas Chromatography Columns, 623
20.3 Gas Chromatography Detectors, 630
20.4 Temperature Selection, 638
20.5 Quantitative Measurements, 639
20.6 Headspace Analysis, 641
20.7 Thermal Desorption, 641
20.8 Purging and Trapping, 642
20.9 Small and Fast, 643
20.10 Separation of Chiral Compounds, 644
20.11 Two-Dimensional GC, 645
Chapler18
Sample Preparation: Solvent and Solid-Phase
Extraction 579
18.1 Distribution Coefficient, 579
18.2 Distribution Ratio, 580
18.3 Percent Extracted, 581
18.4 Solvent Extraction of Metals, 583
18.5 Accelerated and Microwave-Assisted
Extraction, 585
18.6 Solid-Phase Extraction, 586
18.7 Microextraction, 590
18.8 Solid-Phase Nanoextraction (SPNE), 593
Chapler19
Chramatograplni: Principles and Theorq 59G
19.1 Countercurrent Extraction: The
Predecessor to Modern Liquid
Chromatography, 598
19.2 Principles of Chromatographie
Separations, 603
19.3 Classification of Chromatographie
Techniques, 604
19.4 Theory of Column Efficiency in
Chromatography, 607
19.5 Chromatography Simulation
Software, 616
Chapler 21
Liquid Chromalographg and Electrophoresis 649
21.1 High-Performance Liquid Chromatography, 651
21.2 Stationary Phases in HPLC, 654
21.3 Equipment for HPLC, 665
21.4 Ion Chromatography, 692
21.5 HPLC Method Development, 700
21.6 UHPLC and Fast LC, 701
21.7 Open Tubulär Liquid Chromatography
(OTLC), 702
21.8 Thin-Layer Chromatography, 702
21.9 Electrophoresis, 708
21.10 Capillary Electrophoresi s, 711
21.11 Electrophoresis Related Techniques, 724
Chapler 22
Mass Speclromelrij 735
22.1 Principles of Mass Spectrometry, 735
22.2 Inlets and Ionization Sources, 740
22.3 Gas Chromatography-Mass Spectrometry, 741
22.4 Liquid Chromatography-Mass
Spectrometry, 746
22.5 Laser Desorption/Ionization. 750
22.6 Secondary Ion Mass Spectrometry. 752
22.7 Inductively Coupled Plasma-Mass
Spectrometry, 753
viii
CONTENTS
22.8 Mass Analyzcrs and Dctectors, 753
22.9 Hybrid Instruments and Tandem Mass
Speetrometry, 764
Chapter 23
Hinelic MelhoJs of Bnalqsis 7G9
23.1 Kinetics—The Basics, 769
23.2 Catalysis, 771
23.3 Enzyme Catalysis, 772
Chapter 24
Automation in Heasurements 784
24.1 Principles of Automation, 784
24.2 Automated Instruments: Process Control, 785
24.3 Automatic Instruments, 787
24.4 Flow Injection Analysis, 789
24.5 Sequential Injection Analysis, 791
24.6 Laboratory Information Management
Systems, 792
Mable on rexlbooh Website: www.wileii.com/college/cbrisNan
Chapter 25
Clinical Ctiemistfi] C1
25.1 Composition of Blood, C1
25.2 Collection and Preservation of Samples, C3
25.3 Clinical Analysis—Common
Determinations, C4
25.4 Immunoassay, C6
Mable on rexrbooH Website: www.wileg.com/college/cbrisNon
Chapter 25
Environmental Samplina and Analysis Ejjl
26.1 Getting a Meaningful Sample, ENI
26.2 Air Sample Collection and Analysis, EN2
26.3 Water Sample Collection and Analysis, EN9
26.4 Soil and Sediment Sampling, ENI 1
26.5 Sample Preparation for Trace Organics, EN 12
26.6 Contaminated Land Sites—What Needs to
Be Analyzed?, EN 12
26.7 EPA Methods and Performance-Based
Analyses, EN 13
Mable on rextbooh Website: www.wileg.com/college/cbristian
Chapter 6
Century offhe Gene—Genomicsand
Protenmics: 088 Sequencinp and Protein Profiling El
G.l Of What Are We Made?, Gl
G.2 What Is DNA?, G3
G.3 Human Genome Project, G3
G.4 How Are Genes Sequenced?, G5
G.5 Replicating DNA: The Polymerase Chain
Reaction, G6
G.6 Plasmids and Bacterial Artificial
Chromosomes (BACs), G7
G.7 DNA Sequencing, G8
G.8 Whole Genome Shotgun Sequencing, Gll
G.9 Single-Nucleotide Polymorphisms, Gll
G.10 DNA Chips, G12
G.ll Draft Genome, Gl3
G. 12 Genomes and Proteomics: The Rest of the
Story, Gl3
APPENDIX fl LITERATURE ÖF RNRLVTICHL
CHEMISTRV 794
APPENDIX B REVIEW OF MRTHEMRTICRL OPERATIONS:
EXPONENTS, LOGRRITHMS, ÄND THE pURDRRTIC
FORHÜLR 797
APPENDIX C TABLES OF CDNSTANTS 801
Table C.l Dissociation Constants for Acids, 801
Table C.2a Dissociation Constants for Basic
Species, 802
Table C.2b Acid Dissociation Constants for
Basic Species, 803
Table C.3 Solubility Product Constants, 803
Table C.4 Formation Constants for Some
EDTA Metal Chelates, 805
Table C.5 Some Standard and Formal
