Non-noble metal fuel cell catalysts:
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| Format: | Buch |
| Sprache: | English |
| Veröffentlicht: |
Weinheim
Wiley-VCH
2014
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| Online-Zugang: | Inhaltstext Inhaltsverzeichnis |
| Beschreibung: | XVIII, 428 S. Ill., graph. Darst. |
| ISBN: | 352733324X 9783527333240 9783527664917 9783527664924 9783527664931 |
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| 245 | 1 | 0 | |a Non-noble metal fuel cell catalysts |c ed. by Zhongwei Chen ... |
| 264 | 1 | |a Weinheim |b Wiley-VCH |c 2014 | |
| 300 | |a XVIII, 428 S. |b Ill., graph. Darst. | ||
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CONTENTS
PREFACE XIII
LIST OF CONTRIBUTORS XV
1 ELECTROCATALYSTS FOR ACID PROTON EXCHANGE MEMBRANE (PEM) FUEL
CELLS - AN OVERVIEW 1
MICHAEL BRON
1.1 INTRODUCTION 1
1.2 ACID PEM FUEL CELL BACKGROUND AND FUNDAMENTALS 2
1.2.1 ACID PEM FUEL CELL OVERVIEW - HISTORY, STATUS, AND ADVANTAGES 2
1.2.2 ACID PEM FUEL CELL REACTIONS - THERMODYNAMICS AND KINETICS 4
1.3 ACID PEM FUEL CELL CATALYSIS FOR CATHODE 0
2
REDUCTION REACTION 9
1.3.1 ELECTROCHEMICAL THERMODYNAMICS OF 0
2
REDUCTION REACTION 10
1.3.2 PT-BASED CATALYSTS FOR THE OXYGEN REDUCTION REACTION 10
1.3.3 ELECTROCHEMICAL KINETICS AND MECHANISM OF THE 0
2
REDUCTION
REACTION CATALYZED BY PT CATALYSTS 16
1.4 CATALYST CHALLENGES AND PERSPECTIVE IN ACID PEM FUEL CELLS 18
1.4.1 PT CATALYST COST ANALYSIS AND MAJOR CHALLENGES 18
1.4.2 SUSTAINABILITY 19
1.4.3 MAJOR TECHNICAL CHALLENGES FOR NON-NOBLE METAL CATALYSTS AND
MITIGATION STRATEGIES 19
1.4.4 NON-NOBLE METAL CATALYST OVERVIEW 20
1.5 CONCLUSION 22
REFERENCES 22
2 HEAT-TREATED TRANSITION METAL-N
X
C
Y
ELECTROCATALYSTS FOR THE
0
2
REDUCTION REACTION IN ACID PEM
FUEL CELLS 29
FR6D6RIC JAOUEN
2.1 INTRODUCTION 29
2.1.1 WHY THE SEARCH FOR NON-PRECIOUS METAL CATALYSTS FOR
0
2
REDUCTION? 29
2.1.2 ACTIVITY, POWER PERFORMANCE, AND DURABILITY CONSTRAINTS ON ME/N/C
CATALYSTS 33
2.1.3 MILESTONES ACHIEVED BY ME/N/C CATALYSTS OVER THE LAST 50 YEARS 37
HTTP://D-NB.INFO/1043456538
VI | CONTENTS
2.1.3.1 MILESTONE 1 37
2.1.3.2 MILESTONE 2 38
2.1.3.3 MILESTONE 3 39
2.1.3.4 MILESTONE 4 39
2.1.3.5 MILESTONE 5 39
2.2 SYNTHESIS APPROACHES FOR HEAT-TREATED ME/N/C CATALYSTS 40
2.2.1 THE SUPPORTED-MACROCYCLE APPROACH 41
2.2.2 THE TEMPLATING METHOD 42
2.2.3 THE FOAMING AGENT APPROACH 43
2.2.4 THE N MOLECULE OR METAL-LIGAND APPROACH 45
2.2.5 THE N-POLYMER APPROACH 48