Reduction Electrode Potentials, 806
flvailable on textbooh Website: www.wileg.com/college/cbristian
APPENDIX 0 SAFETV IN THE LABQRATQAV S1
CONTENTS
ix
Rvailable on rexrbooh Website: iiiiiitii.iiiileij.com/collese/ctiristion
fiPPENDIX E PERIODIC THBLES ON THE WEB PI
HPPENDIXFflNSWERS TO PROBLEMS
(Malte on textbooh Website: www.wiles.com/college/christian
Experiments
El
Use offipparatüs
Experiment 1 Use ofthe Analytical Balance, El
Experiment 2 Use of the Pipet and Buret and
Statistical Analysis, E2
Experiment 3 Analysis of Volumetrie
Measurements Using
Spectrophotometric Microplate
Readers and Spreadsheet
Calculations, E4
Gfavimetri]
Experiment 4 Gravimetrie Determination of
Chloride, E6
Experiment 5 Gravimetrie Determination of SO3
in a Soluble Sulfate, E9
Experiment 6 Gravimetrie Determination of
Nickel in a Nichrome Alloy, El 1
Rcid-Base Titrations
Experiment 7 Determination of Replaceable
Hydrogen in Acid by Titration
with Sodium Hydroxide, El 2
Experiment 8 Determination of Total Alkalinity
ofSodaAsh, E14
Experiment 9 Determination of Aspirin Using
Back Titration, El6
Experiment 10 Determination of Hydrogen
Carbonate in Blood Using
Back-Titration, El 8
Complexometric Titration
Experiment 11 Determination of Water Hardness
withEDTA, El 9
Precipitation Titrations
Experiment 12 Determination of Silver in an
Alloy: Volhard's Method, E21
Experiment 13 Determination of Chloride in a
Soluble Chloride: Fajans' Method. E23
Potentiometrie Measurements
Experiment 14 Determination of the pH of Hair
Shampoos, E24
Experiment 15 Potentiometrie Determination of
Fluoride in Drinking Water Using
a Fluoride Ion-Selective Electrode, E25
Reduction—Qxidation Titrations
Experiment 16 Analysis of an Iron Alloy or Ore
by Titration with Potassium
Dichromate, E27
Experiment 17 Analysis of Commercial
Hypochlorite or Peroxide Solution
by Iodometric Titration, E30
Experiment 18 Iodometric Determination of
Copper, E32
Experiment 19 Determination of Antimony by
Titration with Iodine, E34
Experiment 20 Microscale Quantitative Analysis
of Hard-Water Samples Using an
Indirect Potassium Permanganate
Redox Titration, E36
Potentiometrie Titrations
Experiment 21 pH Titration of Unknown Soda
Ash, E38
Experiment 22 Potentiometrie Titration of a
Mixture of Chloride and Iodide, E40
Spectrocfiemicol Measurements
Experiment 23 Spectrophotometric Determination
of Iron, E41
Experiment 24 Spectrophotometric Determination
of Iron in Vitamin Tablets Using a
96 Well Plate Reader, E43
Experiment 25 Determination of Nitrate Nitrogen
in Water, E46
Experiment 26 Spectrophotometric Determination
of Lead on Leaves Using Solvent
Extraction, E47
Experiment 27 Spectrophotometric Determination
of Inorganic Phosphorus in Serum, E48
Experiment 28 Spectrophotometric Determination
of Manganese and Chromium in
Mixture. E50
X
CONTENTS
Experiment 29 Spectrophotometric Determination
of Manganese in Steel Using a 96
Well Plate Reader, E52
Experiment 30 Ultraviolet Spectrophotometric
Determination of Aspirin,
Phenacetin, and Caffeine in APC
Tablets Using Solvent Extraction, E54
Experiment 31 Infrared Determination of a
Mixture of Xylene Isomers, E56
Experiment 32 Fluorometric Determination of
Riboflavin (Vitamin EU), E57
fliomic Bpectromefry Measuremen^s
Experiment 33 Determination of Calcium by
Atomic Absorption
Spectrophotometry, E57
Experiment 34 Flame Emission Spectrometric
Determination of Sodium, E60
Solid-Ptiase Extraction and Ctiromatographii
Experiment 35 Solid-Phase Extraction with
Preconcentration, Elution, and
Spectrophotometric Analysis, E61
Experiment 36 Thin-Layer Chromatography
Separation of Amino Acids, E67
Experiment 37 Gas Chromatographie Analysis of
a Tertiary Mixture, E69
Experiment 38 Qualitative and Quantitative
Analysis of Fruit Juices for
Vitamin C Using
High-Performance Liquid
Chromatography, E70
Experiment 39 Analysis of Analgesics Using
High-Performance Liquid
Chromatography, E71
Mass Spectiometrij
Experiment 40 Capillary Gas
Chrom atography-Mas s
Spectrometry, E72
Hinetic flnalqsis
Experiment 41 Enzymatic Determination of
Glucose in Blood, E74