2.2.6 GASEOUS N-PRECURSOR APPROACH (NH
3
AND CH
3
CN) 50
2.2.7 THERMALLY DECOMPOSABLE METAL-ORGANIC
FRAMEWORKS (MOF) 52
2.3 IMPORTANT PARAMETERS FOR HIGHLY ACTIVE ME/N/C
CATALYSTS 54
2.3.1 PYROLYSIS TEMPERATURE 54
2.3.1.1 METAL MACROCYDES SUPPORTED ON CARBON AND PYROLYZED IN INERT
ATMOSPHERE 54
2.3.1.2 SEPARATE METAL AND NITROGEN PRECURSORS OR METAL-LIGAND COMPLEXES
IMPREGNATED ON A CARBON SUPPORT AND PYROLYZED IN INERT OR REACTIVE
ATMOSPHERE
56
2.3.2 THE TRANSITION METAL 57
2.3.2.1 BINARY METAL CATALYSTS 58
2.3.2.2 METAL CONCENTRATION 59
2.3.3 THE NITROGEN CONTENT AND SPECIATION BY X-RAY PHOTOELECTRON
SPECTROSCOPY (XPS) 61
2.3.4 THE CARBON SUPPORT/HOST 64
2.4 NATURE OF THE ACTIVE SITES 73
2.4.1 TIME-OF-FLIGHT SECONDARY ION MASS SPECTROSCOPY 73
2.4.2 X-RAY ABSORPTION SPECTROSCOPY AND EXTENDED X-RAY ABSORPTION FINE
STRUCTURE 75
2.4.2.1 STUDIES ON PYROLYZED MACROCYCLES 76
2.4.2.2 STUDIES ON CATALYSTS SYNTHESIZED FROM SEPARATE METAL, N AND C
PRECURSORS 77
2.4.3 MOSSBAUER SPECTROSCOPY 79
2.4.3.1 STUDIES ON FEPC AND FE- PORPHYRIN, UNPYROLYZED OR PYROLYZED AT
T 500 C 80
2.4.3.2 STUDIES ON FE MACROCYCLES PYROLYZED AT T 700 C 81
2.4.3.3 STUDIES ON FE-N-C CATALYSTS OBTAINED BY PYROLYSIS OF SEPARATE
FE, N,
AND C PRECURSORS 85
2.4.4 TURNOVER FREQUENCY AND SITE DENSITY 91
2.5 ELECTROCHEMICAL INVESTIGATION BY RDE/RRDE METHODS 94
2.5.1 RDE AND THE THIN FILM PROBLEM: MODEL AND EXPERIMENT 94
CONTENTS I VII
2.5.2 ACTIVITY FOR H
2
0
2
REDUCTION OR OXIDATION: A MAJOR DIFFERENCE FROM
PT-BASED CATALYSTS 99
2.5.3 THE PH EFFECT: ANOTHER LOOK AT THE TURNOVER FREQUENCY OF DIFFERENT
ACTIVE SITES 103
2.6 CONCLUSIONS 105
ACRONYMS 106
ACKNOWLEDGMENTS 106
REFERENCES 107
3 MODIFIED CARBON MATERIALS FOR O
Z
REDUCTION REACTION ELECTROCATALYSTS
IN ACID PEM FUEL CELLS 119
DEEPILCA SINGH, JESAIAH KING, AND
LIMIT S. OZJCAN
3.1 INTRODUCTION 119
3.2 DOPED CARBON MATERIALS 119
3.2.1 NITROGEN-DOPED CARBONS
121
3.2.1.1 N-DOPED CNTS AND CNFS 122
3.2.1.2 N-DOPED FULLERENE 124
3.2.1.3 CARBON NITRIDES 124
3.2.1.4 GRAPHITIC CARBON NITRIDE 125
3.2.1.5 N-DOPED GRAPHENE 125
3.2.2 DOPING WITH OTHER HETEROATOMS 127
3.3 DOPED CARBONS AS ORR CATALYSTS 130
3.3.1 NITROGEN-DOPED CARBON MATERIALS PREPARED WITHOUT A METAL 139
3.4 CONCLUSIONS 140
ACKNOWLEDGMENT 141
REFERENCES 141
4 TRANSITION METAL CHALCOGENIDES FOR OXYGEN REDUCTION ELECTROCATALYSTS
IN PEM FUEL CELLS 157
KUNCHAN LEE, NICOLAS ALONSO-VANTE, AND JIUJUN ZHANG
4.1 INTRODUCTION 157
4.2 NON-NOBLE METAL CHALCOGENIDE ELECTROCATALYSTS FOR OXYGEN REDUCTION
REACTION 160