FSouj Iniechon flnalqsis
Experiment 42 Characterization of Physical
Parameters of a Flow Injection
Analysis System, E76
Experiment 43 Single-Line FIA:
Spectrophotometric Determination
of Chloride, E79
Experiment 44 Three-Line FIA:
Spectrophotometric Determination
of Phosphate, ESO
Team Experiments
Experiment 45 Method Validation and Quality
Control Study, E82
Experiment 46 Proficiency Testing:
Determination of z Values of
Class Experiments, E84
Index 815 |
| any_adam_object | 1 |
| author | Christian, Gary D. Dasgupta, Purnendu K. Schug, Kevin A. |
| author_GND | (DE-588)133493083 (DE-588)1028192460 |
| author_facet | Christian, Gary D. Dasgupta, Purnendu K. Schug, Kevin A. |
| author_role | aut aut aut |
| author_sort | Christian, Gary D. |
| author_variant | g d c gd gdc p k d pk pkd k a s ka kas |
| building | Verbundindex |
| bvnumber | BV041950776 |
| callnumber-first | Q - Science |
| callnumber-label | QD101 |
| callnumber-raw | QD101.2 |
| callnumber-search | QD101.2 |
| callnumber-sort | QD 3101.2 |
| callnumber-subject | QD - Chemistry |
| classification_rvk | VG 5010 |
| classification_tum | CHE 200f |
| ctrlnum | (OCoLC)882935693 (DE-599)OBVAC11161544 |
| dewey-full | 543 |
| dewey-hundreds | 500 - Natural sciences and mathematics |
| dewey-ones | 543 - Analytical chemistry |
| dewey-raw | 543 |
| dewey-search | 543 |
| dewey-sort | 3543 |
| dewey-tens | 540 - Chemistry and allied sciences |
| discipline | Chemie / Pharmazie Chemie |
| edition | 7. ed. |
| format | Book |
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| genre | 1\p (DE-588)4123623-3 Lehrbuch gnd-content |
| genre_facet | Lehrbuch |
| id | DE-604.BV041950776 |
| illustrated | Illustrated |
| indexdate | 2025-03-24T15:01:22Z |
| institution | BVB |
| isbn | 9780470887578 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027393745 |
| oclc_num | 882935693 |
| open_access_boolean | |
| owner | DE-19 DE-BY-UBM DE-91G DE-BY-TUM |
| owner_facet | DE-19 DE-BY-UBM DE-91G DE-BY-TUM |
| physical | XXII, 826 S. Ill., graph. Darst. |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | Wiley |
| record_format | marc |
| spelling | Christian, Gary D. Verfasser (DE-588)133493083 aut Analytical chemistry Gary D. Christian , Purnendu K. (Sandy) Dasgupta , Kevin A. Schug 7. ed. Hoboken, NJ Wiley 2014 XXII, 826 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Analytische Chemie (DE-588)4129906-1 gnd rswk-swf Chemische Analyse (DE-588)4009840-0 gnd rswk-swf Chemistry, analytic Quantitative Textbooks 1\p (DE-588)4123623-3 Lehrbuch gnd-content Analytische Chemie (DE-588)4129906-1 s DE-604 Chemische Analyse (DE-588)4009840-0 s 2\p DE-604 Dasgupta, Purnendu K. Verfasser (DE-588)1028192460 aut Schug, Kevin A. Verfasser aut HBZ Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027393745&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis 1\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk 2\p cgwrk 20201028 DE-101 https://d-nb.info/provenance/plan#cgwrk |
| spellingShingle | Christian, Gary D. Dasgupta, Purnendu K. Schug, Kevin A. Analytical chemistry Analytische Chemie (DE-588)4129906-1 gnd Chemische Analyse (DE-588)4009840-0 gnd |
| subject_GND | (DE-588)4129906-1 (DE-588)4009840-0 (DE-588)4123623-3 |
| title | Analytical chemistry |
| title_auth | Analytical chemistry |
| title_exact_search | Analytical chemistry |
| title_full | Analytical chemistry Gary D. Christian , Purnendu K. (Sandy) Dasgupta , Kevin A. Schug |
| title_fullStr | Analytical chemistry Gary D. Christian , Purnendu K. (Sandy) Dasgupta , Kevin A. Schug |
| title_full_unstemmed | Analytical chemistry Gary D. Christian , Purnendu K. (Sandy) Dasgupta , Kevin A. Schug |
| title_short | Analytical chemistry |
| title_sort | analytical chemistry |
| topic | Analytische Chemie (DE-588)4129906-1 gnd Chemische Analyse (DE-588)4009840-0 gnd |
| topic_facet | Analytische Chemie Chemische Analyse Lehrbuch |
| url | http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027393745&sequence=000002&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
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