4.3 SYNTHESIS METHODS FOR NON-NOBLE METAL CHALCOGENIDES 163
4.3.1 NONORGANIC SOLVENT METHODS 164
4.3.2 ORGANIC SOLVENT METHODS AT LOW TEMPERATURE 165
4.4 OXYGEN REDUCTION REACTION ON NON-NOBLE METAL CHALCOGENIDES
168
4.4.1 MECHANISM OF OXYGEN REDUCTION REACTION 168
4.4.2 THEORETICAL APPROACH FOR ORR MECHANISM 172
4.5 METHANOL TOLERANCE 175
4.6 FUEL CELL MEASUREMENTS 177
4.7 CONCLUSIONS 178
REFERENCES 179
VIIII
CONTENTS
5 TRANSITION METAL OXIDES, CARBIDES, NITRIDES, OXYNITRIDES, AND
CARBONITRIDES FOR 0
2
REDUCTION REACTION ELECTROCATALYSTS FOR ACID PEM
FUEL CELLS 183
AKIMITSU ISHIHARA, HIDETO IMAI, AND KEN-ICHIRO OTA
5.1 INTRODUCTION 183
5.2 TRANSITION METAL NITRIDES AND CARBONITRIDES AS CATHODE
CATALYSTS 185
5.3 STABILITY OF OXIDES IN ACID ELECTROLYTE 186
5.4 NON-NOBLE METAL OXIDE-BASED CATHODE CATALYSTS 187
5.4.1 STABILITY OF GROUP 4 AND 5 METAL OXIDE-BASED CATALYSTS 187
5.4.2 FORMATION OF COMPLEX OXIDE LAYER CONTAINING ACTIVE SITES 188
5.4.3 SUBSTITUTIONAL DOPING OF NITROGEN 189
5.4.4 CREATION OF OXYGEN DEFECTS WITHOUT USING CARBON AND NITROGEN 191
5.4.5 OXIDATION OF COMPOUNDS INCLUDING CARBON AND NITROGEN 193
5.4.6 PERFORMANCE OF SINGLE CELL WITH OXIDE-BASED CATHODES 197
5.5 CONCLUSIONS 198
ACKNOWLEDGMENTS 198
REFERENCES 199
6 THEORETICAL MODELING OF NON-NOBLE METAL ELECTROCATALYSTS FOR ACID
AND ALKALINE PEM
FUEL CELLS 205
EBEN DY AND ZHENG SHI
6.1 INTRODUCTION 205
6.2 MECHANISMS OF ORR 205
6.2.1 ROLE OF THE CATALYST 206
6.2.2 EFFECT OF PH 208
6.3 SIMPLE METAL-N
4
MACROCYCLES 212
6.4 HEAT-TREATED TRANSITION METAL NITROGEN-CARBON PRECURSORS
(M-N
X
/C) 216
6.5 FUNCTIONALIZED GRAPHITIC MATERIALS 221
6.5.1 DOPED GRAPHENE MATERIALS 222
6.5.2 DOPED CARBON NANOTUBE MATERIALS 227
6.5.3 METAL-FUNCTIONALIZED GRAPHENE MATERIALS 229
6.6 CONDUCTING POLYMERS 232
6.7 OUTLOOK 235
REFERENCES 236
7 MEMBRANES FOR ALKALINE POLYELECTROLYTE FUEL CELLS 243
JING PAN, CHEN CHEN, AND LIN ZHUANG
7.1 INTRODUCTION 243
7.2 TWO MAIN CHALLENGES OF APES 244
7.2.1 PURSUING HIGH CONDUCTIVITY AS WELL AS LOW SWELLING DEGREE 244
7.2.2 HIGH CHEMICAL STABILITIES OF CATION GROUPS 244
7.3 APES REPORTED IN THE LITERATURE 245
7.3.1 HETEROGENEOUS APE MEMBRANES 246
CONTENTS
IIX
7.3.1.1 ION-SOLVATING POLYMERS 246
7.3.1.2 ORGANIC-INORGANIC HYBRID APE MEMBRANES 247
7.3.1.3 COMPOSITE APE MEMBRANE 248
7.3.2 HOMOGENEOUS APE MEMBRANES 249
7.3.2.1 FILM-MODIFIED APES 249
7.3.2.2 POLYMER-MODIFIED APES 250
7.3.2.3 MONOMER-POLYMERIZED APE 250
7.4 STRATEGIES FOR IMPROVING THE IONIC CONDUCTIVITY OF APE 254
7.5 EFFORTS OF IMPROVING THE CHEMICAL STABILITY OF THE CATIONIC
FUNCTIONAL
GROUP 258
7.5.1 CATIONIC GROUPS WITH CONJUGATED STRUCTURE 258
7.5.2 CATIONIC GROUPS WITH STRONG ELECTRON DONOR 260
7.6 RESEARCH ON THE CHEMICAL STABILITY OF APE BACKBONE 261
7.7 CONCLUSIONS AND PERSPECTIVE 261
REFERENCES 264
8 ELECTROCATAIYSTS FOR ALKALINE POLYMER EXCHANGE MEMBRANE (PEM) FUEL
CELLS - OVERVIEW 271
RONGZHONG JIANG AND DERYN CHU
8.1 INTRODUCTION 271
8.2 ALKALINE FUEL CELL OVERVIEW - HISTORY, STATUS, AND ADVANTAGES 272
8.3 ALKALINE FUEL CELL AND ALKALINE PEM FUEL CELL - THERMODYNAMICS
AND KINETICS 274
8.3.1 THERMODYNAMICS OF H
2
/0
2
FUEL CELL REACTIONS IN ALKALINE
ELECTROLYTE 274
8.3.2 KINETICS OF 0
2
REDUCTION IN ALKALINE FUEL CELLS 276
8.3.3 MECHANISMS OF OXYGEN REDUCTION AT NOBLE METAL SURFACE 279
8.3.4 MECHANISMS OF OXYGEN REDUCTION AT NON-NOBLE METAL SURFACE 282
8.3.5 KINETICS AND MECHANISMS OF H
2
OXIDATION 284
8.4 SILVER-BASED MATERIALS FOR CATHODE ELECTROCATAIYSTS IN ALKALINE PEM
FUEL CELLS 286
8.4.1 STARTING MATERIALS AND SYNTHESIS STRATEGIES FOR SILVER-BASED
ELECTROCATAIYSTS 287
8.4.1.1 CHEMICAL SYNTHESIS OF POWDER AG CATALYSTS 288
8.4.1.2 SOME SYNTHETIC METHODS FOR POROUS AG MEMBRANES AND POROUS
ELECTRODES 291
8.4.2 PHYSICAL AND ELECTROCHEMICAL CHARACTERIZATIONS 291
8.4.2.1 X-RAY POWDER DIFFRACTION (XRD) 291
8.4.2.2 X-RAY PHOTOELECTRON SPECTROSCOPY (XPS) 293
8.4.2.3 TRANSMISSION ELECTRON MICROSCOPY (TEM) 293
8.4.2.4 ELECTROCHEMICAL METHOD 295
8.4.3 SILVER-BASED CATALYSTS FOR ALKALINE PEM FUEL CELLS 297
8.5 CATALYSTS FOR OXIDATION OF A BROAD RANGE OF FUELS FOR ALKALINE PEM
FUEL CELLS 298
8.5.1 NON-CARBON FUELS AND SPECIFIC CATALYSTS FOR THEIR OXIDATION 298
X I CONTENTS
8.5.1.1 HYDROGEN 298
8.5.1.2 BOROHYDRIDE 298
8.5.1.3 HYDRAZINE 299
8.5.1.4 AMMONIA 299
8.5.1.5 SULFIDE 300
8.5.2 SINGLE-CARBON ORGANIC FUELS AND SPECIFIC CATALYSTS FOR THEIR
OXIDATION 300
8.5.2.1 METHANOL 300
8.5.2.2 FORMALDEHYDE 301
8.5.2.3 FORMIC ACID 301
8.5.3 ORGANIC FUELS CONTAINING CARBON-CARBON (C-C) BOND IN THE
MOLECULES AND SPECIFIC CATALYSTS FOR THEIR OXIDATION 302
8.5.3.1 ETHANOL 302
8.5.3.2 ETHYLENE GLYCOL AND DIMETHYL ETHER 303
8.5.3.3 OTHER ORGANIC FUELS CONTAINING TWO OR MORE C-C BONDS IN THEIR
MOLECULES 305
8.5.4 ELECTROCHEMICAL KINETICS AND MECHANISMS OF FUEL ELECTROOXIDATION
IN
ALKALINE MEDIA 305
8.6 MAJOR CHALLENGES OF ALKALINE FUEL CELLS AND ALKALINE PEM FUEL
CELLS 307
ACKNOWLEDGMENTS 309
REFERENCES 309
9 CARBON COMPOSITE CATHODE CATALYSTS FOR ALKALINE PEM FUEL
CELLS 319
QING LI AND GANG WU
9.1 INTRODUCTION 319
9.2 METAL-FREE CARBON CATALYSTS 321
9.2.1 NITROGEN DOPING INTO CARBON 322
9.2.2 NITROGEN-DOPED CARBON NANOTUBE CATALYSTS 324
9.2.3 NITROGEN-DOPED GRAPHENE CATALYSTS 325
9.2.4 OTHER HETEROATOM-DOPED CARBON CATALYSTS 328
9.3 HEAT-TREATED M-N-C (M: FE, CO) CARBON COMPOSITE CATALYSTS 330
9.3.1 HEATING TEMPERATURES 330
9.3.2 TYPE OF TRANSITION METALS 332
9.3.3 NITROGEN PRECURSORS 333
9.4 NANOCARBON/TRANSITION METAL COMPOUND HYBRID CATALYSTS 336
9.4.1 NANOCARBON/METAL OXIDES HYBRID CATALYSTS 337
9.4.2 CARBON/METAL CHALCOGENIDE HYBRID CATALYSTS 341
9.4.3 NANOCARBON/MACROCYCLE COMPOUND CATALYSTS 342
9.5 ORR MECHANISM ON NPMCS IN ALKALINE MEDIA 344
9.6 NPMC CATHODE PERFORMANCE IN ANION EXCHANGE MEMBRANE
FUEL CELL 346
9.7 SUMMARY AND PERSPECTIVE 348
REFERENCES 349
CONTENTS | XI
10 NON-PRECIOUS METAL OXIDES AND METAL CARBIDES FOR ORR IN
ALKALINE-BASED FUEL CELLS 357
WENLING CHU, DREW HIGGINS, ZHONGWEI CHEN, AND RUI CAI
10.1 INTRODUCTION 357
10.2 METAL OXIDES 359
10.2.1 MANGANESE OXIDES 360
10.2.2 OTHER METAL OXIDES 362
10.3 PEROVSKITE-TYPE OXIDES 364
10.3.1 EFFECT OF A- AND B-SITE CATIONS 365
10.3.2 EFFECT OF PREPARATION METHODS 368
10.3.3 DURABILITY OF PEROVSKITE-TYPE OXIDES 370
10.3.4 DESIGN PRINCIPLES FOR ORR ACTIVITY ON PEROVSKITE-TYPE OXIDES 371
10.4 SPINEL-TYPE OXIDES 372
10.5 METAL CARBIDES 377
10.6 CONCLUSION AND OUTLOOK 379
REFERENCES 380
11 AUTOMOTIVE APPLICATIONS OF ALKALINE MEMBRANE FUEL CELLS 389
HIROHISA
T
ANAKA,
KOICHIRO
ASAZAWA, AND TOMOKAZU SAKAMOTO
11.1 INTRODUCTION 389
11.2 HISTORY OF ALKALINE FUEL CELLS IN AUTOMOTIVE APPLICATIONS 392
11.3 FUEL USED IN MODERN ALKALINE PEM FUEL CELLS IN AUTOMOTIVE
APPLICATIONS 395
11.4 COMPONENTS OF AN ALKALINE PEM FUEL CELL MEMBRANE ELECTRODE
ASSEMBLY FOR AUTOMOTIVE APPLICATIONS 398
11.4.1 ANODE CATALYSTS FOR THE DIRECT HYDRAZINE FUEL CELL VEHICLE 398
11.4.2 CATHODE CATALYSTS 404
11.4.3 MEA PERFORMANCE USING NON-NOBLE METAL CATALYSTS 407
11.5 MAJOR CHALLENGES TO OVERCOME IN ALKALINE PEM FUEL CELLS 414
11.6 CONCLUSION 416
ACKNOWLEDGMENTS 417
REFERENCES 418
INDEX 423 |
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| discipline | Chemie / Pharmazie |
| format | Book |
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| id | DE-604.BV041886226 |
| illustrated | Illustrated |
| indexdate | 2024-09-10T01:15:41Z |
| institution | BVB |
| isbn | 352733324X 9783527333240 9783527664917 9783527664924 9783527664931 |
| language | English |
| oai_aleph_id | oai:aleph.bib-bvb.de:BVB01-027330242 |
| oclc_num | 864645896 |
| open_access_boolean | |
| owner | DE-703 DE-29T |
| owner_facet | DE-703 DE-29T |
| physical | XVIII, 428 S. Ill., graph. Darst. |
| publishDate | 2014 |
| publishDateSearch | 2014 |
| publishDateSort | 2014 |
| publisher | Wiley-VCH |
| record_format | marc |
| spelling | Non-noble metal fuel cell catalysts ed. by Zhongwei Chen ... Weinheim Wiley-VCH 2014 XVIII, 428 S. Ill., graph. Darst. txt rdacontent n rdamedia nc rdacarrier Polymer-Elektrolytmembran-Brennstoffzelle (DE-588)4450903-0 gnd rswk-swf Metall (DE-588)4038860-8 gnd rswk-swf Katalysator (DE-588)4029919-3 gnd rswk-swf Polymer-Elektrolytmembran-Brennstoffzelle (DE-588)4450903-0 s Katalysator (DE-588)4029919-3 s Metall (DE-588)4038860-8 s DE-604 Chen, Zhongwei (DE-588)1052279902 edt Erscheint auch als Online-Ausgabe 978-3-527-66490-0 X:MVB text/html http://deposit.dnb.de/cgi-bin/dokserv?id=4485861&prov=M&dok_var=1&dok_ext=htm Inhaltstext DNB Datenaustausch application/pdf http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027330242&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA Inhaltsverzeichnis |
| spellingShingle | Non-noble metal fuel cell catalysts Polymer-Elektrolytmembran-Brennstoffzelle (DE-588)4450903-0 gnd Metall (DE-588)4038860-8 gnd Katalysator (DE-588)4029919-3 gnd |
| subject_GND | (DE-588)4450903-0 (DE-588)4038860-8 (DE-588)4029919-3 |
| title | Non-noble metal fuel cell catalysts |
| title_auth | Non-noble metal fuel cell catalysts |
| title_exact_search | Non-noble metal fuel cell catalysts |
| title_full | Non-noble metal fuel cell catalysts ed. by Zhongwei Chen ... |
| title_fullStr | Non-noble metal fuel cell catalysts ed. by Zhongwei Chen ... |
| title_full_unstemmed | Non-noble metal fuel cell catalysts ed. by Zhongwei Chen ... |
| title_short | Non-noble metal fuel cell catalysts |
| title_sort | non noble metal fuel cell catalysts |
| topic | Polymer-Elektrolytmembran-Brennstoffzelle (DE-588)4450903-0 gnd Metall (DE-588)4038860-8 gnd Katalysator (DE-588)4029919-3 gnd |
| topic_facet | Polymer-Elektrolytmembran-Brennstoffzelle Metall Katalysator |
| url | http://deposit.dnb.de/cgi-bin/dokserv?id=4485861&prov=M&dok_var=1&dok_ext=htm http://bvbr.bib-bvb.de:8991/F?func=service&doc_library=BVB01&local_base=BVB01&doc_number=027330242&sequence=000001&line_number=0001&func_code=DB_RECORDS&service_type=MEDIA |
| work_keys_str_mv | AT chenzhongwei nonnoblemetalfuelcellcatalysts |